TOWARDS THE CREATION OF A EUROPEAN INSTITUTE OF HYDROMETALLURGY NOVEMBER 2012
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1 TOWARDS THE CREATION OF A EUROPEAN INSTITUTE OF HYDROMETALLURGY NOVEMBER 2012
2 CONTEXT AND OBJECTIVES OF THE PROJECT Critical Minerals are strategic elements for Europe Economy Europe is dependant on imports for its critical material supply which demand increases as a result of their increasing use in New Technologies Applications Europe is evolving to adapt to the new situation, with, for example, the Horizon 2020 funding scheme, which will encompass up to 3.2 b for raw materials issues Hydrometallurgy is a technical solution towards increasing recovery from existing critical mineral ores or recycled materials To cover the increased needs for non energetic raw materials, new resources (primary and secondary deposits, resources issued from recycling) must be exploited; those are often lower grade and polymetallic ores, for which conventional purification techniques (Pyrometallurgy) might not be best as well suited as Hydrometallurgy As a state owned Research and Development organism, created in 1945, to ensure national security and scientific and technological work in the nuclear field; the CEA 1, together with its industrial partners, has developed strong competences and skills in hydrometallurgy and industrial project management. In this context, we wish to federate the creation of a European Institute of Hydrometallurgy strongly linked to Marcoule Ensure independent R&D on hydrometallurgy in Europe Make the best synergy and use the R&D capitalization knowledge from nuclear to innovative and complex domains. Achieve EU s ambitious goals concerning extraction (versatility, flexibility, sustainability) and recycling of critical materials. Around 120 persons Process development lab Pilot scale plateform Training professionals 1 Commissariat à l Energie Atomique et aux Energies Alternatives / Atomic Energy and Alternative Energies Commission Marcoule PAGE 2
3 OBJECTIVES OF THE INTERVIEW Understand Your needs with regards to R&D services for the pre-industrialization of new hydrometallurgical processes Your level of satisfaction with your current practices (internalization, subcontracting, others ). Listen to your feedback regarding the creation of a European Institute of Hydrometallurgy and validate that the Institute s offer would match your needs and expectations. Assess if you would be interested in a collaboration with the European Institute of Hydrometallurgy, as a partner or as a customer. PAGE 3
4 A EUROPEAN INSTITUTE OF HYDROMETALLURGY : 120 PEOPLE, MEANS & SERVICES Process development lab R&D at the lab scale Micro-pilot (integrated tests) Online process tracking INNOVATE 24h/24 Pilot test platform Continuous process development Physico-chemical feasibility and robustness Instrumented test lines Process Life-cycle Management Simulation expertise & tools From the lab to the pilot test Transient modeling software Chemical databases Processes modeling TRANSFER Fit for purpose R&D services Provide technical expertise at all levels of the development process and at all scale From lump-sum turnkey deliveries to comprehensive operational support From detailed process research & development to industrial scale-up expertise TRAIN Professional education & training Provide professional training for all level of the organization based on a wide academic network PAGE 4
5 SOME FEATURES OF THE 5,000 M 2 TEST FACILITIES Testing Modular Halls Equipment designed to perform any process steps (leaching tanks, mixer-settler, agitated columns, precipitators, electrolyser) Online instrumentation for real-time process piloting Laboratories in support of thetesting Halls Chemical analysis services Research & Development Laboratories in support of pilot trials EIH Utilities and materials management Preparation hall for treatment of material batchs Workshops, equipment and accessories storage Utilities space (gas reactants, demineralized and cold water, steam, compressed air) Treatment rooms of liquid and gaseous effluents Operation by test campaigns Duration 1-12 weeks continuously (24/24, 7/7) Processing capacity: up to 50 kg/h PAGE 5
6 SKILLS AND EQUIPMENT AVAILABLE TO ASSIST IN HYDROMETALLURGY PROCESS DEVELOPMENT Pretreatment Leaching Metal Recovery Eflluent management Skills Typical Equipment Crushing mills Rotary ovens Modeling/Simulation, for development cost saving and to limit trials PROPRIETARY SOFTWARE: transient modeling software with chemical database, liquid/liquid extraction and other hydrometallurgical processes modeling (process tracking, sensitivity analysis, safety with new molecules, rapidity of simulation, process optimization, analytical control ) Analytical tools, supporting R&D GC/LC, ICP, MS, XRF Generic Competencies Chemical Engineering Fluid mechanics Analytical chemistry and analytical techniques Process modeling Materials Engineering Operating system Structural Chemistry From Concentrate, ores, mattes/laterites, fines, Leaching Tanks : 600L Reactors/autoclaves 600L Bioreactors Clarifiers : 20L/h Leaching columns up to Ø500 mm PRECIPITATION Thickeners (Ø500 mm) Reactors Solid/liquid extraction Precipitation Columns 10kg/h Membrane processes/reverse osmosis/nanofiltration Micro-algae decontamination Environmental expertise Liquid/Liquid Solid/liquid Electrochemistry extraction extraction Electrochemistry Solvent Mixer-settlers with Extraction Resin columns Tankhouse equipment optimized agitating systems (up to 100L/hr) Pulsed columns (from Ø15mm to Ø100mm) Reactors 200L and processes, cathode stripping machine, polymer concrete cells, From tube test to modeling and preindustrial work : a powerful and innovative science Extracting molecule selection Characterization of extractant properties Models development Process flowsheet design for selected molecules Devices experimentation Flowsheet test works Understanding at the atomic scale of the interactions between metal and extracting molecules PAGE 6
7 A THOROUGH UNDERSTANDING OF MANY CHEMICAL ELEMENTS CEA has a deep expertise in chemistry separation of different significant elements, such as Rare Earths, Uranium, Plutonium, coming from historical and current activities 1 H 2 He 3 Li 4 Be 5 B 6 C 7 N 8 O 9 F 10 Ne 11 Na 12 Mg 13 Al 14 Si 15 P 16 S 17 Cl 18 Ar 19 K 20 Ca 21 Sc 22 Ti 23 V 24 Cr 25 Mn 26 Fe 27 Co 28 Ni 29 Cu 30 Zn 31 Ga 32 Ge 33 As 34 Se 35 Br 36 Kr 37 Rb 38 Sr 39 Y 40 Zr 41 Nb 42 Mo 43 Tc 44 Ru 45 Rh 46 Pd 47 Ag 48 Cd 49 In 50 Sn 51 Sb 52 Te 53 I 54 Xe 55 Cs 56 Ba 72 Hf 73 Ta 74 W 75 Re 76 Os 77 Ir 78 Pt 79 Au 80 Hg 81 Tl 82 Pb 83 Bi 84 Po 85 At 86 Rn 87 Fr 88 Ra LANTHANIDES 57 La 58 Ce 59 Pr 60 Nd 61 Pm 62 Sm 63 Eu 64 Gd 65 Tb 66 Dy 67 Ho 68 Er 69 Tm 70 Yb 71 Lu ACTINIDES 89 Ac 90 Th 91 Pa 92 U 93 Np 94 Pu 95 Am 96 Cm 97 Bk 98 Cf 99 Es 100 Fm 101 Md 102 No 103 Lr PAGE 7
8 ASSETS OF THE SITE OF MARCOULE An Industrial & Academic Site of Reference Marcoule Two renowned research organizations: CEA and ICSM R&D at different stages of hydrometallurgical process : development of extracting molecules, separation techniques, development of decontamination processes Collaborations with Labex CHEMISYST, BRGM, COMES (French Committee for strategic materials) International recognition of R&D Ability to carry out large projects (including EU-wide) Extensive experience in favor of industrial activities. Support of the mining activities of Areva and of fields using rare metals (Renewable energies techno., ICT...). Ability to develop processes from the laboratory to the plant, in collaboration with one or more industrial partners Capacity to set up new platforms CEA Marcoule Key Figures 1500 employees 700 researchers included 100 PhD/Doctors 500 Millions annual budget 30 research laboratories 260 priority patents delivered and alive 300 annual scientific publications 1 ISCM Marcoule Key Figures Mix unity of research between CEA, CNRS, ENSCM and UM2 ~70 employees including ~20 PhD/postdocs 20 Millions support from partners and contractors Axis of research: Green chemistry, understand separation, methods and theory, anticipation of life-cycle and optimization of separation. 1 Institut de Chimie Séparative de Marcoule / Marcoule Institute for Separative Chemistry PAGE 8
9 CEA HYDROMETALLURGICAL SUCCESS STORIES From CEA to the Recycling Plant, La Hague Collaboration AREVA/CEA nuclear reprocessing method for the recovery of uranium and plutonium from spent nuclear fuel. CEA contributions: Full development from the lab scale to the industrial scale of all the processes, technologies to the pilot Development of the process modeling code (PAREX) for the liquid / liquid extraction steps of the PUREX process Successful lab test, performances validation and elaboration of a new process to purify uranium for Malvesi refinery Development of an innovative eco-friendly waste recycling process Minimization of experiments and industrial extrapolation thanks to PAREX Conception of extraction operating equipment at the industrial scale Characterization of the flow from the lab scale to the industrial scale Development of a new precipitation reactor for liquid waste treatment Process intensification: installation size reduced, higher decontamination efficiency, reduction of sludge volumes PAGE 9
10 CONTACTS Christine ROSTAING EIH Project Manager CEA, Nuclear Energy Direction (DEN) CEA Marcoule, BP Bagnols sur Cèze Tel: + 33 (0) christine.rostaing@cea.fr Marie-Noelle DESSINGES Technology Transfer Officer CEA Tech Technology Transfer Office CEA Grenoble, Grenoble Cedex Tel: + 33 (0) marie-noelle.dessinges@cea.fr PAGE 10
11 PRESENTATION OF CEA ATOMIC ENERGY AND ALTERNATIVE ENERGIES COMMISSION French leading technological research organisation, from fundamental research to applied research Technology Defense Security Military Applications Division Nuclear Energy Nuclear Energy Division Key technologies Technological Research Division CEA key figures employees 10 research centres 4,3 b budget 1608 priority patents delivered and alive >650 priority patents filing Science Fundamental Research Physical Science Division Life Science Division 150 start-up since 1984 in innovative technologies Mission DAM : French strategic independance Mission DEN : French energetic independance Mission DRT : French industrialisation by innovation Marcoule PAGE 11
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