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1 Elsevier Editorial System(tm) for Computers & Chemical Engineering Manuscript Draft Manuscript Number: Title: Optimisation of a torus reactor geometry using CFD Article Type: Escape 19 Keywords: Optimisation; CFD; Geometry; Torus reactor Corresponding Author: Dr. Christophe Bengoa, Ph.D. Corresponding Author's Institution: Universitat Rovira i Virgili First Author: Laura Pramparo, Ph.D. Order of Authors: Laura Pramparo, Ph.D.; Jeremy Pruvost, Ph.D.; Frank Stüber, Ph.D.; Josep Font, Ph.D.; Agustí Fortuny, Ph.D.; Azael Fabregat, Ph.D.; Patrick Legentilhomme, Ph.D.; Jack Legrand, Ph.D.; Christophe Bengoa, Ph.D. Abstract: Different configurations of torus reactors were investigated, batch and continuous operating modes, square and circular cross-sectioned geometries and, a scale-up of the reactor was finally conducted (100mL, 300mL and 4L). The torus reactor was simulated using the commercial code Fluent. In batch conditions, a linear evolution of the mean circulation velocities with respect to the impeller rotation speed was obtained using square and circular-sectioned torus reactors of 100 ml. Negligible differences were found between both types of section. Finally, the reactor volume was scaled-up from a 100 ml to 300 ml and to a 4 L reactor volume. Larger reactor allowed higher bulk velocities for same impeller rotation speed. Reynolds number and Reynolds mixing number were also calculated. The mean velocities obtained in this case were significantly higher. However, same obtained relationship between Reynolds numbers denoted an important result for scaling-up the performance of torus reactor.
2 * Manuscript Click here to view linked References Optimisation of a torus reactor geometry using CFD Laura Pramparo, a, Jeremy Pruvost, b Frank Stüber, a Josep Font, a Agustí Fortuny, c Azael Fabregat, a Patrick Legentilhomme, b Jack Legrand, b Christophe Bengoa, a,* a Departament d Enginyeria Química, Escola Tècnica Superior d Enginyeria Química, Universitat Rovira i Virgili, Av. Països Catalans 26, Tarragona, Spain b GEPEA, UMR-CNRS 6144, Université de Nantes, CRTT, B.P. 406,F-44602, Saint- Nazaire Cédex, France c Department of Chemical Engineering, Universitat Politecnica de Catalunya, Víctor Balaguer, Vilanova i la Geltrú, Spain. Present address: Departament d Enginyeria Química, Edifici Q-ETSE, Universitat Autònoma de Barcelona, Bellaterra, Spain * Corresponding author. Tel: , Fax: , christophe.bengoa@urv.cat 1
3 Abstract Different configurations of torus reactors were investigated, batch and continuous operating modes, square and circular cross-sectioned geometries and, a scale-up of the reactor was finally conducted (100mL, 300mL and 4L). The torus reactor was simulated using the commercial code Fluent. In batch conditions, a linear evolution of the mean circulation velocities with respect to the impeller rotation speed was obtained using square and circular-sectioned torus reactors of 100 ml. Negligible differences were found between both types of section. Finally, the reactor volume was scaled-up from a 100 ml to 300 ml and to a 4 L reactor volume. Larger reactor allowed higher bulk velocities for same impeller rotation speed. Reynolds number and Reynolds mixing number were also calculated. The mean velocities obtained in this case were significantly higher. However, same obtained relationship between Reynolds numbers denoted an important result for scaling-up the performance of torus reactor. Keywords: Optimisation; CFD; Geometry; Torus reactor 1. Introduction Despite experimental studies have confirmed efficiency of the torus geometry, the optimal conception of torus reactors and their utilisation in industrial scale production require still theoretical research. Little information about hydrodynamic characteristics involved in torus shape reactors is known. Khalid et al. (1996) and Khalid and Legrand 2
4 On the other hand, the Reynolds and the Reynolds mixing numbers for the 4 L reactor were also calculated and are presented in figure 5. A linear relation between the Reynolds and the Reynolds mixing numbers was obtained. This relation is comparable to the one obtained for the 100 ml torus reactor (equation 5), thus, the same approximation was used. Then, there is no difference whatever the reactor volume. It is good for extrapolation. 4. Conclusions The characterization of the flow-field in a torus reactor of 100 ml was carried out for two different configurations. It was obtained that the hydrodynamic is mainly a function of the impeller rotation speed. Negligible influence on the hydrodynamic was observed for flow inlets located perpendicular to the flow circulation. No differences were found using a circular-sectioned reactor due to the small volume and the high turbulence generated inside it. A 300 ml square-sectioned reactor seemed to be more effective than the 100 ml one because it presents higher bulk velocities similar to those predicted for a torus reactor with circular section. However, same relationship was obtained for Reynolds numbers, denoting same performance. The CFD analysis of the 4 L torus reactor shows that better velocities are obtained for bigger volumes of reactor. However, same relationship was found between Reynolds and Reynolds mixing number for all studied configurations. The main practical interest of this work is the possibility to have the same hydrodynamic behaviour for a 0.3 L torus reactor as for several litres torus reactors. This is an important result for scaling-up the performance obtained in lab-scale torus reactor. 11
5 Acknowledgements Laura Pramparo is indebted to the Universitat Rovira i Virgili and the Agència de Gestió d Ajuts Universitaris i de Recerca (AGAUR) of Catalan Government for the predoctoral scholarships. Financial support was provided by the European Community, project REMOVALS, FP References Belleville, P., Nouri L., & Legrand, J. (1992). Mixing characteristics in the torus reactor. Chem. Eng. Technol., 15, 282. Benkhelifa, H., Legrand J., Legentilhomme P., & Montillet, A. (2000). Study of the hydrodynamic behaviour of the batch and continuous torus reactors in laminar and turbulent flow regimes by means of tracer methods. Chem. Eng. Sci., 55, Brucato, A., Ciofalo M., Grisafi F., & Micale, G. (1998). Numerical prediction of flowfields in baffled stirred vessels: a comparison of alternative modeling approaches. Chem. Eng. Sci., 53, Khalid, A., & Legrand, J. (2001). Energy dissipation distribution and mixing in a torus reactor. Chem. Eng. Com., 185,
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