ICP Test Report Certification Packet

Transcription

1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: TR5 Product #: 373xxxxxxx Issue Date: February 8, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2011/65/EU, recasting 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the TR5 RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Remarks:. Please see appropriate pages as identifed in Table 1 1 Form Rev. A 2/21/06

2 Table 1: List of Raw Materials covered by this report Total Parts Raw Material Part Number Raw Material Description Page(s) 1 497xxxx Element 99% Ni DRKOXXX Element Nickel Plated Wires DRCUXXX Element Tinned Copper & Copper Cladded wires DRAGXXX Element Silver Plated wires LOZZ194 (692213) Solder Plastic Cap Socket Ceramic Paper

3 Intertek Consumer Goods GmbH Würzburger Straße Fürth Polyfil AG Gina Gregorio Oberallmendstrasse 20A 6300 Zug / Switzerland Fürth, Test report No. FUHL Testing of a material sample according to the RoHS directive 2011/65/EC Sample description: Ni99.9MAg wire Arrival in lab: ; Period of XRF analysis incl. sample preparation and photo documentation: Head of Inorganic Lab: Claudia List Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item. This report consists of 6 page(s). The test methods signed with * are not listed in the attachment of the accreditation certificate. Conclusion based on tested item Test order Status testing according to the RoHS directive 2011/65/EC conform Please see overview of test results - Test results see next pages - Intertek Consumer Goods GmbH Tel.: Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: Amtsgericht Fürth, HRB 5756 Kay Grönhardt Fürth, Germany cg.germany@intertek.com USt-IdNr. DE Rainer Mast Durch die DAkkS nach DIN EN ISO/IEC akkreditiertes Prüflaboratorium Die Akkreditierung gilt für die in der Urkunde aufgeführten Prüfverfahren.

4 Page 2 of 6 page(s) of our test report No. FUHL dated Sample description: Ni99.9MAg wire nm = non Metal M = Metal cm = composite Material List of component parts: Sample No. Part No. Material Description M Ni99.9MAg wire Intertek Consumer Goods GmbH Tel.: Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: Amtsgericht Fürth, HRB 5756 Kay Grönhardt Fürth, Germany cg.germany@intertek.com Ust-IdNr. DE Rainer Mast

5 Page 3 of 6 page(s) of our test report No. FUHL dated Sample description: Ni99.9MAg wire Comment LOD = Limit of Detection BL = Below Limit OL = Over Limit X = Inconclusive, further test necessary σ = Standard deviation CS = Composite sample Remark: Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb), AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration exceeds the below warning value according to IEC Element Unit non - metal metal Cd mg / kg BL (70-3σ) < X < (130+3σ) OL BL (70-3σ) < X < (130+3σ) OL Pb mg / kg BL (700-3σ) < X < (1300+3σ) OL BL (700-3σ) < X < (1300+3σ) OL Hg mg / kg BL (700-3σ) < X < (1300+3σ) OL BL (700-3σ) < X < (1300+3σ) OL Br mg / kg BL (300-3σ) < X -- Cr mg / kg BL (700-3σ) < X BL (700-3σ) < X Element Unit composite material Cd mg / kg LOD < X < (150+3σ) OL Pb mg / kg BL (500-3σ) < X < (1500+3σ) OL Hg mg / kg BL (500-3σ) < X < (1500+3σ) OL Br mg / kg BL (250-3σ) < X Cr mg / kg BL (500-3σ) < X Intertek Consumer Goods GmbH Tel.: Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: Amtsgericht Fürth, HRB 5756 Kay Grönhardt Fürth, Germany cg.germany@intertek.com Ust-IdNr. DE Rainer Mast

6 Page 4 of 6 page(s) of our test report No. FUHL dated Sample description: Ni99.9MAg wire 1. XRF screening Method: XRF according to IEC 62321:2008* Sample No. Part No. Pb Hg Cd Cr total Br Status BL BL BL BL -- conform Comment: Elements Lead (Pb) Mercury (Hg) Cadmium (Cd) Chromium VI (Cr VI) Polybrominated Biphenyle (PBBs) Polybrominated Diphenyl ether (PBDEs) RoHS-limit value 1000 mg/kg 1000 mg/kg 100 mg/kg 1000 mg/kg 1000 mg/kg 1000 mg/kg - Flow charts see next page(s) - Intertek Consumer Goods GmbH Tel.: Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: Amtsgericht Fürth, HRB 5756 Kay Grönhardt Fürth, Germany cg.germany@intertek.com Ust-IdNr. DE Rainer Mast

7 Page 5 of 6 page(s) Test procedure samples metallic materials, YES screening by XRF? NO sample uniform? YES NO non-destructive sample preparation mechanical sample preparation YES screening procedure by XRF NO meets limits? further testing? YES NO pass entity based conforming sample fail entity based non conforming sample polymer materials, electronics (PCB / component) mechanical sample preparation chemical test procedure (verification) various methods (please see verification test procedure below) YES pass entity based conforming sample meets limits? fail NO entity based non conforming sample Intertek Consumer Goods GmbH Tel.: Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: Amtsgericht Fürth, HRB 5756 Kay Grönhardt Fürth, Germany cg.germany@intertek.com Ust-IdNr. DE Rainer Mast

8 Page 6 of 6 page(s) Verification test procedure Sample Preparation Sample Measurement Acid digestion with microwave / hotplate Pb/Cd/Hg PBBs/PBDEs Cr 6+ Sample solvent extraction Non-metallic material Metallic material Solution Filtration Residue Total digestion ICP-OES/AAS DATA Concentration/ Dilution of extraction solution Filtration GC/MS DATA Alkaline extraction Adding extraction solution Alkaline extraction Heating to 90~95 C for extraction Filtration and ph adjustment Adding 1,5- diphenylcarbazide for color development Positive Spot test Boiling water extraction Negative Adding 1,5- diphenylcarbazide for color development A red color indicates the presence of Cr 6+ If necessary, confirm with UV-VIS or IC-UV/VIS UV-VIS or IC-UV/VIS DATA DATA Intertek Consumer Goods GmbH Tel.: Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: Amtsgericht Fürth, HRB 5756 Kay Grönhardt Fürth, Germany cg.germany@intertek.com Ust-IdNr. DE Rainer Mast

9 Test Report Number : TWNC Applicant: Littelfuse Philippines Inc. Date : Jan 17, 2013 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Copper Nickel Alloy wires Part Number : DRKO Date Sample Received : Jan 11, 2013 Date Test Started : Jan 11, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 1 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

10 Number : TWNC Test Conducted (Ⅰ) Test Result Summary: Result Test Item Unit Test Method Submitted RL samples Heavy Metal Cadmium (Cd) content ppm With reference to IEC 62321: 2008, by microwave digestion and 2 determined by ICP-OES. Lead (Pb) content ppm With reference to IEC 62321: 2008, by microwave digestion and 2 determined by ICP-OES. Mercury (Hg) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. 2 With reference to IEC mg/kg 62321: 2008, by boiling Chromium VI (Cr 6+ ) content with water extraction and Negative cm 2 determined by UV-Vis Spectrophotometer. Remarks: ppm = parts per million based on weight of tested sample = mg/kg = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm 2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result. Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 11, 2013 Test Period : Jan 11, 2013 To Jan 15, 2013 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ * Page 2 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

11 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / Electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Negative *2 Get 50cm 2 sample Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ * Page 3 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

12 Number : TWNC Test Conducted Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ * Page 4 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

13 Number : TWNC Test Conducted Photo *THJ * Page 5 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

14 Test Report Number : TWNC Applicant: Elschukom Elektroschutzkomponentenbau Date : Jan 30, 2013 GmbH Gewerbestrasse 87, D Veilsdorf, Germany Sample Description: One (1) group of submitted samples said to be : Sample Description :Tin plated Wires Style / Item No. :Please see page two to three. Country of Origin :Germany Date Sample Received :Jan 23, 2013 Date Test Started :Jan 23, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 1 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

15 Test Report Number : TWNC Sample Description: Style / Item No. : (A-1) tin plated copper wire Cu, Sn--% (A-2) tin plated, copper plated copper nickel alloy wire Elcon30, Sn--% (A-3) tin plated, copper plated steel wire ElconF, Sn--% (A-4) tin plated, copper plated iron nickel alloy wire ElconD, Sn--% (A-5) tin plated copper nickel alloy wire - CuNi44, Sn--% (A-6) tin plated, silver plated copper wire Cu, Ag--%, Sn--% (A-7) tin plated brass wire Cu80Zn20, Sn--% Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 2 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

16 Test Report Number : TWNC Sample Description: Style / Item No. : (A-9) tin plated silver copper alloy wire AgCu90, Sn--% (ElCu90, Sn--%) (A-10) tin plated copper zinc alloy wire Cu70Zn30, Sn--% (A-11) tin plated copper nickel alloy wire CuNi12, Sn--% (A-12) tin plated silver copper alloy wire Ag72Cu28, Sn--% (A-13) tin plated silver wire Ag1000, Sn--% (A-14) tin plated silver copper alloy wire Ag45Cu55, Sn--%(AgCu55, Sn) (A-15) tin plated silver copper alloy wire AgCu70, Sn--%(ElCu70, Sn) (A-16) tin plated silver copper alloy wire AgCu80, Sn--%(Elcu80, Sn) (A-17) tin plated tungsten wire W, Sn Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 3 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

17 Number : TWNC Test Conducted (Ⅰ) Test Result Summary: Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Test Item Unit Test Method Chromium VI (Cr 6+ ) content ppm ppm ppm mg/kg with 50 cm 2 With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer. Result Mixed all kinds of metal wire RL Negative (#) 0.02 Remarks: ppm = parts per million based on weight of tested sample = mg/kg = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm 2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result. # = Due to the insufficient sample area, reduced total sample surface of 10 cm 2 was used and the dilution factor was adjusted accordingly. Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 23, 2013 Test Period : Jan 23, 2013 To Jan 29, 2013 *THJ * Page 4 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

18 Number : TWNC Test Conducted (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ * Page 5 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

19 Number : TWNC Test Conducted (Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / Electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Negative *2 Get 50cm 2 sample Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ * Page 6 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

20 Number : TWNC Test Conducted Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3,HCl,HF,H 2 O 2,H 3 BO 3 Metals HNO 3,HCl,HF Electronics HNO 3,HCl,H 2 O 2,HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ * Page 7 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

21 Number : TWNC Test Conducted Photo *THJ * Page 8 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C 台北市內湖區瑞光路 423 號 8 樓

22 Test Report Number: SHAH Applicant: ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU Date: JAN 18, 2013 GMBH GEWERBESTRASSE 87,D VEILSDORF, GERMANY Sample Description: Two(2) pieces of submitted samples said to be : (1) Mixed all kinds of metal substrates. (2) Mixed all kinds of plating layers. Item Name : Silver Plated & Pure Silver Wires. Item No. : (B-1) silver plated copper wire Cu, Ag--% (B-2) pure silver wire Ag 1000 (B-3) silver plated purest nickel wire Ni99.98%, Ag1% (B-4) silver-copper alloy plated copper plated iron nickel alloy wire ElconD, AgCu5% (B-5) silver plated constantan wire CuNi44, Ag5% (B-6) silver plated copper - nickel 44 alloy wire CuNi44, Ag10% (B-7) pure silver strips Ag 1000 pure Country Of Origin : Germany. ************************************************************************************************************************************************************ Tests Conducted: As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************ To Be Continued Authorized by: For intertek testing services Ltd., Shanghai Jacob Lin General Manager Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China 上海天祥質量技術服務有限公司上海市宜山路 801 號金陵商務廣場 B 座 Telephone: Facsimile: Page 1 Of 5

23 Tests Conducted Test Report Number: SHAH (A) Test result of RoHS Directive: Testing item Cadmium (Cd) content (mg/kg) Lead (Pb) content (mg/kg) Mercury (Hg) content (mg/kg) Chromium (VI)(Cr 6+ ) result (by boiling water extraction on metal) (mg/kg with 50cm 2 ) Testing item Cadmium (Cd) content (mg/kg) /Plating Lead (Pb) content (mg/kg) /Plating Mercury (Hg) content (mg/kg) /Plating Chromium (VI)(Cr 6+ ) result (by boiling water extraction on metal) (mg/kg with 50cm 2 ) /Plating Result (1) Result (2) Remark:mg/kg with 50cm 2 = milligram per kilogram with 50 square centimeter = not detected (B) RoHS Requirement: Restricted substances Cadmium (Cd) Lead (Pb) Mercury (Hg) Chromium (VI) (Cr 6+ ) Limits 0.01% (100 mg/kg) 0.1% (1000 mg/kg) 0.1% (1000 mg/kg) 0.1% (1000 mg/kg) The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material. (C) Test method: Testing item Testing method Reporting limit Cadmium (Cd) content With reference to IEC Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and 2 mg/kg determined by ICP-OES. Lead (Pb) content With reference to IEC Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and 2 mg/kg determined by ICP-OES. Mercury (Hg) content With reference to IEC Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES. 2 mg/kg Chromium (VI) (Cr 6+ ) content (for With reference to IEC Edition 1.0: 2008, by boiling 0.02mg/kg with 50cm 2 metal) water extraction and determined by UV-VIS (in testing solution) Spectrophotometer. Date sample received: Jan.14, 2013 Testing period: Jan.14, 2013 To Jan.17, 2013 ************************************************************************************************************************************************************ To Be Continued Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China 上海天祥質量技術服務有限公司上海市宜山路 801 號金陵商務廣場 B 座 Telephone: Facsimile: Page 2 Of 5

24 Test Report Number: SHAH Tests Conducted (D) Measurement flowchart: Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC Edition 1.0: 2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs Weigh sample and for different material, digest the sample with appropriate acid *1 Spot test Weigh sample and add alkaline solution Weigh sample and add organic solvent Positive *2 Confirm the tested samples are totally dissolved Yes Make up with deionized water No Get 50cm 2 samples Boiling water extraction Definite temp. Extraction Cool and filter the extract Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by GC-MSD Analyzed by UV-VIS Remarks: *1: list of appropriate acid: Material Acid added for digestion Polymers HNO 3,HCL,HF,H 2O 2,H 3BO 3 Metals HNO 3,HCL,HF Electronics HNO 3,HCL,H 2O 2,HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. ************************************************************************************************************************************************************ To Be Continued Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China 上海天祥質量技術服務有限公司上海市宜山路 801 號金陵商務廣場 B 座 Telephone: Facsimile: Page 3 Of 5

25 Tests Conducted Test Report Number: SHAH ************************************************************************************************************************************************************ To Be Continued Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China 上海天祥質量技術服務有限公司上海市宜山路 801 號金陵商務廣場 B 座 Telephone: Facsimile: Page 4 Of 5

26 Tests Conducted Test Report Number: SHAH ************************************************************************************************************************************************************ End Of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China 上海天祥質量技術服務有限公司上海市宜山路 801 號金陵商務廣場 B 座 Telephone: Facsimile: Page 5 Of 5

27 Test Report Number : TWNC Applicant: Littelfuse Philippines Inc. Date : Nov 01, 2012 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Solder wire Part Number : Date Sample Received : Oct 24, 2012 Date Test Started : Oct 25, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 1 of 6

28 Number : TWNC Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Silvery Metal Wire Heavy Metal Cadmium (Cd) content Lead (Pb) content 84 Mercury (Hg) content Chromium VI (Cr 6+ ) content (mg/kg with 50cm 2 ) Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected < = Less than mg/kg with 50cm 2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received : Oct 24, 2012 Test Period : Oct 25, 2012 To Nov 01, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ * Page 2 of 6

29 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 0.02 mg/kg with 50cm 2 *THJ * Page 3 of 6

30 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water By boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ * Page 4 of 6

31 Number : TWNC Test Conducted Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ * Page 5 of 6

32 Number : TWNC Test Conducted Photo *THJ * Page 6 of 6

33 Test Report Number : TWNC Applicant: Littelfuse Philippines Inc. Date : Oct 31, 2012 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : TRTE cap Part Number : Date Sample Received : Oct 24, 2012 Date Test Started : Oct 25, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 1 of 9

34 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Number : TWNC Result (ppm) Brown Plastic *THJ * Page 2 of 9

35 Test Conducted (Ⅰ) Test Result Summary : Test Item Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) Number : TWNC Result (ppm) Brown Plastic Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Oct 24, 2012 Test Period : Oct 25, 2012 To Oct 30, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ * Page 3 of 9

36 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested 2 ppm samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested 2 ppm samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples 2 ppm are totally dissolved and determined by ICP-OES. With reference to IEC edition Chromium VI (Cr 6+ ) 1.0:2008 in annex C, by alkaline content digestion and determined by UV-Vis 1 ppm spectrophotometer. Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Phthalates Hexabromocyclododecane (HBCDD) With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD. Remark: Reporting limit = Quantitation limit of analyte in sample 5 ppm 5 ppm 50 ppm 50 ppm 10 ppm *THJ * Page 4 of 9

37 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ * Page 5 of 9

38 Test Conducted (Ⅳ) Measurement Flowchart: Number : TWNC Test for Halogen Content Reference Standard:EN Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ * Page 6 of 9

39 Test Conducted (Ⅳ) Measurement Flowchart: Number : TWNC Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ * Page 7 of 9

40 Test Conducted (Ⅳ) Measurement Flowchart: Number : TWNC Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ * Page 8 of 9

41 Test Conducted Number : TWNC Photo *THJ * Page 9 of 9

42 Test Report Number : TWNC Applicant: Littelfuse Philippines Inc. Date : May 15, 2012 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Socket with Pin Part Number : Date Sample Received : May 10, 2012 Date Test Started : May 10, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 10 Tel: (+886-2) Fax: (+886-2)

43 Number: TWNC Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) (1) (2) (3) Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content (For Non-Metal Material) Chromium VI (Cr 6+ ) content (By Boiling Water Negative Extraction On Metal) (mg/kg with 50cm 2 ) (< 0.02)(#) Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Negative (< 0.02)(#) Tel: (+886-2) Fax: (+886-2) Page 2 of 10

44 Number: TWNC Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) (1) (2) (3) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected < = Less than mg/kg with 50cm 2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample surface of 25 cm 2 was used and the dilution factor was adjusted accordingly. Tested Components: (1) Black Body Part (2) Coppery Metal Substrate (3) Silvery Plating On Metal Pin Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : May 10, 2012 Test Period : May 10, 2012 To May 14, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Tel: (+886-2) Fax: (+886-2) Page 3 of 10

45 Number: TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content (For Non- Metal Extraction On Metal) Chromium VI (Cr 6+ ) content (By Boiling Water Extraction On Metal) Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Phthalates Hexabromocyclodode cane (HBCDD) With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD. Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 2 ppm 2 ppm 1 ppm 0.02 mg/kg with 50cm 2 5 ppm 5 ppm 50 ppm 50 ppm 10 ppm Tel: (+886-2) Fax: (+886-2) Page 4 of 10

46 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC edition 1.0:2008 Sample preparation Number: TWNC Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water By boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Tel: (+886-2) Fax: (+886-2) Page 5 of 10

47 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation Number: TWNC For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Tel: (+886-2) Fax: (+886-2) Page 6 of 10

48 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN Number: TWNC Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 7 of 10 Tel: (+886-2) Fax: (+886-2)

49 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Number: TWNC Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 8 of 10 Tel: (+886-2) Fax: (+886-2)

50 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Number: TWNC Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report Page 9 of 10 Tel: (+886-2) Fax: (+886-2)

51 Test Conducted Number: TWNC Photo Page 10 of Tel: (+886-2) Fax: (+886-2)

52 Test Report Number : TWNC Applicant: Littelfuse Philippines Inc. Date : Oct 31, 2012 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Ceramic paper Part Number : Date Sample Received : Oct 24, 2012 Date Test Started : Oct 25, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 1 of 7

53 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Number : TWNC Result (ppm) White Ceramic Paper Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Oct 24, 2012 Test Period : Oct 25, 2012 To Oct 30, 2012 *THJ * Page 2 of 7

54 Test Conducted (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Number : TWNC Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 2 ppm 1 ppm *THJ * Page 3 of 7

55 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS Biphenyls (PBBs) and further HPLC-DAD confirmation 5 ppm when necessary. Polybrominated Diphenyl Ethers (PBDEs) Halogen Content With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Remark: Reporting limit = Quantitation limit of analyte in sample 5 ppm 50 ppm *THJ * Page 4 of 7

56 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ * Page 5 of 7

57 Test Conducted (Ⅳ) Measurement Flowchart: Number : TWNC Test for Halogen Content Reference Standard:EN Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ * Page 6 of 7

58 Test Conducted Number : TWNC Photo *THJ * Page 7 of 7