K.O.C Operational Laboratories Quality Control System. KHALID AL-OTAIBI Chief Chemist, Kuwait Oil Company

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3 K.O.C Operational Laboratories Quality Control System KHALID AL-OTAIBI Chief Chemist, Kuwait Oil Company

4 Khalid Al-Otaibi: Biography Current position: Chief Chemist in Operational Laboratories Team K.O.C since Oct 2015 Current Responsibilities: Managing NK Effluent and sea water Labs Implementing QC procedure Developing opportunities to improve OL capability Designing and coordinating chemical field trails. Previous History: 8 years in K.O.C as production Chemist overseeing all laboratories procedures 2 years in Kuwait inertial ministry as laboratories chemist. He has Bs. Degree in Chemistry from Kuwait University.

5 Talk Outline Introduction The Importance of laboratories quality Laboratories Quality Control System Laborites Quality Control Examples Chemical Quality Control FT-IR Quality test Example Summary and Conclusion

6 Introduction 13 Operational Laboratories in KOC daily routine samples daily tests. Lab results are key to safe and efficient operations Accuracy of the lab results Lab quality control system required Field Chemicals QC.

7 The Importance of laboratories quality Laboratory Quality = Accuracy + Reliability + Timeliness Some inaccuracy is always there in the data generated. Negative consequences of laboratory error. The laboratory is a complex system, involving many steps of activity and many people. The challenge is to reduce the level of inaccuracy. In order to achieve the highest level of accuracy and reliability, its essential to perform all processes and procedures in the laboratory in the best possible way. Quality control system must consider the entire system to achieve good laboratory performance

8 Laboratories Quality Control System Laboratory quality control system It is an ongoing, comprehensive program which analyzes every aspect of an entire operation; it involves determining a quality goal deciding whether or not the goal has been achieved implementing corrective action if the goal has not been reached The QC system must: Assess the samples are representative. Assess the effectiveness of the lab s policies and procedures Assure the accurate, reliable, and prompt reporting of test results. Identify and correct problems. Assure the adequacy and competency of the staff.

9 Operational Laboratories Processes There are many procedures and processes that are performed in the laboratory, and each of these must be carried out correctly in order to assure accuracy and reliability of testing. Monitoring & feedback Samples Receiving and logged in Reporting and record keeping Prepare the samples for testing Results reviewing and approving Samples Analysis

10 Operational Laboratories QC System Elements Technician Performance Quality of the reagents Unified updated procedure Calibrated Glassware How we ensure the Quality of our Results Samples Receiving and handling Calibrated Instruments Documents and records Results reporting

11 Log Sample - Routine

12 Calibration Sheet for Equipment

13 Lab Technicians Performance

14 Lab Technicians Performance

15 Lab Technicians Performance (Ranking)

16 Chemicals quality control Why do need field chemicals Chemical Selection To optimize production. To reduce risks Operate safely and efficiently Meet Kuwait export crude specification. Feed back Chemical Performance Monitoring Chemical Field Trial Field Chemical Supply Chemical QC

17 Operational Laboratories Chemical QC Volume Laser gun to determine the chemical volume in drums. Tank dipping Field Chemicals QC Elements Physical Properties Chemical Properties Visual inspection Density Viscosity ph Flash point Active Ingredients FT-IR

18 Chemical FT-IR

19 Key messages Improved accuracy, accountability has led to ISO accreditation. Improved Work Distribution and better Time Management Minimized influence of human error. Developed a healthy competition & good team spirit among the staffs. Improved the image toward all the end users Brought an awareness among the chemical supplier to be more vigilant on the quality of supplied chemicals.

20 Thank You

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