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1 1231 Website address: Indian Journal of Chemistry ect. B: rganic Chemistry including Medicinal Chemistry VL. 53B UMBE0 ctober 2014 Papers 1237 ew isoquinoline alkaloids from the stem bark of Berberis aristata Javed Ahamad, Kamran J aquvi, Mohd Ali & howkat R Mir* Phytochemistry Research Laboratory, Department of Pharmacognosy and Phytochemistry, Faculty of Pharmacy, Jamia amdard, ew Delh , India
2 ne pot synthesis of 4-(arylidene)-2-[5-(4-hydroxy-6- methyl-2-oxo-2-pyran-3-yl)-thiazol-2-yl]-5-methyl- 2,4-dihydro-pyrazol-3-ones via multi-component approach An efficient, one pot, four-component approach for the synthesis of 4-(arylidene)-2-[5-(4-hydroxy-6-methyl-2-oxo-2-pyran-3-yl)-thiazol-2-yl]-5-methyl-2,4-dihydropyrazol-3-ones has been described. This synthesis involves the simultaneous formation of thiazole and pyrazole ring systems followed by condensation of different aldehydes on active methylene group of pyrazolone under Knoevenagel reaction conditions. Tewodros Birhanu Aychiluhim, anthosh Penta & Vedula Rajeswar Rao* Department of Chemistry, ational Institute of Technology, Warangal , India 1247 A facile clean synthesis of pyrido [2,3-d] pyrimidine and their derivatives in ionic liquids ynthesis of pyrido[2,3-d]pyrimidine derivatives is described. The synthesized compounds have been characterized by IR, 1 and 13 C MR and elemental analysis. C 3 4 1a-d IL + C 2 () 2 C R 1 2 3a-d C 2 4a-d BrC 2 C 2 C ClC 2 C 6a-d 5a-d 7a-d Ashok K Yadav* & Manisha Gupta Department of Chemistry, University of Rajasthan, Jaipur , India
3 UV-Vis spectrophotometry plus PLC to measure the level of catechin / poly- phenolics and to understand its oxidized conditions in commercially available green and black teas Catechin ankar P Mitra Acotrix Inc. 100 Berber Avenue, Worcester, MA 01606, UA 1263 ynthesis, characterization and antimicrobial activity of 2-(11-oxodibenzo [b,f][1,4]thiazepin-10(11)-yl)- (substituted phenyl) acetamide derivatives 2-(11-xodibenzo [b,f][1,4]thiazepin-10(11)-yl)- (substituted phenyl) acetamide (A 1-13 ), 2-chloro-(substituted) phenyl acetamide attached to 11 position of dibenzo [b,f][1,4]thiazepin-11 (10) -one 4 have been synthesized in the presence of sodium hydride. Jitesh Tailor, Priti C Patel & G M Malik* Department of Chemistry, avyug cience College, Rander Road, urat , India
4 A simple and highly efficient process for synthesis of Gefitinib and its intermediate A highly efficient one pot conversion of 4-methoxy-3-benzyloxy-6- nitro benzoate to 6-benzoyloxy-7-methoxy quinazoline-4-one using Fe/acetic acid and formamidine acetate followed by debenzylation of 4-(3-chloro-4-flurophenylamino)-6-benzoyloxy-7-methoxy quinazoline using methanesulfonic acid in chloroform is described. F CC 3 2 Cl eeraj Kumar*, Anil Chowdhary, mprakash Gudaparthi, ilesh G Patel, anjay K oni & Pradeep harma Chemical R & D, Cadila Pharmaceuticals Ltd., 1389, Trasad Road, Dholka, Ahmedabad , India 1275 ynthesis of novel isoxazolo[2'',3'':1',2']pyrimido [4',5':4,5]pyrimido[6,1-b]quinazoline-8-ones and their in vitro anticancer and antimicrobial activities C C + ethanol, pta reflux, 2h 2 C DMF-DMA, Ac, ethanol reflux 2h C 3 C 3 Anthranilic acid reflux, 2h C 3 C3 6 5 E Rajanarendar*, B Kishore, Ramakrishna, D agaraju & P Venkateshwarlu Department of Chemistry, Kakatiya University, Warangal , India
5 1235 otes 1284 Lupane-triterpenoids from stem bark of Dillenia indica From the methanol extract of the stem bark of Dillenia indica, one new triterpene acid ester,dillenic acid 1 along with four known compounds, betulinic acid 2, 3-epi- betulinic acid 3, 3-epidihydrobetulinic acid 4 and 3α-hydroxy-lup-20(29)-en-23,28-dioic acid 5 have been isolated. tructure of the new compound 1 is elucidated on the basis of detailed spectroscopic (including 2D MR) and chemical studies. Compound 3 is reported for the first time as natural product and compounds 2 and 4 are reported for the first time from this plant. Partha arathi Ghosh, Indrajit il arma, oriko ato, Yoshihiro arigaya & Biswanath Dinda* Department of Chemistry, ational Institute of Technology, Agartala, Jirania , India 1288 Catalyst-free access to pseudo multi-component synthesis of benzopyranopyrimidines A catalyst-free multi-component reaction of salicylaldehyde, malononitrile and secondary amine that leads to the formation of benzopyranopyrimidine framework with intense fluorescence emission behavior is described. The method is simple and suggests broad applicability of the protocol. 2 R' R R + C C 2 5 R' R R R' T haikh, J D Patil, D Gaikwad, P G egade, P B Patil, K A Undale, M M Mane & D M Pore* Department of Chemistry, hivaji University, Kolhapur , India
6 ynthesis of a new class of bis heterocycles A variety of bis heterocycles-oxazolyl / thiazolyl / imidazolyl pyrroles and pyrazoles have been prepared adopting 1,3-dipolar cycloaddition of tosylmethyl isocyanide and diazomethane to oxazolyl / thiazolyl / imidazolyl acryl amides. X 7/8/9 X 1/2/3 Cl X 13/14/15 1,7,13: X = 2,8,14: X = 3,9,15: X = = a) Ph b) 4-Me.Ph c) 4-Cl.Ph Venkatapuram Padmavathi*, Tumma reelatha, Putta Ramachandra Reddy & Kuppireddygari Divya Department of Chemistry, ri Venkateswara University, Tirupati , India Authors for correspondence are indicated by (*)
Indian Journal of Chemistry
263 Website address: www.niscair.res.in; http://nopr.niscair.res.in Indian Journal of Chemistry ect. B: rganic Chemistry including Medicinal Chemistry VL. 51B UMBE 1 January 2012 apid Communication 269
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