ICP Test Report Certification Packet

Transcription

1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Inrush Protector Product #: 399xxxxxxx Series Issue Date: Spetember 5, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the Inrush Protector RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: 1 Form Rev. A 2/21/06

2 Table 1: List of Raw Materials covered by this report Total Parts Raw Material Part Number Raw Material Description Page(s) 1 DRCU Melting Wire LOZZ194 (692213) Solder Wire (T6626) Plastic Cap (G3813) Socket with Pin GLZZxxx (6481xx) Yarn

3 Validit For Queali Please Co nown ith scs Test Report ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH GEWERBESTMSSE 87, D VEILSDORF, GERMANY No. : CE/20f f/10411a Dale :2011to1t1iPage:1of10 l:l [Ilat][ttltttl The following sample(s) waa/were submitted and identifi.d by/on bohalfofth. ctient as : Sample Description Style/llem No. Country of Origin Sample Receiving Date Tesling Period COPPER CLAD & COPPERALLOY WIRES PLEASE REFER TO PAGE 5 GERMANY 2011tO1tU 2011 t01 t t01 tll T 6t Result(s) Please refer to next page(s). irh 161cpddr r ronlylortusmp 13)rsred ih6redrcpdqndbc '!r; r.i'{il t:rir.t.r\ I u t., t.r:l!{. ny9&,3dbgg{3c codlonsds fff 6d,m'c romd dm6ft suq ont 'nd w th n h rmg d cred s 6' selrg&!d@ Edonsun6lh.ra :: rr.r i!.!,.+rir'i r *6101,e

4 Test Report No. : CE/2011/10411A Date : 2o11tl1t1i Page.2 d 1O ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GI, BH GEWEREESTRASSE 87, D VEILSDORF, GERMANY Test Resulgsl PART NAME No.1 IUIXEDALL COLOR METAL WIRE (NCLUDING THE PLATING LAYER) O1 KIS) T 6t ltem (s): R ult Unlt Method irol No.1 Cadmium (Cd) mg/kg With reference to IEC : 2008 and perfomed by ICP-AES. n.d. Lead (Pb) mg/kg With reference to IEC : 2008 and pertormed by ICP-AES. 2 n,d, Mercury (Hg) mg/kg With reference to IEC 62321: 2008 and pedormed by ICP.AES. 2 n.o, Hexavalent Chromium Cr(Vl) by With reference to IEC 62321: 0.02mg/kgNegative Spot test / boiling weter 2008 and perfomed by Spot test / with 50 cm" extlaction boiling water extraction Method. surfac (See Note 5) Perfl uorooctane sulfonates ms/ks With reference to US EPA 3540C: 10 n.d. (PFOS) 1996 method for PFOS Content. PFOS -Acid Analysis {ras pedormed by PFOS - Metal Salt LC/I\, S. PFOS -Amide PFOA (CAS No.: S7-1) mg/kg With reference to us EPA 3540C: 10 n.o method for PFOA Content. Analysi6 wa6 pedomed by LC/MS. Halog n Halogen-Fluorine (F)(CAS No.: \ 50 n.cl. HalogenChlorine (Cl)(CAS No.: 50 n.d ') With reference to BS EN msit<s 14582:2007. Analysis was Halog n-brcmine (Br)(CAS No.: pgrformed by lc. 50 n.d. 0 t ) Halogenlodine (l)(cas No.: 01i13624,L8) 50 n.o, 'nr[3t6r, Fddsontrorbsampr ltbdd Thsr.dr6poi mdberopducd x pr ntul comfiy,jr+r,rr-ia.i:;1.'r'1t11'!irriirlrrit r!.\.,r1'r:i:r,r).l\::fi:1,,'. 1r{r{ rhsd;mdts$uadbylhsconp3iylub]dbbgob.condibbols bafmi]taidoblgal63fdhim pm3b'lytlo6c]glandh3fu.lr:ri.r i!r ari rl reldzre rd I + s6lorrje tt w'rsfon

5 Test Report ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH GEWERBESTMSSE 87, D VEILSDORF, GERMANY No. r CE/2011/10411A Date 201.1t11h1Page:3of10 Test ltem (s): Unit M thod MDL Result No.l Sum of PBB3 n.o. Monobromobiphenyl 5 n.o, Dibrcmobiphenyl 5 n,d, Tribromobiphenyl 5 n.o. Tetrabromobiphenyl 5 n.d, Pentabromobiphenyl 5 n.d. Hexabromobiphenyl 5 n.d. Heptabromobiphenyl 5 n.o. Octabromobiphenyl n.d. Nonabromobiphenyl 5 n.o, Decabromobiphenyl With reference to IEC 62321: 5 n.d. mg/kg Sum of PBDEa 2008 and performed by GC/[,S. n.o. Monobromodiphenyl ether 5 n.o. Dibromodiphenyl ether n.d, Tribromodiphenyl ether n.o. Telrabromodiphenyl ether n.d. Pentabromodiphgnyl ether n.d. Hexabromodiphenyl ether 5 n.d. Heptabromodiphenyl ether n.d. Octebrornodiphenyl ether n.d. Nonabromodiphenyl elher 5 n.d. Decabrcmodiphenyl ether 5 n.d- cd tu1'r)j1,ll.rtii,:a!!!1j;:l.rrli:":llf ',.i!t!1ih1.1..ir;i;t!,r,1 :'jlliii. ny sub.d b ft G*.6rcood ' o^s or s tu suq o^t and *ihin rtu rimb or cr frt id nolbdl6pldudacepi'nlu]'6d

6 Test Report No. : CE/2011/10411A Dale 2111t01t1j page : 4 of 10 ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GIUBH GEWERBESTRASSE 87, D VEILSDORF, GERMANY rtl lfltlrfl ttt]t Note : 1 mgkg = ppm; 0.1M7o= 1000ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4."-"=NotRegulated 5. SpoFtest: Negative = Absence of Cr(Vt) coating / surface layer, Positive = Presence of Cr(Vl) co ting / sudace layer; (The tested sample should be further verified by boiling-wet r-extraction method if the spotest result cannot be confirmed.) Boaling-water3xtraclion : Negativ = Absence of Cr(Vt) coating / 6lrface layer. Positive = Presence of Cr(Vl) co ting / surface layer; the detecled concentration in boiling-\n ter- xtraclion 6olution is equal or greater than 0.02 mg/kg with 50 cm2 sample surface area. 6. '" = Quatitative anatysis (No Unit) 7. The sample(s) was/were analyzed on behalf of the applic nt as mixing 6ample in onetesting. The above result(s) \r/eslflere only given asthe infomality value. PFOS Reference lnfonnation : Di ctlve 2006/12ZEC (1) May not be placed on the ma*et or used as a subslance or constituent of preparations In a concentetion equalto or higherthan % by ma$s. (2) May not be placed on the ma*et in semi-finished products or articles, or parts thereof, if the concentration of PFOS is equal to or higher than 0. 1 % by mas calculated with reference to the mags of structuelly or micrd*ructurally distinct parts that contain PFOS or, for textiles or other coated materials, if the amount of PFOS is equal to or higher than 1pg/m2 of the coated material. cmfoy,r r r,iiii r' n rlrr'rllti,,.ir"i A i relrgnd ft srsd@d mdbeld l-nr i*:1l?-1:i u r r,l. r :.. 111t4 m3dmdgsldbybocdr &b] dbrsmg.^dcmd[@'ore ueron rh6tr nohr.id dbrhe{trs und lb rm fary ft6 c@p.iy s,o 6,.ep6B bi I srd 6 cr6r 'nd 6 3 d6 nis6orrrerd,lts6lorrrsrr pesr<n,

7 Test Report No. : CE ADane: Page : 5 of 10 ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH GEWERBESTMSSE 87, D VEILSDORF, GERMANY ITIIllllI[l l IIIl Style/ltem No. : (r) COPPER TIN ALLOY W RE CuSn6 (2) E\A/N 02,01.. COPPER CLAD WIRE. ELCON 30 (3) EWN COPPER CLAD STEELWIRE. ELCON F (4) EWN 02.01,. COPPER CLAD IRON.NICKEL.ALLOY WIRE - ELCON D (5) EWN SILVER COPPERALLOYWIRE -AgCu50 (6) EWN SILVER COPPERALLOYWIRE -Agougo (7) EWN 02.0'1. - COPPERWIRE - Cu99.g% (8) s.---- SILVER COPPER ALLOY WIRE -Ag72Cu28 (9) E!ryN COPPER - ZINC -ALLOYWIRE- Cu80 Zn20 00) SILVER COPPERALLOY WIRE -Ag45Cu45 (Agcuss) (11) COPPER PLATED, BRASS PLATED SPRING-STEEL WIRE - FST, Cu -% cm ry {+rjiii.r.,r ljfil' lr{ij]; ;llrl}:e* l.1l+lr41.r\ ;:1j'r. r Jr.']llir'r ny 34d ro a cdser.6dtr og d s tu odm.bmd dm6d sdt tu 'm,brs or ab' t dnt and w ih'n h rmis o, cr.d s Br lbr.ghbadd ddsunoso'e.dbe'gduddceplnfulwim

8 Test Report ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH GEWERBESTMSSE 87, D VEILSDORF. GERMANY No. : CE/2011/10411A Dar'.e :2o11t1it11 Page:6of10 ] ti tl][ttttt 1) Thqse samples were dissoked totally by pre-conditioning method according to below flow chart ( Cf' test method excluded ) 2) Name of the person who made measurement: Climbgreat yang 3) Name of the person in charge of measurement: Troy Chang Cutting / Prep ration Acid digestion by suitable acid depended on difierent sample matedal (a8 belo\,t, table) Add appropriate amount of digestion reagent Heat to appropriate t rnperature to xtract 1) AlkaliFusion 2) HCllodissotue Cool, filter digestate throughfilter Sample Material Sl el, copper, aluminum, solder Glaaa Gold, platinum, palladium, ce mic Silver Plastic Others Digqstion Acid Aqua regia, HNO3, HCl, HF, HrO, HNO/HF Aqua regia HNO3 H2SO+ HrOr, HNO3, HCI Any acid to total digestion measure the ab6orbance at 540 nm by W-VIS ComFnv.-rl:j.iii!.j :1 rll{rl: JlrrUirlt.,:.ihi':n1.1': Th3fumds636dbyih6cofip3nysuq6db6G*dcodIbisds id.bd@]c'o@dodn.ds'slbr irr;+' -J:r{jlir:.. rb.. qhb a^d ob dm3 uddar rh6 ra i9b'ly61o&c.d.dstsd@ndi '! rr : r;i ruir' irsld)r'?le

9 Test Report No. : CE/2011/ Dde 2011t11h1 page : 7 of.10 ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GI\4BH [t l ltt GEWERBESTMSSE 87, D VEILSDORF, GERMANY ltlt]l Analytical flow chart of Soxhlet extraction (LC/MS) procedure 1) Name of the person wfio made measurement: Lydia Fu 2) Name ofthe person in charge of measurement: Shinjyh Chen r Test ltems: PFOS/PFOA, Benzotriazote Sampl pretreatmenvseparation cm ry *irl jr1j:r,,i..1+$ :' ny36,sd oic53ts codtonsols suqsd b T ms ad cmdms ro, E mpolt r66d rhs I6d r@n ennd b mt atu wihin rb tmb or cbrt! B lbffoheaddigaronsunerhsta ::!, ir flr, lr,: it+sortae

10 Test Report ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GI/ BH GEWERBESTMSSE 87, D VEILSDORF, GERI'ANY No. : CE2011l10411A Date : 2011t01t11Page:8of10 tl lt][tltttii Analytical flow chart of halogen content 1) Name ofthe person who made measurement: Rita Chen 2) Name of the person in charge of measurcmentt Troy Chang S mple preteatnent / Separation Weighting and putting sampte in cell Oxygen Bomb Combustion / Ab6orption Dilution to fixed volume Analysis was performed by lc npsglcdd rhs6r@d6ndb!ir.;iltlir Er.,.iiihdar. :i+i r.1.!i.,!.1 r sd by be Comp' &b]adbt3m6andcmdi66fue sfbb' t s ro 6craradssem t:,i.r +!r lir..rin r s6 onre

11 Test Report No. : CE/2011/1M11A Dale :2011t01t11Page I of 10 ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GI\4BH GEWERBESTRASSE 87, D VEILSDORF. GERI\4ANY tr fi lt[tllttil First testing process -----> PBB/PBDE analyticat FLOW CH,ART 1) fbre of the person who fibde fi asurerpnt: RonEn Wong 2) llafie of the person in charge of reasurenent: Troy Chang Optional screen process.--- ConfinYEtion proce6s -.> Screen analysis """""1.."'... Sarple extractbn/ Soxhlet rnethod v ConcentratdDilute Extracisd solution Filtef Analysis by GC/MS.,r i.r' r!:i*r, irlli_,ri.r:frl'\,:t:l l,rirrir ny9!b]adlo8g6s condionso s ie aedidrc6md dmed suq o^t 5d w rhn rb imb d cr dt 'br.gh65dd'gd]oisund'1h.tr! isr

12 Test Report No. : CE/201/10411A D.iie -. 2o11toit11 Page : ELSCHUKOM ELEKTROSCHUTZKO[, PONENTENBAU GMBH GEWERBESTRASSE 87, D VEILSDORF, GERMANY 10 of 10 at] ttl lltat l " End ot Report " ip315lr6$d Th: 161'@d nrcr b.']irl!..!i!::.;:ijli'll- l'lri ].!].]' : ],.] 'x:'!: ny slbred ro 6 06ne6r cmdr 06 d s slqed b reh6 trd cmdro6,o. E vn ro rhe I'mraloi or 'ab tt

13 Test Report Number : TWNC Applicant: Littelfuse, Philippines Inc. Date : Nov 22, 2010 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Solder (metal) Part Number : Date Sample Received : Nov 17, 2010 Date Test Started : Nov 17, 2010 : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 5

14 Number : TWNC Testing Item Result (ppm) Silvery Metal Heavy Metal Cadmium (Cd) content Lead (Pb) content 322 Mercury (Hg) content Chromium VI (Cr 6+ ) content (mg/kg with 50cm 2 ) Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected < = Less than mg/kg with 50cm 2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of testing. Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Nov 17, 2010 Testing Period : Nov 17, 2010 To Nov 22, 2010 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 Of 5

15 Number : TWNC (Ⅲ) Test Method: Testing Item Testing Method Reporting Limit 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 0.02 mg/kg with 50cm 2 Page 3 Of 5

16 Number : TWNC (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / Electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Negative *2 Get 50cm 2 sample Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Analyzed by UV-VIS Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Page 4 Of 5

17 Number : TWNC Photo Page 5 Of 5

18 Test Report Number : TWNC Applicant: Littelfuse, Philippines Inc. Date : Nov 19, 2010 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : TE Caps Part Number : Date Sample Received : Nov 16, 2010 Date Test Started : Nov 17, 2010 : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 6

19 Number : TWNC (Ⅰ) Test Result Summary : Testing Item Result (ppm) Brown Plastic Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) 268 Bromine (Br) Iodine (I) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Nov 16, 2010 Testing Period : Nov 17, 2010 To Nov 19, 2010 Page 2 Of 6

20 Number : TWNC (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Testing Item Testing Method Reporting Limit Cadmium (Cd) 1.0:2008 in clause 8/9/10, by content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. 2 ppm Lead (Pb) content 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content determined by ICP-OES. 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Page 3 Of 6

21 Number : TWNC (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Remarks: Analyzed by UV-VIS *1: List Of Appropriate Acid: Material Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 4 Of 6

22 Number : TWNC (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard: EN Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill the combustion flask with oxygen Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 5 Of 6

23 Number : TWNC Photo Page 6 Of 6

24 Test Report Number : TWNC Applicant: Littelfuse, Philippines Inc. Date : May 25, 2011 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : TE Socket with pin Part Number : Date Sample Received : May 20, 2011 Date Test Started : May 21, 2011 : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 7

25 Number : TWNC (Ⅰ) Test Result Summary : Test Item Result (ppm) (1) (2) (3) Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Chromium VI (Cr 6+ ) content (mg/kg with 50cm 2 ) -- Negative (< 0.02) Negative (< 0.02) Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Page 2 Of 7

26 Number : TWNC (Ⅰ) Test Result Summary : Test Item Result (ppm) (1) (2) (3) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected < = Less than mg/kg with 50cm 2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Tested Components (1) Black Body Part (2) Silvery Plating On Metal Pin (3) Silvery Metal Substrate Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : May 20, 2011 Test Period : May 21, 2011 To May 24, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 3 Of 7

27 Number : TWNC (Ⅲ) Test Method: Test Item Test Method Reporting Limit 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content determined by ICP-OES. 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 1 ppm 0.02 mg/kg with 50cm 2 5 ppm 5 ppm 50 ppm Page 4 Of 7

28 Number : TWNC (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 Of 7

29 Number : TWNC (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard:EN Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 6 Of 7

30 Number : TWNC Photo Page 7 Of 7

31 Test Report Number : TWNC Applicant: Littelfuse, Philippines Inc. Date : Nov 22, 2010 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : TRTE Yarn Part Number : Date Sample Received : Nov 16, 2010 Date Test Started : Nov 17, 2010 : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 6

32 Number : TWNC (Ⅰ) Test Result Summary : Testing Item Result (ppm) White Yarn Heavy Metal Cadmium (Cd) content Lead (Pb) content 18 Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) 214 Bromine (Br) Iodine (I) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Nov 16, 2010 Testing Period : Nov 17, 2010 To Nov 22, 2010 Page 2 Of 6

33 Number : TWNC (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Testing Item Testing Method Reporting Limit Cadmium (Cd) 1.0:2008 in clause 8/9/10, by content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. 2 ppm Lead (Pb) content 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content determined by ICP-OES. 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Page 3 Of 6

34 Number : TWNC (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Remarks: Analyzed by UV-VIS *1: List Of Appropriate Acid: Material Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 4 Of 6

35 Number : TWNC (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard: EN Sampling/grinding or cutting Add absorbent in a calorimetric bomb & place weighed sample in equipment Fill the calorimetric bomb with oxygen Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 5 Of 6

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