RAMA KRISHNA PEDDINTI, Ph.D.
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1 RAMA KRISHNA PEDDINTI, Ph.D. Associate Professor Department of Chemistry Indian Institute of Technology Roorkee Roorkee , Uttarakhand, INDIA Tel: (0) RESEARCH AREAS Asymmetric Synthesis Domino Reactions Arene Functionalizations Green Protocols in Organic Synthesis Carbohydrate Research Antibacterial Activity Studies Purification and structure determination of proteins RESEARCH HIGHLIGHTS The group has developed various asymmetric organocatalysts from naturally available proline and derivatives of camphor-10-sulfonic acid and glucosamines. The catalytic activity of these organocatalysts has been investigated in various asymmetric transformations. Novel sugar derivatives were synthesized. Developed green protocols for the synthesis of an array of heterocycles under solvent-free and catalyst-free conditions. Synthesized several vesicular acetylcholine transporter inhibitors. Highly unstable o-benzoquinone monoimines were chemically generated for the synthesis of hitherto unknown 1,4-benzoxazine derivatives. A plethora of halogenated bicyclo[2.2.2]octenones were synthesized. SELECTED PUBLICATIONS Recent papers S. K. R. Parumala, S. R. Surasani, R. K. Peddinti S-Arylation of thiols with masked o-benzoquinones: Synthesis of alkyl aryl/diaryl sulfides. New J. Chem (DOI: /c4nj01381f) 1
2 S. R. Surasani, S. K. R. Parumala, R. K. Peddinti Diels-Alder reactions of 4-halo masked o-benzoquinones. Experimental and theoretical investigations. Org. Biomol. Chem. 2014, 12, R. T. Naganaboina, A. Nayak, R. K. Peddinti Expedient synthesis of novel 1,4-benzoxazine and butenolide derivatives. Org. Biomol. Chem. 2014, 12, G. Choudhary, R. T. Naganaboina, R. K. Peddinti Expedient synthesis of novel 1,4-benzoxazine and butenolide derivatives. RSC Advances 2014, 4, S. K. R. Parumala, R. K. Peddinti Reversal of polarity in masked o-benzoquinones: Rapid access to unsymmetrical oxygenated biaryls. Org. Lett. 2013, 15, R. T. Naganaboina, R. K. Peddinti BF 3.etherate mediated Friedel-Crafts alkylation of arenes with 2-hydroxy-1,4- benzoxazines: Synthesis of 2-aryl-1,4-benzoxazine derivatives. J. Org. Chem. 2013, 78, Synthesis and characterization of monosaccharide derivatives and application of sugar-based prolinamides in asymmetric synthesis. Eur. J. Org. Chem. 2012, N. Bodipati, R. K. Peddinti Hypervalent iodine mediated synthesis of carbamate protected p-quinone monoimine ketals and p-benzoquinone monoketals. Org. Biomol. Chem. 2012, 10, N. Bodipati, R. K. Peddinti Chemical generation of o-quinone monoimines: Rapid construction of novel 1,4- benzoxazine derivatives. Org. Biomol. Chem. 2012, 10, (Hot paper) G. Choudhary, R. K. Peddinti Introduction of a clean and promising protocol for the synthesis of Michael adducts and 1,4-benzoheterocycles: An emerging innovation. Green Chem. 2011, 13, Glucosamine-based primary amines as novel organocatalysts for the asymmetric aldol reaction. J. Org. Chem. 2011, 76, G. Choudhary, R. K. Peddinti Towards absolute green protocol: An expeditious, highly efficient, catalyst-free and solvent-free synthesis of nitroamines and nitrosulfides by Michael addition. 2
3 Green Chem. 2011, 13, R. Rani, R. K. Peddinti Michael reaction of ketones and -nitrostyrenes catalyzed by camphor-10- sulfonamide-based prolinamide Tetrahedron Asymm. 2010, 21, Sugar-based novel organocatalysts: Enantioselective aldol reactions of cycloalkanones with aromatic aldehydes. Tetrahedron Asymm. 2010, 21, R. Rani, R. K. Peddinti Camphor-based novel organocatalysts: Enantioselective aldol reactions of cycloalkanones with aromatic aldehydes. Tetrahedron Asymm. 2010, 21, C.-C. Liao, R. K. Peddinti Chapter 4 (1,2-Naphthoquinones including 1,5-, 1,7-, 2,3-, 2,6-naphthoquinones) in Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, Volume 28 (Quinones and Heteroatom Analogs), PROJECTS COMPLETED 1. Asymmetric Organocatalysis with L-Proline and its Derivatives. Nov Feb. 2009, DST. 2. Novel,-Diarylprolinol-derived Chiral Ligands for Catalytic Asymmetric Synthesis. CSIR, Apr Sept Dearomatization of 3-Methoxy-2-naphthol: Synthesis of Benzannulated Bicyclo[2.2.2]octenone Frameworks. MHRD, Apr Mar Novel Methodologies for the Generation of o-benzoquinone Monoimides: Synthesis of 1,4-Benzoxazine Derivatives. CSIR, Oct 2009 Mar Microwave Heating Technology: A Green Chemistry Approach for Functionalization of Arenes. MHRD, May 2010 Apr ONGOING PROJECTS 1. Domino Reactions and Asymmetric Organocatalytic Reactions. DST, Jun May
4 GROUP MEMBERS (Ph.D.) 1. Rashmi Rani (Graduated in 2011) 2. Garima (Graduated in 2011) 3. Jyoti Agarwal (Graduated in 2011) 4. Seshi Reddy Surasani (Graduated in 2011) 5. Naganjaneyulu Bodipati (Graduated in 2012) 6. Ram Tilak Naganaboina (Graduated in 2014) 7. Jyoti Singh Tomar (2010-) 8. Santosh Kr. Reddy Parumala (2011-) 9. Arun Sharma (2011-) 10. Ujjawal Kumar Bhagat (2011-) 11. Shivangi Sharma (2011-) 12. Pallavi Singh (2012-) 13. Balakrishna Aegurula (2013-) 14. Neha Taneja (2013-) 15. Shweta Bisht (2013-) 16. Nitika Sharma (2013-) 17. Piyush Tehri (2014-) PROJECT FELLOWS M.Tech. 1. Srinivasa Rao Palla (Biological Activity Studies) 1. Hemkant Saini (2013-) 2. Pravin Kumar (2013-) PREVIOUS GROUP MEMBERS (M.Sc. & M.Tech.) Year of Year of M.Sc. M.Tech. Graduation Graduation Anjali Jha 2005 Virendra Singh Rajora 2006 Sudarshana Mukherjee 2005 Mahesh Chander Singh 2007 Sujata Kashyap 2005 Deepika Kanwar 2008 Garima Singh 2006 Bhaskara Rao Pasumarti 2010 Jissy A. K Monika Das 2011 Anju Duley 2007 Ankita Singh 2013 Shankha Pattanayak 2007 Ankur Singhal 2014 Dipankar Sahoo 2008 Farhana Shehla 2008 Sunil Kumar Bonagani 2009 Nithish Kumar Verma
5 Oishika Panda 2012 Donthi Murali 2013 Shikha Sharma 2014 RESEARCH FACILITIES The research group is well equipped with basic facilities to perform reactions for organic synthesis/ asymmetric synthesis. Laboratory has facilities to carry out reactions under inert atmosphere and at low temperatures up to 90 o C. It also procured HPLC instrument along with chiral columns. In addition, instruments such as FT-IR, UV-Vis, GC, GC-MS, HRMS, CHN analyzer, etc., are available in the Department and 500 MHz NMR and XRD instruments are available in the Institute Instrumentation Centre. FURTHER DETAILS OF THE GROUP For further details of the group, visit the following sites metric_synthesis_lab.html 5
RAMA KRISHNA PEDDINTI, Ph.D.
RAMA KRISHNA PEDDINTI, Ph.D. Associate Professor Department of Chemistry Indian Institute of Technology Roorkee Roorkee-247667, Uttarakhand, INDIA Tel: (0)1332-285438 E-mail: rkpedfcy@iitr.ernet.in, ramakpeddinti@gmail.com
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