Room-Temperature Quantum Sensing in CMOS: On-Chip Detection of Electronic Spin States in Diamond Color Centers for Magnetometry

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Mohamed I. Ibrahim*, Christopher Foy*, Donggyu Kim*, Dirk R.

1 Room-Temperature Quantum Sensing in CMOS: On-Chip Detection of Electronic Spin States in Diamond Color Centers for Magnetometry Mohamed I. Ibrahim*, Christopher Foy*, Donggyu Kim*, Dirk R. Englund, and Ruonan Han *Equal Contribution Massachusetts Institute of Technology

2 Introduction CMOS-Based Quantum Magnetometer System Architecture Microwave Signal Generation Optical Excitation Filtering Optical Fluorescence Readout Experimental Data Measurement Results Using Layer of Nano-Diamonds Measurement Results Using Bulk Diamond Conclusion Outline Slide 1

3 Nitrogen Vacancy (NV) in Diamond Magnetometer Nitrogen vacancy center in diamond Optically detected magnetic resonance (ODMR) Slide 2

Nitrogen Vacancy (NV) in Diamond Magnetometer 0.

4 Nitrogen Vacancy (NV) in Diamond Magnetometer nt/ Hz Ensemble of NVs Clevenson, et al. Nature Physics 2015 Clevenson, et al. Nature Physics 2015 Sensitivity Where N is number of NVs Slide 3

Nature (2008) Bacteria magnetic imaging Le Sage, et al.

5 Nitrogen Vacancy (NV) in Diamond Magnetometer Magnetic structure imaging Balasubramanian, et al. Nature (2008) Bacteria magnetic imaging Le Sage, et al. Nature 2013 Nano-tesla sensitivity Nanometer spatial resolution Vector field measurements Ambient conditions (room temperature) Slide 4

6 NV Magnetometer System Components Green Laser Signal generator Photodetector Microwave antenna CMOS integrated NV magnetometer (TSMC 65nm Le Sage, LP et process) al. Nature 2013 Optical filters Slide 5

7 Introduction CMOS Based Quantum Magnetometer System Architecture Microwave Signal Generation Optical Excitation Filtering Optical Fluorescence Readout Experimental Results Measurement Results Using Layer of Nano-Diamonds Measurement Results Using Bulk Diamond Conclusion Outline Slide 6

8 CMOS Based Quantum Magnetometer Slide 7

9 Microwave Signal Generation 2.87 GHz microwave signal generation 2.6 GHz 3.1 GHz for optically detected magnetic resonance (ODMR) measurements 10 Gauss field strength at 2.87 GHz with 95% homogeneity To increase the contrast To drive the NVs with equal strength for spin control pulsed sequences (Echo, Ramsey,..) Slide 8

10 Microwave Signal Generation Microwave Coil B z = B 0 1 π Q E k 1 α2 β 2 + K k Q 4α α =, β =, k =, r = x + y and Q = 1 + a + β ma is required to get 10 Gauss for diameter coil Slide 9

11 Microwave Signal Generation Microwave Coil Slide 10

12 Microwave Signal Generation Microwave Coil EM simulated performance Slide 11

13 Microwave Signal Generation 10 Gauss with 95% uniformity 6 ma DC current in the driver 25x field strength more than simple non-resonant loop 2.6 GHz-3.1 GHz Microwave frequency sweep Slide 12

14 Optical Spin Readout Optical filter is required for green light rejection Photodiode is used to detect red fluorescence Slide 13

15 Optical Excitation Filtering Plasmonic Filter Green light (532 nm) Filter 3D structure 800 nm Red light (700 nm) Filter cross section 900 nm Measured isolation is 10 db FDTD simulated performance Slide 14

16 Optical Fluorescence Readout P+ N-well Photo-diode P Eddy L L diode P Eddy 4 Cuts the losses in anode and cathode n n diode P Eddy L3 n L 3 Measured responsivity is 0.23 A/W Slide 15

17 Introduction CMOS Based Quantum Magnetometer System Architecture Microwave Signal Generation Optical Excitation Filtering Optical Fluorescence Readout Experimental Results Measurement Results Using Layer of Nano-Diamonds Measurement Results Using Bulk Diamond Conclusion Outline Slide 16

18 Passivation Layer Removal Background fluorescence is emitted from the passivation (silicon nitrite) layer Reactive ion etching (RIE) for passivation layer removal 250 µm 250 µm Fluorescence Intensity Fluorescence Intensity Before etching After etching Slide 17

19 Nano-Diamonds Deposition Deposition of diamond nano-crystals solution 250 µm 250 µm Before deposition After deposition & evaporation Slide 18

20 Nano-Diamonds Measurement Results Sensitivity: CW where γ = 1 σδν γ C = 2.8 MHz/Gauss, σ Std. dev., Δν Linewidth, C Contrast, t Integration Time Slide 19

21 Bulk Diamond Measurement Results Sensitivity: CW where γ = 1 σ γ m = 2.8 MHz/Gauss, σ Std. dev., m, t Integration Time Slide 20

22 Bulk Diamond Measurement Results Slide 21

23 Introduction CMOS Based Quantum Magnetometer System Architecture Microwave Signal Generation Optical Excitation Filtering Optical Fluorescence Readout Experimental Results Measurement Results Using Layer of Nano-Diamonds Measurement Results Using Bulk Diamond Conclusion Outline Slide 22

24 Performance Summary Technology Vector meas. Optical isolation Sensing area Form factor Sensitivity This work (Nanodiamonds) 65nm CMOS No 10 db 50 μm 50 μm ~ 1 3 ** 73 μt Hz This work (Bulk Diamond) 65nm CMOS Yes 20 db 50 μm 50 μm ~ 1 3 ** 2.5 μt Hz Nature physics (2015) * Discrete devices Yes >60 db 1 mm 1mm ~ nt Hz *Clevenson, et al. Nature Physics 2015 ** Does not include LASER Slide 23

25 Conclusion Combines the advantages of CMOS and NV center in diamond in a small form factor Couples tightly the CMOS components with NV qubits Offers on-chip spin state readout Easy integration of control logic Less IOs Closed-loop feedback between spin-manipulation and readout Enables compact and scalable advanced quantum systems. Slide 24

Nitrogen-Vacancy Centers in Diamond A solid-state defect with applications from nanoscale-mri to quantum computing

Nitrogen-Vacancy Centers in Diamond A solid-state defect with applications from nanoscale-mri to quantum computing Research into nitrogen-vacancy centers in diamond has exploded in the last decade (see