Response Surface Methodology
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1 Response Surface Methodology Bruce A Craig Department of Statistics Purdue University STAT 514 Topic 27 1
2 Response Surface Methodology Interested in response y in relation to numeric factors x Relationship between y and x is unknown Describe influence using model y = f(x)+ǫ Objective is to find levels which maximize response y = f(x 1,x 2,...,x k )+ǫ ǫ represents noise or error in response Call η = f(x 1,x 2,...,x k ) the response surface Contours - values of x such that η is constant STAT 514 Topic 27 2
3 1st and 2nd Order Approximations Use suitable approximation of f First order - Linear function of factors y = β 0 +β 1 x β k x k +ǫ Second order - Quadratic function of factors y = β 0 + β i x i + β ii x 2 i + β ij x i x j +ǫ While both approximations are likely unrealistic in toto, often resonable in small region of surface Use sequential approach to find optimum 1 Response surface design determines {x i } 2 Least squares to estimate parameters 3 Use resulting contours to move in optimal direction STAT 514 Topic 27 3
4 The Method of Steepest Ascent Move rapidly to general vicinity of optimum Use approximate model to move in proper direction Consider linear model ˆη = ˆβ 0 + k ˆβ i x i i=1 Contours of ˆη are series of parallel lines Move in direction which increase ˆη the quickest Move perpendicular to contour lines Often center points to make determination easier STAT 514 Topic 27 4
5 The Method of Steepest Ascent Direction based on the slope estimates ˆβ i Steps proportional to the regression coefficients Choose step size for one of the variables ( x j ) Move others accordingly x i = ˆβ i ˆβ j / x j See Table 11-3 for an example STAT 514 Topic 27 5
6 Example Consider Montgomery Problem A chemical plant produces oxygen by liquefying air and separating it into its component gases by fractional distillation. Current operating conditions are Temp = -220 C and pressure ratio of 1.2. The researchers are interested in maximizing the purity of oxygen. They ran a 2 2 factorial with n = 4 center points. Given the center points, we can test for interaction. The data are coded temp = Temp pres = Ratio data purity; input temp pres x1x1 = temp*temp; x1x2 = temp*pres; cards; ; proc reg; model pure = temp pres x1x1 x1x2; STAT 514 Topic 27 6
7 Example - SAS output Dependent Variable: PURE Sum of Mean Source DF Squares Square F Value Prob>F Model Error C Total Parameter Standard T for H0: Variable DF Estimate Error Parameter=0 Prob > T INTERCEP TEMP PRES X1X X1X A one degree change in temp is equivalent to a 1/5=.2 temp step once standardized. This means we increase pressure by (.2)(.25/.85) =.059. STAT 514 Topic 27 7
8 Example - SAS output The following table summarizes moving in this direction and the observed purity (simulated results). It appears that a maximum is reached around ten steps. Another linear approximation should be made centered now at (-210,1.2590). ŷ ij = x T +.25x P Coded Natural Variables Variables Steps x 1 x 2 Temp Pres Response STAT 514 Topic 27 8
9 Checking Linear Approximation Do Lack of Fit Test : Use the center points to estimate pure error. Use SS Interaction or ˆβ 12 (created by adding x 1 x 2 term in the model) to compute lack of fit error. ˆσ 2 = /4 3 =.2 3 =.0666 If linear, there will be no interaction effect. The estimate ˆβ 12 is simply 1/2 the estimated effect which is 2ˆβ 12 =.5( ) =.2 The SS 12 =(.4) 2 /4 =.04. This is also the lack-of-fit SS. The F test is.04/.0666 = 0.6 and has a P-value of around.5. Compare average of center points to design points : If there is no curvature, the average of the four design points should be equal to the average of the center points. The difference between these two averages is an estimate of the pure quadratic term β 11 +β 22. In this example, it is 336/ /4 =.2 The SS is (4)(4)(.2) 2 /(4+4) =.08. The F test is.08/ = 1.33 and has a P-value of around.3. This also suggests that the linear model is appropriate. STAT 514 Topic 27 9
10 Analysis of Second Order Model Due to curvature, determine stationary point ˆη x i = 0 Stationary point is a minimum, maximum, or saddle point Use contours or canonical analysis to determine behavior Can write quadratic approximation as (page 486) y = β 0 +x b+x Bx+ǫ Solution is x s =.5B 1 b with ˆη = ˆβ x sb Canonical analysis looks at eigenvalues and eigenvectors of B STAT 514 Topic 27 10
11 Example Consider Montgomery Problem An experimenter wants to optimize crystal growth as a function of three variables x 1,x 2, and x 3. The design used is a factorial with six center points and six axial points (see Figure 11-20). We will use Proc RSREG which does a quadratic response surface analysis. data purity; input x1 x2 x3 cards; ; proc rsreg; model resp=x1 x2 x3 / lackfit; STAT 514 Topic 27 11
12 Example - SAS Output Breaks down regression SS into linear, quadratic terms Degrees of Type I Sum Regression Freedom of Squares R-Square F-Ratio Prob > F Linear Quadratic Crossproduct Total Regress **Appears to be a quadratic component but very little crossproduct **Overall regression not significant but that s not a concern **Would expect contours to be fairly circular Does lack of fit test Degrees of Sum of Residual Freedom Squares Mean Square F-Ratio Prob > F Lack of Fit Pure Error Total Error **No apparent lack of fit to quadratic model STAT 514 Topic 27 12
13 Example - SAS Output Gives the parameter estimates and standard errors Deg of Parameter Standard T for H0: Parameter Freedom Estimate Error Parameter=0 INTERCEPT X X X X1*X X2*X X2*X X3*X X3*X X3*X ***Large T for 2 of the three quadratic terms STAT 514 Topic 27 13
14 Performs canonical analysis Example - SAS Output Degrees of Sum of Factor Freedom Squares Mean Square F-Ratio Prob > F X X X Canonical Analysis of Response Surface (based on coded data) Critical Value Factor Coded Uncoded X X X Predicted value at stationary point Eigenvectors Eigenvalues X1 X2 X Stationary point is a maximum. STAT 514 Topic 27 14
15 Response Surface Designs Want points sparse but give info over entire region Blocking is possible Designs can be built sequentially Provides internal estimate of error/lack of fit Orthogonal first order designs Minimize the variance of regression coefficients 2 k Factorial (with center points) Fractional factorial of Resolution III or higher Central composite designs (2nd order) 2 k factorial Fractional factorial of Resolution V or higher Add center points and 2k axial runs STAT 514 Topic 27 15
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