TEST REPORT NUMBER: SHAH TESTS CONDUCTED. (A) TEST RESULT SUMMARY FOR RoHS DIRECTIVE:

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Bernice Patrick
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2 TESTS COUCTED (A) TEST RESULT SUMMARY FOR RoHS DIRECTIVE: TESTING ITEM RESULT (ppm) (1) CADMIUM (Cd) CONTENT (ppm) (<2) LEAD (Pb) CONTENT (ppm) 5030 MERCURY (Hg) CONTENT (ppm) (<2) CHROMIUM VI (Cr 6+ ) CONTENT (ppm)(for NON- (<1) METAL) POLYBROMINATED BIPHENYLS (PBBs) MONOBROMOBIPHENYL (MonoBB) (ppm) DIBROMOBIPHENYL (DiBB) (ppm) TRIBROMOBIPHENYL (TriBB) (ppm) TETRABROMOBIPHENYL (TetraBB) (ppm) PENTABROMOBIPHENYL (PentaBB) (ppm) HEXABROMOBIPHENYL (HexaBB) (ppm) HEPTABROMOBIPHENYL (HeptaBB) (ppm) OCTABROMOBIPHENYL (OctaBB) (ppm) NONABROMOBIPHENYL (NonaBB) (ppm) DECABROMOBIPHENYL (DecaBB) (ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMODIPHENYL ETHER (MonoBDE) (ppm) DIBROMODIPHENYL ETHER (DiBDE) (ppm) TRIBROMODIPHENYL ETHER (TriBDE) (ppm) TETRABROMODIPHENYL ETHER (TetraBDE) (ppm) PENTABROMODIPHENYL ETHER (PentaBDE) (ppm) HEXABROMODIPHENYL ETHER (HexaBDE) (ppm) HEPTABROMODIPHENYL ETHER (HeptaBDE) (ppm) OCTABROMODIPHENYL ETHER (OctaBDE) (ppm) NONABROMODIPHENYL ETHER (NonaBDE) (ppm) DECABROMODIPHENYL ETHER (DecaBDE) (ppm) PAGE 2 OF 8

3 TESTS COUCTED TESTING ITEM RESULT (ppm) (2) CADMIUM (Cd) CONTENT (ppm) (<2) LEAD (Pb) CONTENT (ppm) (<2) MERCURY (Hg) CONTENT (ppm) (<2) CHROMIUM (VI)(Cr 6+ ) RESULT (FOR METAL) N TESTING ITEM RESULT (ppm) (3) LEAD (Pb) CONTENT (ppm) (<2) REMARKS: ppm = PARTS PER MILLION = mg/kg < = LESS THAN = NOT DETECTED N = NEGATIVE THE SUBMITTED SAMPLE (1) WAS NOT HOMOGENEOUS MATERIAL A SAMPLING RAOMLY. NOTE :DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMEMENT 2005/717/EC. (B) RoHS REQUIREMENT RESTRICTED SUBSTANCES CADMIUM (Cd) LEAD (Pb) MERCURY (Hg) CHROMIUM (VI) (Cr 6+ ) POLYBROMINATED BIPHENYLS (PBBs) POLYBROMINATED DIPHENYL EHTERS (PBDEs) LIMITS 0.01% (100 ppm) THE ABOVE LIMITS WERE QUOTED FROM 2002/95/EC A AMEMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL. PAGE 3 OF 8

4 TESTS COUCTED (C) TEST METHOD : TESTING ITEM TESTING METHOD REPORTING LIMIT CADMIUM (Cd) CONTENT LEAD (Pb) CONTENT MERCURY (Hg) CONTENT CHROMIUM (VI) (Cr 6+ ) CONTENT (FOR NON-METAL) CHROMIUM (VI) (Cr 6+ ) CONTENT (FOR METAL) POLYBROMINATED BIPHENYLS (PBBs)& POLYBROMINATED DIPHENYL ETHERS (PBDEs) 111/95/CDV, BY ACID DIGESTION A DETERMINED BY ICP-OES 111/95/CDV, BY ACID DIGESTION A DETERMINED BY ICP - OES 111/95/CDV, BY ACID DIGESTION A DETERMINED BY ICP - OES 111/95/CDV, BY ALKALINE DIGESTION A DETERMINED BY UV-VIS SPECTROPHOTOMETER 111/95/CDV, BY BOILING WATER EXTRACTION A DETERMINED BY UV- VIS SPECTROPHOTOMETER 111/95/CDV, BY SOLVENT EXTRACTION A DETERMINED BY GC/MS/HPLC 2 ppm 2 ppm 2 ppm 1 ppm 0.02mg/kg with 50cm 2 (IN TESTING SOLUTION) 5 ppm NOTE: TESTS WERE COUCTED WITH REFERENCE TO 111/95/CDV VERSION WHICH IS STILL A DRAFT METHOD A SUBJECT TO FUTURE CHANGES PRIOR TO PUBLICATION. REPORTING LIMIT=QUANTIZATION LIMIT OF ANALYZE IN SAMPLE DATE SAMPLE RECEIVED : APR.28, 2008 TESTING PERIOD : APR.28, 2008 TO APR.29, 2008 PAGE 4 OF 8

5 TESTS COUCTED MEASUREMENT FLOWCHART(IEC 62321) 1. TEST FOR Cd/Pb/Hg CONTENTS Weigh sample and place in a microwave digestion vessel Add digestion reagent Digest samples in microwave digestion oven Analyze by ICP-OES Make up with deionized water Transfer the digestive solution into a volumetric flask 2. TEST FOR Cd/Pb CONTENTS Weigh sample and place in a conical flask Add digestion reagent Digest samples on hot plate Analyze by ICP-OES Make up with deionized water Transfer the digestive solution into a volumetric flask PAGE 5 OF 8

6 TESTS COUCTED 3. TEST FOR CHROMIUM (VI) CONTENT Weigh sample in an Erlenmeyer flask Add digestion solution and heating at hot plate Adjust the ph of the solution to 7.5±0.5 and transfer the solution to a volumetric flask Adjust the ph of the solution to 2.0±0.5 and make up with deionized water Add diphenylcarbazide solution Make up with deionized water Analyze the mixture by using UV-Vis spectrophotometer with wavelength set at 540 nm PAGE 6 OF 8

7 TESTS COUCTED 4. TEST FOR CHROMIUM (VI) CONTENT (BOILING WATER EXTRACTION ON METAL) Prepare the test solution and a sample with about 50cm 2 surface area Heat 50mL of DI water in a beaker to boiling and totally immerse the sample inside the beaker. Leach for 10 minutes while the water continues to boil Add the test solution to beaker, a red color indicates the presence of Cr(VI) If absorbance value greater than standard solution, the sample is considered to have a hexavalent chromium coating. If not, the test result is negative If the color developed is difficult to judge, could use UV-Vis spectrophotometer with wavelength set at 540 nm to confirm the result 5. TEST FOR PBBs/PBDEs CONTENTS Weigh sample and place in a thimble Extracted by Soxhlet extraction with organic solvent Concentrate the extract Analyze by GC-MSD /HPLC Make up with organic solvent Transfer the extract into a volumetric flask PAGE 7 OF 8

8 TESTS COUCTED E OF REPORT PAGE 8 OF 8

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