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1 CTETS 67 Website address: Indian Journal of Chemistry Sect. B: rganic Chemistry including Medicinal Chemistry VL. 50B UMBE 1 January 011 CTETS apid Communication 73 Enantiospecific approach to AB-ring system of the diterpenes fusicoccanes Enantiospecific synthesis of AB ring system of the tricyclic diterpenes fusicoccanes has been described. A B C A B CM fusicoccanes 1 CEt limonene A Srikrishna* & Gopalasetty agaraju Department of rganic Chemistry, Indian Institute of Science, Bangalore , India Papers 77 An efficient synthesis of symmetrical, -alkylidene bisamides catalyzed by phosphortungstic acid Symmetrical, -alkylidene bisamides have been synthesized by condensation of aromatic aldehydes and amides in the presence of phosphotungstic acid as a catalyst under thermal and neat microwave irradiation conditions. C + Phosphotungstic acid Toluene, eflux, 0-7 h Gurusamy arichandran*, Savarimuthu DavidAmalraj & Ponnusamy Shanmugam Department of Polymer Science, University of Madras, Guindy Campus, Chennai , India IDIA J CEM, 50B (1)011
2 68 83 Synthesis, configurational analysis and antimicrobial activity of imidazolidinone, thiazolidinone and isoxazolone derivatives of 9,10-phenanthrenequinone A facile synthesis of imidazolidinone, thiazolidinone and isoxazolone derivatives has been described by Knoevenagel type condensation reactions of 9,10-phenanthrenequinone with active methylene heterocycles/compounds. The products have been characterized by spectral data. Semiempirical studies have been performed to understand the stereochemical course of the reaction. Some of the synthesized products have been screened for antimicrobial activity. Y Y + Komal Arora, Sonali Verma, ahul Joshi, P Pardasani & T Pardasani* Department of Chemistry, University of ajasthan, Jaipur , India 89 Conventional as well as microwave assisted synthesis and antimicrobial screening of 4-aryl-3- chloro-1-[(5-nitroindazol-1-yl) acetamido]--oxoazetidines Several new 4-aryl-3-chloro-1-[(5-nitroindazol-1-yl) acetamido]--oxo-azetidines, 4a-l have been synthesized from -(5- nitroindazol-1-yl) acetamidyl amino arylidenes, 3a-l. The reactions have been carried out by both conventional as well as microwave method. All the synthesized compounds have been screened for their antibacterial and antifungal activity against some selected micro organisms. C C = C (3a-l) Ar (4a-l) C C CAr Cl Where Ar = Substituted aryl groups Apoorva Upadhyay*, S K Srivastava, S D Srivastava & Yadav Synthetic rganic Chemistry Laboratory, Department of Chemistry, Dr.. S. Gour University (A Central University), Sagar , India IDIA J CEM, 50B (1) 011
3 CTETS 69 otes 98 Synthesis of 4-(3)-quinazolinones by microwave assisted tandem reaction and evaluation of their antibacterial and antifungal activities A one pot synthesis of quinazolinone derivatives from the reaction of anthranilic acid and primary aromatic amines with Vilsmeier reagent (DMF/PCl 3 ) has been carried out under microwave irradiation. All the synthesized compounds have been screened for their in vitro antibacterial and antifungal activity. 1. PCl 3 / DMF C. 1 a-j 3a-j M Gnana uba Priya, Y Zulykama, K Girija, S Murugesh & P T Perumal* Department of Biotechnology, Sastra University, Thanjavur , India 103 Application of -(1-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium tetrafluoroborate (TBTU) for the synthesis of acid azides Acid azides have been efficiently prepared from carboxylic acids employing peptide coupling agent TBTU. The protocol is extended to synthesize urethane protected amino acid azides also. -C TBTU, DIPEA a 3 in DMS alkyl, aryl carboxylic acids at 0 o C and -protected α-amino acids -C 3 acid azides Shankar A aik, Lalithamba S & Vommina V Sureshbabu* Peptide esearch Laboratory, Department of Studies in Chemistry, Central College Campus, Bangalore University, Dr. B.. Ambedkar Veedhi, Bangalore , India 110 Green synthesis of -amino-5-substituted-1,3,4- oxadiazoles at the platinum anode in acetic acid The electroorganic synthesis of -amino-5-substituted-1,3,4- oxadiazoles from the anodic oxidation of semicarbazone have been carried out at platinum anode in acetic acid under constant potential electrolysis in an undivided cell. 1 C + C 1 Electrocyclization 1 Laxmi Kant Sharma, Sushma Singh & K P Singh* Electrochemical Laboratory of Green Synthesis, Department of Chemistry, University of Allahabad, Allahabad 11 00, India IDIA J CEM, 50B (1)011
4 Phenolic constituents from the galls of Pistacia integerrima Stewart Phytochemical investigation of the galls of Pistacia integerrima Stewart (Pistaceaceae) has yielded three new phytoconstituents characterized as 14 -phenoxytetradecanyl 3,5- dihydroxybenzoate (pistiphloroglucinyl ester), 4 -phenoxy-nbutyl-1 -(3-oxy-5-hydroxy) -benzoic acid (pistaciaphenyl ether) 3 and 3 -(1,3-dihydroxy-5-phenoxy-1,5 -dimethoxybenzene (pisticiphloroglucinyl ether) 4 along with the known compound ß- sitosterol 1. 7 C C 1 ' C C ' 1 " 6 1 " Shamim Ahmad, Mohammed Ali* & Shahid Ansari Phytochemical esearch Laboratory, Department of Pharmacognosy and Phytochemistry, Faculty of Pharmacy, Jamia amdard, amdard University, ew Delhi , India 119 An efficient synthesis of 3-chloromethyl-1,-benzisoxazoles via modified Boekelheide rearrangement An efficient and simple method for preparation of 3- chloromethyl-1,-benzisoxazoles by modified Boekelheide rearrangement using phosphorous oxychloride and TEA in moderate to good yield PCl 3 3 Cl TEA Veera eddy Arava*, Laxminarasimhulu Gorentla, Uday Bhaskara ao Siripalli & Pramod Kumar Dubey 1 1 & D Laboratories, SUVE Life Sciences Ltd., #18, Phase III, Jeedimetla, yderabad , India IDIA J CEM, 50B (1) 011
5 CTETS A convenient and simple transformation of acid hydrazides to, -diacylhydrazines with g (Ac) under solid state conditions A highly efficient and practical methodology for the transformation of acid hydrazides 1 to, -diacylhydrazines is described under solid state conditions at T utilizing inexpensive and easily available reagent g(ac) with good yields + g(ac) Grinding 1 K Mogilaiah*, E Anitha, K Shiva Kumar & Shiva Prasad Department of Chemistry, Kakatiya University, Warangal , India Authors for correspondence are indicated by (*) IDIA J CEM, 50B (1)011
Indian Journal of Chemistry
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