ICP Test Report Certification Packet

Transcription

1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: 327 series (Micro2 Fuses) Product #: 327 series (Micro2 Fuses) Issue Date: December 8, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the 327 series RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Remarks: Please see appropriate pages as identifed in Table 1 1 Decemeber 01, 2005 Littelfuse, Inc. Page 1

2 Table 1: List of Raw Materials covered by this report Total Parts Raw Material Part Number Raw Material Description Page(s) Zinc Strip Blue Colorant Hot Stamp Foil Body - Compound Tan Colorant Brown Colorant Red Colorant Yellow Colorant Green Colorant Body - Technyl

3

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28 Report No.: MX Date: RESULTS REPORT INTERTEK TESTING SERVICES DE MEXICO SA DE CV LABORATORIO CD. DE MEXICO DELIVER TO: Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila ATTENTION: Ing. María Valdez It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

29 Report No.: MX Date: TEST REPORT APPLICANT Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila Ing. María Valdez SAMPLE DESCRIPTION One (1) group of submitted samples said to be : Sample Description Series 287,999 Item No. 3) N/P Colorant Tan Country of Origin NP Buyer's Name NP Supplier's Name NP Date sample received Testing period to ******************************************************************************************** TEST COUCTED As requested by the applicant, for details please refer to attached pages. ******************************************************************************************** CONCLUSION Sample Number Testing item Conclusion Failed component Failed result Pass 3 N/P Colorant Tan See Result summary ******************************************************************************************** TEST COUCTED It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

30 Samples: Report No.: MX Date: ) N/P Colorant Tan TEST RESULT SUMMARY FOR RoHS DIRECTIVE : TESTING ITEM Ω RESULT (ppm) Cadmium (Cd) content 0,01% (100 ppm) Lead (Pb) content 0,1% (1000 ppm) Mercury (Hg) content 0,1% (1000 ppm) Chromium (VI) (Cr 6+ ) 0,1% (1000 ppm) POLYBROMINATED BIPHENYLS (PBBs) Total 0,1% (1000 ppm) Monobromobiphenyl (MonoBB) --- Dibromobiphenyl (DiBB) --- Tribromobiphenyl (TriBB) --- Tetrabromobiphenyl (TetraBB) --- Pentabromobiphenyl (PentaBB) --- Hexabromobiphenyl (HexaBB) --- Heptabromobiphenyl (HeptaBB) --- Octabromobiphenyl (OctaBB) --- Nonabromobiphenyl (NonaBB) --- Decabromobiphenyl (DecaBB) --- POLYBROMINATED DIPHENYL ETHERS (PBDEs) Total 0,1% (1000 ppm) Monobromodiphenyl (MonoBDE) --- Dibromodiphenyl (DiBDE) --- Tribromodiphenyl (TriBDE) --- Tetrabromodiphenyl (TetraBDE) --- Pentabromodiphenyl (PentaBDE) --- Hexabromodiphenyl (HexaBDE) --- Heptabromodiphenyl (HeptaBDE) --- Octabromodiphenyl (OctaBDE) --- Nonabromodiphenyl (NonaBDE) --- Decabromodiphenyl (DecaBDE) --- (3) Limit It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

31 TESTING ITEM Fluor (F) content Report No.: MX Date: RESULT (ppm) (3) Chlorine (Cl) content 202 Bromine (Br) content Iodine (I) content ppm = parts per million based on dry weight of sample. µg/cm 2 = microgram per square centimeter. mg/kg WITH 50cm 2 = milligram per kilogram with 50 square centimeter. < = less than. = Not detected. The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω. Prepared and checked by: For Intertek Laboratory Manager The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,). NOTE :DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMEMENT 2005/717/EC. # =ACCORDING TO IEC 62321, A POSITIVE RESULT IICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION A SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX WERE TESTED TOGETHER. Test method: It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

32 Report No.: MX Date: Sample Number 3 Testing item Chromium VI (Cr 6+ ) content Ω Testing method With reference to USEPA 3060, by EPA 7196 Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm QHU p76, MELA 20,0 Sample Number 3 3 Testing item POLYBROMINATE D BIPHENYLS (PBBs) POLYBROMINATE D DIPHENYL ETHERS (PBDEs) Ω Testing method Quality control Batch: Analysis Date: Determined by GC-MSD PCL Determined by GC-MSD PCL Analyzed By: CONT CONT Reporting limit ppm 50,0 50,0 Sample Number Testing item Ω Testing method Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm 3 Lead (Pb) content With reference to USEPA 3052, by EPA 6010 MET p MARY 5,0 Sample Number Testing item Ω Testing method Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm 3 Cadmium (Cd) content With reference to USEPA 3052, by EPA 6010 MET p MARY 2,0 Sample Number Testing item Ω Testing method Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm 3 Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET p RNC 0,25 Sample Number 3 Fluor 3 Chlorine 3 Bromine 3 Iodine Testing item Testing method Quality control Batch: Analysis Date: With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography Analyzed By: CONT CONT CONT CONT Reporting limit ppm It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

33 Test Report Number : TWNC Applicant: Littelfuse, S.A. de C.V. Date : Jun 30, 2011 Blvd. Fausto Z. Martinez #1800 Col. Magisterio Seccion 38 C.P Piedra Negras, Coahuila, Mexico Sample Description: One (1) group of submitted samples said to be : Part Description : COLORANT BROWN Part Number : Date Sample Received : Jun 28, 2011 Date Test Started : Jun 28, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 1 Of 6

34 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Number : TWNC Result (ppm) Black Plastic Pellets Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Jun 28, 2011 Test Period : Jun 28, 2011 to Jun 30, 2011 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 2 Of 6

35 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Number : TWNC Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 2 ppm 1 ppm Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 3 Of 6

36 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MSD Biphenyls (PBBs) and further HPLC confirmation when 5 ppm necessary. Polybrominated Diphenyl Ethers (PBDEs) With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. Remark: Reporting limit = Quantitation limit of analyte in sample 5 ppm Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 4 Of 6

37 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 5 Of 6

38 Test Conducted Number : TWNC Photo Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 6 Of 6

39 Test Report Number : TWNC Applicant: Littelfuse, S.A. de C.V. Date : Jun 30, 2011 Blvd. Fausto Z. Martinez #1800 Col. Magisterio Seccion 38 C.P Piedra Negras, Coahuila, Mexico Sample Description: One (1) group of submitted samples said to be : Part Description : COLORANT RED Part Number : Date Sample Received : Jun 28, 2011 Date Test Started : Jun 28, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 1 Of 6

40 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Number : TWNC Result (ppm) Black Plastic Pellets Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Jun 28, 2011 Test Period : Jun 28, 2011 to Jun 30, 2011 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 2 Of 6

41 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Number : TWNC Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 2 ppm 1 ppm Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 3 Of 6

42 Number : TWNC Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MSD Biphenyls (PBBs) and further HPLC confirmation when 5 ppm necessary. Polybrominated Diphenyl Ethers (PBDEs) With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. Remark: Reporting limit = Quantitation limit of analyte in sample 5 ppm Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 4 Of 6

43 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 5 Of 6

44 Test Conducted Number : TWNC Photo Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 6 Of 6

45 Report No.: MX Date: RESULTS REPORT INTERTEK TESTING SERVICES DE MEXICO SA DE CV LABORATORIO CD. DE MEXICO DELIVER TO: Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila ATTENTION: Ing. María Valdez It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

46 Report No.: MX Date: TEST REPORT APPLICANT Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila Ing. María Valdez SAMPLE DESCRIPTION One (1) group of submitted samples said to be : Sample Description Serie 287 Item No. 1) N/P Colorant Yellow Country of Origin NP Buyer's Name NP Supplier's Name NP Date sample received Testing period to ******************************************************************************************** TEST COUCTED As requested by the applicant, for details please refer to attached pages. ******************************************************************************************** CONCLUSION Sample Number Testing item Conclusion Failed component Failed result Pass 1 N/P Colorant Yellow See Result summary ******************************************************************************************** TEST COUCTED It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

47 Samples: Report No.: MX Date: ) N/P Colorant Yellow TEST RESULT SUMMARY FOR RoHS DIRECTIVE : TESTING ITEM Ω RESULT (ppm) Cadmium (Cd) content 0,01% (100 ppm) Lead (Pb) content 0,1% (1000 ppm) Mercury (Hg) content 0,1% (1000 ppm) Chromium (VI) (Cr 6+ ) 0,1% (1000 ppm) POLYBROMINATED BIPHENYLS (PBBs) Total 0,1% (1000 ppm) Monobromobiphenyl (MonoBB) --- Dibromobiphenyl (DiBB) --- Tribromobiphenyl (TriBB) --- Tetrabromobiphenyl (TetraBB) --- Pentabromobiphenyl (PentaBB) --- Hexabromobiphenyl (HexaBB) --- Heptabromobiphenyl (HeptaBB) --- Octabromobiphenyl (OctaBB) --- Nonabromobiphenyl (NonaBB) --- Decabromobiphenyl (DecaBB) --- POLYBROMINATED DIPHENYL ETHERS (PBDEs) Total 0,1% (1000 ppm) Monobromodiphenyl (MonoBDE) --- Dibromodiphenyl (DiBDE) --- Tribromodiphenyl (TriBDE) --- Tetrabromodiphenyl (TetraBDE) --- Pentabromodiphenyl (PentaBDE) --- Hexabromodiphenyl (HexaBDE) --- Heptabromodiphenyl (HeptaBDE) --- Octabromodiphenyl (OctaBDE) --- Nonabromodiphenyl (NonaBDE) --- Decabromodiphenyl (DecaBDE) --- (1) Limit It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

48 TESTING ITEM Fluor (F) content Chlorine (Cl) content Bromine (Br) content Iodine (I) content Report No.: MX Date: RESULT (ppm) (1) ppm = parts per million based on dry weight of sample. µg/cm 2 = microgram per square centimeter. mg/kg WITH 50cm 2 = milligram per kilogram with 50 square centimeter. < = less than. = Not detected. The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω. Prepared and checked by: For Intertek Laboratory Manager The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,). NOTE :DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMEMENT 2005/717/EC. # =ACCORDING TO IEC 62321, A POSITIVE RESULT IICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION A SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX WERE TESTED TOGETHER. Test method: It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

49 Report No.: MX Date: Sample Number 1 Testing item Chromium VI (Cr 6+ ) content Ω Testing method With reference to USEPA 3060, by EPA 7196 Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm QHU p76, MELA 20,0 Sample Number 1 1 Testing item POLYBROMINATE D BIPHENYLS (PBBs) POLYBROMINATE D DIPHENYL ETHERS (PBDEs) Ω Testing method Quality control Batch: Analysis Date: Determined by GC-MSD PCL Determined by GC-MSD PCL Analyzed By: CONT CONT Reporting limit ppm 50,0 50,0 Sample Number Testing item Ω Testing method Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm 1 Lead (Pb) content With reference to USEPA 3052, by EPA 6010 MET p MARY 5,0 Sample Number Testing item Ω Testing method Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm 1 Cadmium (Cd) content With reference to USEPA 3052, by EPA 6010 MET p MARY 2,0 Sample Number Testing item Ω Testing method Quality control Batch: Analysis Date: Analyzed By: Reporting limit ppm 1 Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET p RNC 0,25 Sample Number 1 Fluor 1 Chlorine 1 Bromine 1 Iodine Testing item Testing method Quality control Batch: Analysis Date: With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography With reference to EN 14582:2007 by calorimetric bomb method with oxygen and PCL determined by ion chromatography Analyzed By: CONT CONT CONT CONT Reporting limit ppm It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s). 1ª. Emisión Junio 2005, 1 Revisión Junio 26, ILTA/003/GENS-F8 Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo C.P , Del. Azcapotzalco, México, D.F. Tel.:

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55 Applicant: Test Report Littelfuse S.A. de C.V. Automotive Business Unit Blvd. Fausto Z. Martinez #1800 Col. Magisterio Seccion 38 C.P Piedras Negras, Coahuila Mexico. Number : TWNC Date : Jul 08, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : BODY (TECHNYL) Part Number : Date Sample Received : Jul 05, 2011 Date Test Started : Jul 05, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 1 Of 6

56 Number : TWNC Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Test Item Black Plastic Pellets Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) 571 Bromine (Br) Iodine (I) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Jul 05, 2011 Test Period : Jul 05, 2011 To Jul 08, 2011 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 2 Of 6

57 Number : TWNC Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC edition Cadmium (Cd) 1.0:2008 in clause 8/9/10, by microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content determined by ICP-OES. With reference to IEC edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to IEC edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 3 Of 6

58 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Acid Added For Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 4 Of 6

59 Number : TWNC Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard:EN Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 5 Of 6

60 Number : TWNC Test Conducted Photo Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) Fax: (+886-2) Page 6 Of 6