Engineering - CLS Day. Thomas Ellis Director of Research Canadian Light Source

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1 Engineering - CLS Day Thomas Ellis Director of Research Canadian Light Source

2 E-gun & Linear Accelerator 250 MeV Canadian Light Source Transfer Line & Booster Ring Commissioned Storage Ring 2.9 GeV 200 ma Commissioned Beamlines & End Stations Commissioning

3 SYNCHROTRON BRILLIANCE AND ESRF FLUX 1E+15 X-Ray tube - 110KV - 2.5mm ESRF ID 200mA - Wiggler: 1.4T - 1.6m - 150mm Photons/s/0.1%/mrad 1E+14 1E+13 1E+12 1E+11 1E+10 1E Photon Energy (KeV)

4 CLS Linac LINAC ELECTRON GUN

5 CLS Booster BOOSTER RING LINAC-BOOSTER INJECTION

6 CLS Storage Ring STORAGE RING BOOSTER-STORAGE RING INJECTION

7 Typical Storage Ring Sector SYNCHROTRON LIGHT TO EXPERIMENTAL STATIONS PLAN VIEW (1 of 12 CELLS) meter SCALE ELECTRON BEAM

8 Storage Ring Sector

9 Beamline Construction SGM/PGM First Radiation Enclosure Shield Wall Plane Grating Monochromator Beamline Spherical Grating Monochromator Beamline

10 Phase I Beamlines OSR HXMA Far IR Mid IR SGM PGM SM CMCF

11 CLS Beamlines

12 Brilliance at the CLS

13 Techniques X-ray absorption near edge structure (XANES) Extended X-ray absorption fine structure (EXAFS) X-ray diffraction (XRD) Fourier transform infrared (FTIR) spectroscopy and microscopy

14 Fibrinogen on filler-loaded polyurethane STXM scanning transmission X-ray microscopy - detect transmitted X-rays; image by raster scanning sample SR Linear absorption (OD for 1 nm *10-3 ) Styrene-acrylonitrile fibrinogen PIPA polyurethane matrix Energy (ev) Chemical map derived from pixel-by-pixel fit of reference spectra to image sequence SAN PIPA Fg Hitchcock, Morin, Brash et al, J. Biomaterials Science Poly. Ed. (2002) 2 µm

15 Microprobe Study of Mine Tailings 5 µm Spot Size 500 µm As(-1) + As(III) As(V) 500 µm Energy (kev) Nickel Map Arsenic Map As(-1) + As(III) As(V) Energy (kev) Iron Map Calcium Map B.T. Moldovan, D.T. Jiang, M.J. Hendry Environ. Sci. Technol. 37, 873 (2003) Photon Energy: 12 kev Spot size: 5µm

16 Principle of synchrotron-radiation-based extended X-ray absorption fine structure (EXAFS) McGill sample: B crystalline scorodite Backscattering adsorption x(k) X-ray k(χ -1 ) Energy (kev) Scattering As k edge spectrum for crystalline scorodite [Fe(AsO) 4 2H 2 O] Element-specific-edge jump XAFS (oscillation) Single scattering model

17 Phase I Beamlines OSR HXMA Far IR Mid IR SGM PGM SM CMCF

18 Beamline Progress October 2004 First PGM experiment March 2005 First light into HXMA hutch First SGM experiment May 2005 First light into Far-IR hutch First HXMA experiment First Far-IR experiment First scheduled PGM user June 2005 First scheduled SGM user July 2005 First scheduled HXMA user Installation of CMCF undulator August 2005 First light from CMCF undulator September 2005 First light into SM hutch First light into Mid-IR hutch

19 User Access to CLS Three Types of Access General User Peer Reviewed Intent to Publish $1 per 8 hour shift Beamline Team Priority Access MOU negotiated % Program peer reviewed every three years Purchased 1 st come, 1 st served Commercial or academic No peer review Proprietary research Rates based on cost recovery and services offered

20 CALL FOR PROPOSALS Deadline: October 3, 2005 Canadian Light Source Inc. is again issuing a limited call for proposals for experimental beam time for the period of January 1 to June 30, This call includes the following beamlines: PGM - Variable Line Spacing Plane Grating Monochromator ( ev) SGM - High Resolution Spherical Grating Monochromator ( ev) HXMA - Hard X-ray MicroAnalysis (5,000 40,000 ev) Far IR - High Resolution Far Infrared Spectroscopy ( cm-1) Mid IR - Mid IR Spectromicroscopy ( cm-1)

21 Useful Contacts User Services Office Industry Events & e-news

22 CLSI 8th Annual Users' Meeting and Workshops November 18th - 20th, 2005

23 Paul Dumas - Synchrotron SOLEIL Infrared Synchrotron Emission: From Spectroscopy to Imaging Thomas Irving - Illinois Institute of Technology, (BioCAT) Time-resolved X-ray Diffraction Studies of Indirect Flight Muscle of Living Drosophila Johannes Lehmann - Cornell University, Soil Fertility Management/Soil Biogeochemistry Synchrotron-based Spectroscopy in soil organic matter research Rob Lewis - Monash University, X-ray and Synchrotron Physics Lungs Revealed: Phase Contrast X-Ray Imaging Brian Mark - University of Manitoba, Department of Microbiology Resolving a 400 Angstrom Cell Edge Using Synchrotron X-ray Radiation to Successfully Determine the Crystal Structure of Human Hexosaminidase by Multiple Isomorphous Replacement Derek Peak - University of Saskatchewan, Soil Science Using P XANES Spectroscopy to Improve Management of Soils Receiving Biosolids and Animal Manures Elisabeth Schultke - University of Saskatchewan, Anatomy & Cell Biology Overcoming Size Limitations: Imaging in a Small Animal Model of Malignant Brain Tumor Mark Sutton - McGill University, The Centre for the Physics of Materials Using Coherent X-rays to Study Thermal Fluctuations in Materials: Watching Atoms Dance John Tse - University of Saskatchewan, Physics & Engineering Physics High Pressure and Synchrotron Radiation

24 Associated Workshops: Building Time Resolved Experimental Programs at the Canadian Light Source (Full Day) Applications of Micro-Tomography in Science (1/2 Day) Pioneering Research in Plant Science Using Synchrotron Light (1/2 Day) Synchrotron Applications in Paleontology and Archaeology (1/2 Day)

25 Phase II layout BMIT SyLMAND SXRBM VESPERS REIXS CMCF2

26 Available Phase III BMIT Available Phase III CLS North Face

27 Initial Capital Funding Partners Operating Funding Partners

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