ICP Test Report Certification Packet

Transcription

1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - FKS Product #: xxx Series Issue Date: November 17, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the FUSE - FKS RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks:. 1 Form Rev. A 2/21/06

2 Table 1: List of Raw Materials covered by this report Total Parts Raw Material Part Number Raw Material Description Page(s) xxxx Melting Element xxxx FKS Housing FKS Housing - Colorant FKS Socket Terminal FKS Socket Terminal FKS Cover

3 For Please Test Report No. : CE2011l10412A Dale : Page:1ofI ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH t[]tiltt][ltttl l GEWERBESTRASSE 87, D VEILSDORF, GERMANY The tollowing sample(s) waa/were submitted and identified by/on behalf of the client as : Sample De6cdption Style/ltem No. Country of Origin Sample Receiving Date Testing Period COPPER NICKEL ALLOY WIRES, NICKEL PLATED WIRES (1\ TUNGSTEN - TINNED WIRE - W, Sn t2\ o--- EWN COPPER - NICKEL 44 ALLOY (CONSTANTAN) WIRE - CuNi44 (3) EWN COPPER - NICKEL-ZINC -ALLOY WIRE (NS 18). CuNi182n20 (4) COPPER - NICKEL -ALLOY WIRE - CuNi 2 (5) COPPER - NICKEL -ALLOY WIRE - CuNi 12 (6) COPPER - NICKEL -ALLOY WIRE - CuNa 6 (n COPPER - NICKEL -ALLOY WIRE - CuNi 22 (8) IRON - NICKEL -ALLOY WIRE - FeNi36 (lnvar) (9) 10,1.0125,0-. COPPER. MANGANESE - NICKEL -ALLOY WIRE - CuMnl2Ni GERMANY 2011tO1tU 2011tO1tUrO 2011t01n1 Taet Re3ult(s) Please refer to next page(s). tgndlb. d Oird.d Lffiry-TrF.l 'ni[9lsll po1]3l ron ylo1b3ampq,b*dlh3l.d@d mdbe comeany irr,,1,.r 1,1,r,1ii, r,ir,rll,!ld r-rr1.i-$41!-!i...,. ]t{r{ ny suqsd b c c4 cond itrs d s subrd ro Tams ad cdrm. tu E only,id*lhlnlmimgdc 6dti3' nolb.loplducdd.opl'nlu].llfud

4 Test Report No. : CE/2011/ Dale : Page:2of9 ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH l [tt]l[tttt]l GEWERBESTMSSE 87, D VEILSDORF, GERI'ANY Test Rasult(s) PART l.lame No. 1 MIXED ALL COLOR IVETAL WIRE (NCLUDING THE PLATING LAYER) (9 KIS) T65t ltom (s): Unit Method T$DL Re3ult No.1 Cadmium (Cd) mg/kg With reference to IEC : n.o and p r{orm d by ICP.AES. Lead (Pb) m!/kg With reference to IEC 62321: 2 n.d and perfomed by ICP-AES. Mercury (Hg) mg/kg With reference to IEC : 2 n.d and performed by CP4ES. Hexavalent Chromium Cr(Vl) by Spotest / boiling wate. With reference to IEC 62321: 2008 and perfomed by Spot test / 0.02mg/kg Negative with 50 cmz extraction boiling water extraction Me'thod. surface (See Note 5) area Perf luorooc.tane sulf onates mg/kg With referenc to US EPA 3g0C: 10 n.o. (PFOS) '1996 method for PFOS Content. PFOS - Acid Analysas w s perfomed by PFOS - Metal Salt LC/MS. PFOS -Amide PFOA {CAS No.: ) mg/kg With reference to US EPA 3540C: '10 n.d method for PFOA Conlent. Analysis was p rfomed by LC/MS. Halogen Halogen-Fluorine (F)(CAS No.: ' 50 n.d. Halogen-Chlorine (Cl)(CAS No.: 50 n.d ) With reference to BS EN mg/kg 14582:2007. Analysis w s Halogen-Bomine (Br)(CAS No.: pedormed by lc. 50 n.o, ) Halogenlodine (l)(cas No.: 014fi244-8) 50 n.d. s(3) tdd rh6 Gn rcpd 6nd b G cohr.^yr.jf,ili;i..-rlll: 'rrl1r:l i ]]rlrl{:, g * /.i:.rirl!'tl1!r'u}, ^ 9[].'l' ft.';d;"d."*.dbylh.c"np,.y3ufdb6cme]cdnd1h.sds r- d6dec io*d d;'.d' ''.iq.i o i.'",t c*or-' or e,"amr*r**01,,*oo geian myandu hilheimgolce.ls'nskdio^5.fa^y1hcmpsys9glspoi3b'9alobc 6la^d!lsd u. $";,'ehb and obrs6r -s -d* ib 'd il+mrc),ttts I t *6rcrr!!!t wwret@f

5 Test Report No. I CE201'1/10412A Da'.e Page:3ofg ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH GEWERBESTMSSE 87, D-S8669 VEILSDORF, GERMANY ll II tttl lt Test ltom (s): Unlt Method MOL Resu!t No.l Sum of PBBs n.o. Monobromobiphenyl 5 n.d. Dibromobiphenyl n.d. Tribromobiphenyl n.d. Tetrabromobiphenyl 5 n.d- Pentabomobiphenyl 5 n.d. Hexabromobiphenyl 5 n.d. Heptab.ornobiphenyl 5 n.o. Octabromobiphenyl 5 n.o. Nonabromobiphenyl n.d. Decabromobiphenyl With reference to IEC mgkg 62321: n.d. Sum of PBDES 2008 and perfomed by GC/MS. n.d. Monobromodiphenyl ether n.d. Dibromodiphenyl ether 5 n.d. Tribrcmodiphenyl ether n.d. Tet bromodiohenvl ether 5 n,d, Pentabromodiphenyl ether n.o. Hexabfomodiphenyl ether n.d. Heptabromodiphenyl eth r n.d. Octabrcmodiohenvl ether 5 n.d. Nonabromodiphenyl elher 5 n.d. Oecabromodiphenyl ether 5 n.d. cmfnv F:rL r,:;.ji r..r.rii tr!l,;t:, irrrir9{ ri!:jn}q.lf :ii1.,,,,ilsrt ysub]dbbgsb condle6ois poi3b 9tro 6 c!6l and b s em

6 Test Report No.: CE A Date:2O11101h1 Page: 4 of g ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GIIBH GEWERBESTRASSE 87, D VEILSDORF, GERMANY l[ lt][tltllll Note : 1. mg/kg = ppm; 0.1wf/o = 1000ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4."-"=NotRegulated 5. Soot-test: Negative = Absence of Cr(Vl) coating / surface layer, Positive = P sence of Cr(Vl) coating / surface layer; (The te6ted sample should be further veritied by boiling-water-extraction method if the spotest result cannot be confirmed.) Boi lin g-\i/eter-extraction: Negative = Absence of Cr(Vl) coating / surface layer. Positive = Presence of Cr(Vl) coating / surface layer; the detecled concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50 cm2 sample surface area. 6. " = Qualitative analysis (No Unit) 7- The sample(s) waslrcre an lyzed on behalf of the applicant as mixing sample in onetesting. The above result(s) warlr re only given a6the infomality value. PFOS Reference lntormation : Directive 20O6/I2ZEC (1) May not be placed on the market or used as a substance or constituent of preparations in a concentraiion equ lto or higherthan /6 by mass. (2) May not be placed on the market in gemi-finished producls or articles, or pa.ts thereof, if the concentration of PFOS is equalto or higherthan 0.1 % by m ss calculated with rcference to the mass of shuc'turally or microstruclurally distinct parts that contain PFOS or, for textiles or other coated material6, if the amount of PFOS is equal to or higher than lyg/m2 of the coated material..jilit. t!i; irrjui:lri...i[,:r!r1... r:;:;t,:. ^!i lutiu nysuqsd b G6sErcodltrsd s nsby6ioisc ; rlr h;,,ir336ior)rrq

7 Test Report No. : CE/2011/10412A Date: 2011/0'1/11Page:5of9 ELSCHUKOM ELEfi ROSCHUTZKOMPONENTENBAU GMBH GEWERBESTRASSE 87, D VEILSDORF. GERIIANY 1) These samples were disgolved totally by preronditioning method acco.ding to belo\tflor/ chan. ( Cf- test method excluded ) 2) Name of the person who made measurement: Climbgreat Yang 3) Name of the p rson in charge of measurement: T@y Chang Cutting / Prepsration Acid digestion by suitable acid dedended on different samole material (as b low table) Add appropiate amount of digestion reagenl Heat to appropriate temperature to odract 1) AlkaliFu6ion 2) HCI to dissolve Cool, filte. djgestate throughfilter Sample Material $eel, copper, aluminum, solder Glass Gold, platinum. p lladium, ceramic Silver Plastic Others Digestion Acid Aqua regia, HNq, HCl, HF, HrO, HNO3/HF Aqua regia HNO3 H,SO4, H'O', HNq, HCI Any acid to total digeslion measure the absorbance at 540 nm by uv-vls cmfry rrtrr f jr,r. _r litr, t.l#.._1.rrtd,r rt i. r,r.t i+rr,.4t.c rl.i i ii. ril :,t?!ll rb6docsd s *udbyfuc6mpa tur 6dd.bm51dnetu sla he rm'broi d 'ab' rv l Ei.lghtsadd 'ga0nsunebsenndbereprdudo:c4lifulwldl ':' n r fj!4rii il,&dtre

8 Test Report No. : CE/2011/10412A Oale : Page:6of9 ELSCHUKOM ELEKTROSCHUTZKONIPONENTENBAU GMBH tl]tl [][tlltt l GEWERBESTMSSE 87, D VEILSDORF, GERMANY Analytical flow chart of Soxhlet extraction (LC/MS) procedure 1) Name ofthe person who made measurcment: Lydia Fu 2) Name of the person in charge of measurement Shinjyh Ch6n r Test ltems: PFOS/PFOA. Benzotriazole Sample pretreatmenusepa tion Data nlh ladg@dd{onyblheghp]a1s]loddths eg@d Dde c6bry L i /il:.ir,! irl'..:r:l*i.i iilrlt.:r:d.l--1iif14.11\ rh6d@hde$6dbylhecohpanyab]dlohgsae cddi6bolss for sdo iimal dm6ds s6l ont and, rb n h. hb ot cr sd 5 i31 lmlrgh6afud Edonsune$.r.nndbel4ducd6:c pli'u

9 Test Report No. : CE/20'11/10412A Date : /11Page:7ofg ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU G[IBH GEWERBESTRASSE 87, D VEILSDORF, GERMANY t ti Itt]l Analytical flow chart of halogen content '1) Name of the p rson who made measurement: Rita Chen 2) Name of the person in charge of measurement: Troy Chang Sample pretroatmenl / Separation Weighting and putting sample in c ll Orygen Bornb Combustion / Absorption Dilution to fixed volume Analy6is wa6 perfomed by lc d31t bse ftsbi@d mdb rh3dum*'66oeby$6cdp* pois bl It n b rb crmr 'd 66 tun lm.'ghgrmoh garm3uid.r'bra rqiorvrenafda dkcompany A

10 Test Report No. : CE/201/10412A Dad:e 2011t01111Page:8ofg ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH GEWERBESTRASSE 87, D VEILSDORF. GERI,IIANY lmllllll rrrrl ] First testing process -----' 1) MrE of theperson who nede reasureb nl: RonEn Wong 2) MrE of theperson in charge of neasu nedt: Troy Chang Optional screen prccess.--- ConfifirEtion procecs -.> PBB/PBDE analytical FLOW CHART Screen analysis "' ""' " ' 't' "" ' """ Sarple extlactiorv Soxhlet nethod Concentrate/Dilute Extracted solution Filter Anatysis by GCi [rs.- ir '!iri'::ajirll ont and *rhn$ermrsorcr6ds isr lh.llghl.sftdobr'odonsunglh6u..'"'..,,i,. I,l' r-".." -i ry suqed e b c53cr cod r ons o' s 5uhd ro r ms ad csdi ms ro, els) r6d rhs 6n rcfn 6nd b rc L r- 1,iaq6

11 Test Report No. : CE/2011/'10412A Oale : Page:9of9 ELSCHUKOIU ELEKTROSCHUTZKOMPONENTENBAU GIVBH GEWERBESTRASSE 87, D VEILSDORF, GERMANY ll [ l ltttttll '. End of Report " mpeglredd rhs r i rcfn mnd b.,r i.r,::, r:i*r, i r,,li..;.i!,.lnrt" i:1...j lrlr ror e6ddn romsr dmeft 3uqed b refts ed Cmdi ob ro, Ee :, i ::1 rlissdtli

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20 TEST REPORT NUMBER : TWNC APPLICANT: LITTELFUSE, INC. DATE : JAN 19, E. NORTHWEST HWY DESPLAINES IL SAMPLE DESCRIPTION: ONE (1) GROUP OF SUBMITTED SAMPLES SAID TO BE : PART DESCRIPTION : COLORANT PINK PART NUMBER : FACILITY : DUNSEN DATE SAMPLE RECEIVED : JAN 14, 2009 DATE TEST STARTED : JAN 14, 2009 *************************************************************************** TEST COUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS PLEASE REFER TO ATTACHED PAGES. *************************************************************************** AUTHORIZED BY: ON BEHALF OF INTERTEK TESTING SERVICES TAIWAN LIMITED K. Y. LIANG DIRECTOR THIS REPORT SHALL NOT BE REPRODUCED EXCEPT IN FULL, WITHOUT THE WRITTEN APPROVAL OF THE LABORATORY. 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 1 OF 9

21 NUMBER : TWNC TEST COUCTED (Ⅰ) TEST RESULT SUMMARY : TESTING ITEM RESULT (ppm) PINK PLASTIC BEAN HEAVY METAL CADMIUM (Cd) CONTENT LEAD (Pb) CONTENT MERCURY (Hg) CONTENT CHROMIUM VI (Cr 6+ ) CONTENT POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MONOBB) DIBROMINATED BIPHENYLS (DIBB) TRIBROMINATED BIPHENYLS (TRIBB) TETRABROMINATED BIPHENYLS (TETRABB) PENTABROMINATED BIPHENYLS (PENTABB) HEXABROMINATED BIPHENYLS (HEXABB) HEPTABROMINATED BIPHENYLS (HEPTABB) OCTABROMINATED BIPHENYLS (OCTABB) NONABROMINATED BIPHENYLS (NONABB) DECABROMINATED BIPHENYL (DECABB) POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MONOBDE) DIBROMINATED DIPHENYL ETHERS (DIBDE) TRIBROMINATED DIPHENYL ETHERS (TRIBDE) TETRABROMINATED DIPHENYL ETHERS (TETRABDE) PENTABROMINATED DIPHENYL ETHERS (PENTABDE) HEXABROMINATED DIPHENYL ETHERS (HEXABDE) HEPTABROMINATED DIPHENYL ETHERS (HEPTABDE) OCTABROMINATED DIPHENYL ETHERS (OCTABDE) NONABROMINATED DIPHENYL ETHERS (NONABDE) DECABROMINATED DIPHENYL ETHER (DECABDE) HALOGEN CONTENT FLUORINE (F) CHLORINE (Cl) 2986 BROMINE (Br) IODINE (I) REMARKS : ppm = PARTS PER MILLION BASED ON WEIGHT OF TESTED SAMPLE = NOT DETECTED RESPONSIBILITY OF CHEMIST: IRENE CHIOU / KEVIN LIU / CATHY CHEN DATE SAMPLE RECEIVED : JAN 14, 2009 TESTING PERIOD : JAN 14, 2009 TO JAN 17, 2009 ****************************************************************************** 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 2 OF 9

22 NUMBER : TWNC TEST COUCTED (Ⅱ) ROHS REQUIREMENT : RESTRICTED SUSTANCES CADMIUM (Cd) LEAD (Pb) MERCURY (Hg) CHROMIUM (VI)(Cr 6+ ) POLYBROMINATED BIPHENYLS (PBBs) POLYBROMINATED DIPHENYL EHTERS (PBDEs) LIMITS 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) (Ⅲ) TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT WITH REFERENCE TO IEC /95/CDV IN CLAUES 8/9/10, BY CADMIUM (Cd) CONTENT MICROWAVE DIGESTION UNTIL THE TESTED 2 ppm SAMPLES ARE TOTALLY DISSOLVED A DETERMINED BY ICP-OES LEAD (Pb) CONTENT WITH REFERENCE TO IEC /95/CDV IN CLAUES 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED A DETERMINED BY ICP-OES 2 ppm WITH REFERENCE TO IEC /95/CDV IN CLAUES 7, BY MICROWAVE MERCURY (Hg) CONTENT DIGESTION UNTIL THE TESTED SAMPLES 2 ppm ARE TOTALLY DISSOLVED A DETERMINED BY ICP-OES WITH REFERENCE TO USEPA 3060A & CHROMIUM VI (Cr 6+ ) 7196A, BY ALKALINE DIGESTION A CONTENT DETERMINED BY UV-VIS 1 ppm SPECTROPHOTOMETER POLYBROMINATED BIPHENYLS (PBBs) WITH REFERENCE TO IEC /95/CDV IN ANNEX A, BY SOLVENT EXTRACTION A DETERMINED BY GC-MSD A FURTHER HPLC CONFIRMATION WHEN NECESSARY 5 ppm ****************************************************************************** 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 3 OF 9

23 NUMBER : TWNC TEST COUCTED (Ⅲ) TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT POLYBROMINATED DIPHENYL ETHERS WITH REFERENCE TO IEC /95/CDV IN ANNEX A, BY SOLVENT EXTRACTION A DETERMINED BY GC-MSD 5 ppm (PBDEs) A FURTHER HPLC CONFIRMATION WHEN NECESSARY HALOGEN CONTENT WITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN A DETERMINED BY ION CHROMATOGRAPHY 50 ppm REMARKS : REPORTING LIMIT = QUANTITATION LIMIT OF ANALYTE IN SAMPLE TESTS WERE COUCTED WITH REFERENCE TO 111/95/CDV VERSION WHICH IS STILL A DRAFT METHOD A SUBJECT TO FUTURE CHANGES PRIOR TO PUBLICATION. ****************************************************************************** 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 4 OF 9

24 NUMBER : TWNC TEST COUCTED (Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/Pb/Hg CONTENTS REFERENCE STAARD: IEC (111/95/CDV) SAMPLING/GRIING OR CUTTING FOR DIFFERENT MATERIAL, DIGEST THE SAMPLE WITH APPROPRIATE ACID *1 CONFIRM THE TESTED SAMPLES ARE TOTALLY DISSOLVED MAKE UP WITH DEIONIZED WATER ANALYZED BY ICP-OES REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 METALS HNO 3, HCl,HF ELECTRONICS HNO 3, HCl,H 2 O 2, HBF 4 ****************************************************************************** 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 5 OF 9

25 NUMBER : TWNC TEST COUCTED (Ⅳ) MEASUREMENT FLOWCHART: TEST FOR CHROMIUM (VI) CONTENT REFERENCE STAARD:USEPA 3060A/7196A SAMPLING/GRIING OR CUTTING WEIGH SAMPLE A ADD EXTRACTION REAGENT EXTRACT AT HOT PLATE BY APPROPRIATE TEMP. COOL A FILTER THE EXTRACT MAKE UP WITH DEIONIZED WATER A ADD DIPHENYL-CARBAZIDE SOLUTION ANALYZED BY UV-VIS ****************************************************************************** 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 6 OF 9

26 NUMBER : TWNC TEST COUCTED (Ⅳ) MEASUREMENT FLOWCHART: TEST FOR PBBS/PBDES CONTENTS REFERENCE STAARD: IEC (111/95/CDV) SAMPLING/GRIING OR CUTTING WEIGH SAMPLE A ADD ORGANIC SOLVENT SOXHLET EXTRACTION OR SOLVENT EXTRACTION CONCENTRATE THE EXTRACT A MAKE UP WITH ORGANIC SOLVENT ANALYZED BY GC-MSD ****************************************************************************** 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 7 OF 9

27 NUMBER : TWNC TEST COUCTED (Ⅳ) MEASUREMENT FLOWCHART: TEST FOR HALOGEN CONTENT REFERENCE STAARD:EN SAMPLING/GRIING OR CUTTING ADD ABSORBENT IN A COMBUSTION FLASK & PLACE WEIGHED SAMPLE IN EQUIPMENT FILL THE COMBUSTION FLASK WITH OXYGEN IGNITE THEN LEAVE THE FLASK AT ROOM TEMPERATURE TRANSFER THE ABSORBENT INTO A VOLUMETRIC FLASK MAKE UP WITH DEIONIZED WATER ANALYZED BY ION CHROMATOGRAPHY ****************************************************************************** E OF REPORT 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 8 OF 9

28 NUMBER : TWNC TEST COUCTED PHOTO 8/F., No. 423, Ruiguang Road, Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) PAGE 9 OF 9

29 Test Report Number : TWNC Applicant: Littelfuse, S.A. de C.V. Date : Aug 03, 2011 Blvd. Fausto Z. Martinez #1800 Col. Magisterio Seccion 38 C.P Piedra Negras, Coahuila, Mexico Sample Description: One (1) group of submitted samples said to be : Part Description : FKS SOCKET Part Number : Date Sample Received : Jul 29, 2011 Date Test Started : Aug 02, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 1 of 5

30 Number : TWNC Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) (1) (2) Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content (mg/kg with 50cm 2 ) Negative (< 0.02) Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected < = Less than mg/kg with 50cm 2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Tested Components (1) Coppery Metal Base Material (2) Silvery Plating Layer Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received : Jul 29, 2011 Test Period : Aug 02, 2011 To Aug 03, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 2 of 5

31 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested 2 ppm samples are totally dissolved and Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 0.02 mg/kg with 50cm 2 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 3 of 5

32 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC edition 1.0:2008 Sample preparation Number : TWNC Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water By boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Remarks: Analyzed by UV-VIS *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 4 of 5

33 Test Conducted Number : TWNC Photo 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 5 of 5

34 Test Report Number : TWNC Applicant: Littelfuse, S.A. de C.V. Date : Aug 03, 2011 Blvd. Fausto Z. Martinez #1800 Col. Magisterio Seccion 38 C.P Piedra Negras, Coahuila, Mexico Sample Description: One (1) group of submitted samples said to be : Part Description : FKS SOCKET Part Number : Date Sample Received : Jul 29, 2011 Date Test Started : Aug 02, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 1 of 5

35 Number : TWNC Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) (1) (2) Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content (mg/kg with 50cm 2 ) Negative (< 0.02) Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected < = Less than mg/kg with 50cm 2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Tested Components (1) Coppery Metal Base Material (2) Silvery Plating Layer Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received : Jul 29, 2011 Test Period : Aug 02, 2011 To Aug 03, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 2 of 5

36 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested 2 ppm samples are totally dissolved and Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 0.02 mg/kg with 50cm 2 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 3 of 5

37 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC edition 1.0:2008 Sample preparation Number : TWNC Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water By boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Remarks: Analyzed by UV-VIS *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 4 of 5

38 Test Conducted Number : TWNC Photo 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 5 of 5

39 Test Report Number : TWNC Applicant: Littelfuse, S.A. de C.V. Date : Aug 08, 2011 Blvd. Fausto Z. Martinez #1800 Col. Magisterio Seccion 38 C.P Piedra Negras, Coahuila, Mexico Sample Description: One (1) group of submitted samples said to be : Part Description : FKS COVER Part Number : Date Sample Received : Jul 29, 2011 Date Test Started : Aug 01, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 1 of 7

40 Number : TWNC Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Transparent Plastic Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) 126 Bromine (Br) Iodine (I) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Jul 29, 2011 Test Period : Aug 01, 2011 To Aug 08, F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 2 of 7

41 Number : TWNC Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 2 ppm 1 ppm 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 3 of 7

42 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MSD Biphenyls (PBBs) and further HPLC confirmation when 5 ppm necessary. Polybrominated Diphenyl Ethers (PBDEs) Halogen Content With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Remark: Reporting limit = Quantitation limit of analyte in sample 5 ppm 50 ppm 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 4 of 7

43 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 5 of 7

44 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard:EN Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 6 of 7

45 Number : TWNC Test Conducted Photo 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. Tel: (+886-2) Fax: (+886-2) Page 7 of 7