GSA DATA REPOSITORY Grasby et al. Supplemental Methods
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1 GSA DATA REPOSITORY Grasby et al. Supplemental Methods The previously reported Buchanan Lake section (Grasby and Beauchamp, 2009; Grasby et al., 2011; Sanei et al., 2012), was sampled from 20 to 100 cm intervals over 142 m (234 samples). Smith Creek area data, reported here for the first time, represents 900 m of lower Triassic strata sampled at 3 m intervals (271 samples). The lower 475 m of the section was sampled along a small tributary, one km southwest of Smith Creek where the upper Griesbachian to lower Smithian (up to the occurrence of E. romunderi) record is best exposed and easily accessible. The remainder of the section (starting from the occurrence of E. romunderi) was sampled along Smith Creek. In the field outcrop surfaces were cleaned and fresh exposed rock was collected. In the laboratory any remaining weathered surfaces were removed and clean samples were powdered using an agate mortar and pestle. Total organic carbon (TOC) was measured using Rock-Eval 6, with +- 5% analitical error of reported value, based on repeats and reproducibility of standards run after every 5th sample. Elemental determinations for Mo and Al are based on total dissolution of the sample using concentrated nitric, perchloric and hydrofluoric acids followed by a lithium metaborate fusion of any residual material. Samples were analyzed by ICP mass spectrometry (+- 5% based on reproducibility of standards). For determination of 13 C org, samples were washed with hydrochloric acid, and rinsed with distilled water to remove any carbonate before determination of 13 C of organic carbon ( 13 C org +/ 0.2 ). Stable isotope measurements were conducted at the Isotope Science Laboratory, University of Calgary. Based on regional thermal maturation studies, using spore, pollen and conodont color alteration, and vitrinite reflectance (Utting et al., 1989), our studied sections are located in a thermal alteration index (TAI) zone of 4 or less (below greenschist facies), indicating that alteration of 13 C org values due to burial diagenesis is negligible (Hayes et al., 1983). References Grasby, S.E., and Beauchamp, B., 2009, Latest Permian to Early Triassic basin-to-shelf anoxia in the Sverdrup Basin, Arctic Canada: Chemical Geology, v. 264, p , doi: /j.chemgeo Grasby, S.E., Sanei, H., and Beauchamp, B., 2011, Catastrophic dispersion of coal fly ash into oceans during the latest Permian extinction: Nature Geoscience, v. 4, p , doi: /ngeo1069. Hayes, J.M., Kaplan, I.R., and Wedeking, K.W., 1983, Precambrian organic geochemistry, preservation of the record, in Schopf, J.W., ed., Earth s Earliest Biosphere: Its Origin and Evolution: Princeton, New Jersey, Princeton University Press, p Sanei, H., Grasby, S.E., and Beauchamp, B., 2012, Latest Permian mercury anomalies: Geology, v. 40, p , doi: /g Page 1 of 2
2 Utting, J., Goodarzi, F., Dougherty, B.J., and Henderson, C.M.B., 1989, Thermal maturity of Carboniferous and Permian rocks of the Sverdrup Basin, Canadian Arctic Archipelago Geological Survey of Canada, Paper no , 20 p. Page 2 of 2
3 Supplementary Table DR1: Geochemical Data for the Smith Creek and Buchanan Lake Sections. Depths are measured in metres (m) relative to base of section. N.a = not analysesd Smith Creek Section Buchanan Lake Section Sample no. m above base d 13 C % TOC Mo/Al Fe py % Sample no. m above base d 13 C % TOC Mo/Al Fe py % C C C C C C C C C C C C C C C C C n.a C C C C C C C C C C C C n.a C C C C C C C C C C C C C C C C C C C C C C C C C C C n.a C C C C C C C C C C
4 C C C C C C a C C a C C a C C a C C a C C a C C a C C a C C a n.a C C a C C a C C a C C a C C a C n.a C a C C a C C a C C a C C a C C a C C a C C a C C a C C a C C a C C a n.a C C a C C a C C a C C a C C a C C a n.a C n.a C a C C C C
5 C C C C C C C C C C C n.a C C C C C C C C C C C C C C C C C C C C C C C C C C C C C C C C n.a C C C C C C C C C C n.a C C C C n.a C C C C n.a C C C C C C C C C C C C C
6 C C C C C C C C C C C C C C C C C C C C C C C n.a C C C C C C C C C n.a C C C C C C C C C C C C C n.a C C C
7 C C C C C C C C C C n.a C n.a C C C C C C C C C C C n.a C C C C C C C C C C C n.a C C C C
8 C C C C C C C C C C C C C C C C n.a C C n.a C C C C C C C C C C C C C C C C C C C
9 C C C C C C C C C C C C C C C C C C C C C C C C C n.a C n.a C C C C C C C C C C C
10 C C C C C C C C C C C C C C C C C
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