HYDRO. Norsk Hydro a.s Bergen. Research Centre documentation. Exploration and Production
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1 HYDRO Norsk Hydro a.s Bergen. Doc. type: I_I Agreement I I Amendment LJU Report L_l Other Research Centre documentation Exploration and Production. Storage I_ years I_ years
2 ANALYTICAL PROGRAM
3 EXPERIMENTAL: GC/MS saturated biomarkers Analytical method: version June (Mass Spectometric Detection Saturated-biomarkers version C)
4 Detection parameters for pre-selected. common fragmention-ions: Experiment method: Detected retension time interval: :: -:: GC/FID Splitine Cl :T> of the iniected sampje Cycle time: GC/MS
5 Automatic sampler HP- Splittless injection:
6 EXPERIMENTAL: GC/MS aromatic biomarkers Analytical method: MSD_ARO version March (Mass Spectometric Detection Aromatic-biomarkers) Gas chromatographic and linked quadropole Mass Spectrometric (MS) analysis of Aromatic biomarkers. And a parallel Flame lonization Detection (FID)
7 Detection parameters
8 Automatic sampler HP- Splittless injection:. mm./splm : Injected sample:
9 EXPERIMENTAL: GC/MS-MRM Analytical method: MRS A version Oct. (Metastable reaction monitoring version-a) Gas chromatographic and st field-free region metastable reaction monitoring analysis of saturated biomarkers. Detected pre-selected groups
10 Detection parameters for ore-selected parent-daughter ion transitions: Experiment method:
11 Automatic samnler HP- Splittless inj l min /splitt l. Injected sample:
12 RESULTS The data are presented by increasing depths and accordingly: Results from
13 Results from
14 Detected comounds and annotations accorordin to the "Norweian Industr Guide to Oranic Geochemical Analysis. Feb. ": Internal standard Abbrev. baa Ion-window,
15 -JZ.OUKV abs abr abs abr abs STERANES: Pregnanes abr Abbrev
16 Saturated biomarkers, SAT-MSD, peak heights MSDSXLS Sample Type File name _D _.D _.D _.D.D.D..D _.D.D _.D _.D _.D _.D _.D _.D _.D _.D.D.D.D.D.D.D.D.D.D.D.D.D.D.D.D _S.D File path F E E E E E E E E E E E E E E E E E DS F F F F F F F F F F F F DS DA Proj.tf Operator Method JKB.GN H H H H H H H H H H H H H H H H H Aquired date Seq.#.. :.. :.. :..:.. :.. :.. :.. :.. :..:.. :.. :.. :..:.. :.. :..:.. :..:..:..:.. :.. :..:.. :..:..:.. :.. :..:..:..:..: Workup Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Amounts: baa
17 Saturated biomarkers, SAT-MSD, peak heights MSDS.XLS.. : Sample Heights: baa / / / / / / i /R /S /R /S o /R /S / Ts norab Tm b o norab ab sos
18 Saturated biomarkers, SAT-MSD, peak heights MSDS.XLS.. : Sample norab ab Ts ba D ab L D ba G abs abr ba abs abr abs abr abs abr abs abr aa
19 Saturated biomarkers, SAT-MSD, peak heights MSDSXLS Sample bb aa bb dbs dbr bbr bbs aar bbr bbs aas bbr bbs aar bbr bbs
20 Saturated biomarkers, SAT-MSD, absolute amounts MSDS.XLS.. : Sample Type L File name.d _.D J.D _.D..D.D _.D _.D.D _.D..D..D _.D..D _.D _.D _.D.D.D.D.D.D.D.D.D.D.D.D.D.D.D.D _S.D File path F E E E E E E E E E E E E E E E E E DS F F F F F F F F F F F F DS DA Proj.# Operator Method JKB.GN H H H H H H H H H H H H H H H H H MSD S C MSD S C Aquired date Seq.#.. :.. :.. :.. :.. :.. :.. :.. :.. :.. :.. :.. :.. :..:.. :.. :.. :.. :..:..:..:.. :.. :..:.. :..:..:.. :.. :..:..:..:..: Workup Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Geochem Amounts: baa
21 Saturated biomarkers, SAT-MSD, absolute amounts MSDS.XLS.. : Sample / / / / / / /R /S /R /S /R /S / Ts norab Tm b norab ab norab
22 Saturated biomarkers, SAT-MSD, absolute amounts MSDSXLS Sample ab Ts ba D ab D L_ ba G abs abr ba abs abr abs abr abs abr abs abr - aa bb aa
23 Saturated biomarkers, SAT-MSD, absolute amounts MSDSXLS Sample bb dbs dbr bbr bbs aar bbr bbs aas bbr bbs aar bbr bbs
24 Saturated biomarkers, SAT-MSD, peak heights MSDS.XLS..: Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA Type File name File path Lab.ref. BIOM.D DS Lab.ref. BIOM.D DS Lab.ref. BIOMA.D E Lab.ref. BIOMA.D E Lab.ref. BIOMA.D E Lab.ref. BIOMA.D E Lab.ref. BIOMA.D F Lab.ref. BIOMA.D F Proj.# Operator Method Aquired date Seq.#..:..:.. :.. :..:.. :..:.. : Workup Amounts: baa
25 Saturated biomarkers, SAT-MSD, peak heights MSDS.XLS.. : Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA Heights: baa / / / / / / /R /S /R /S /R /S / Ts norab Tm b norab ab
26 Saturated biomarkers, SAT-MSD, peak heights MSDS.XLS.. : Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA norab ab Ts ba D ab D ba G abs abr ba abs abr abs abr abs abr abs abr aa
27 Saturated biomarkers, SAT-MSD, peak heights MSDS.XLS..: Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA bb aa bb dbs dbr bbr bbs aar bbr bbs aas bbr bbs aar bbr bbs
28 Saturated biomarkers, SAT-MSD, absolute amounts MSDS.XLS..: Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA Type File name File path Lab.ref. BIOM.D DS Lab.ref. BIOM.D DS Lab.ref. BIOMA.D E Lab.ref. BIOMA.D E Lab.ref. BIOMA.D E Lab.ref. BIOMA.D E Lab.ref. BIOMA.D F Lab.ref. BIOMA.D F Proj.# Operator Method Aquired date Seq.#..:..:.. :.. :..:.. :..:.. : Workup Amounts: baa
29 Saturated biomarkers, SAT-MSD, absolute amounts MSDS.XLS..: Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA / / / / / / /R /S /R /S /R /S / Ts norab Tm b norab ab norab
30 Saturated biomarkers, SAT-MSD, absolute amounts MSDS.XLS.. : Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA ab Ts ba D ab D ba G abs abr ba abs abr abs abr abs abr abs abr aa bb aa
31 Saturated biomarkers, SAT-MSD, absolute amounts MSDS.XLS.. : Sample BIOM BIOM BIOMA BIOMA BIOMA BIOMA BIOMA BIOMA bb dbs dbr bbr bbs aar bbr bbs aas bbr bbs aar bbr bbs
32 Results from
33 Detected compounds and annotations accorording to the "Norwegian Industry Guide to Organic Geochemical Analysis. Feb. ": Internal standard Aryl isoprenoids Abbreviation d-n dlo-p -C CAI CAI CAI CAI CAI CAI CAI CAI C AI CAI C Naphtalenes
34 Biphenyls Fluorenes Dibenzothiophene Phenantrenes Retene Triaromatic,,-TMN BP -MBP -MBP C-BP C-BP C-BP F Cl-F Cl-F J-MF DBT -MDBT +-MDBT -MDBT JP -MP -MP -MP -MP EP+EP+,DMP EP,+,+,-DMP,+,+,+,-DMP,+,+,-DMP,-DMP,-DMP,+,+,-DMP,-DMP Reiene TA TA STA RTÅ/STA STA RTA KTA , <
35 Aromatic biomarkers, Well /- compound amounts ng/mg EOM or peak heights Sample name: Type File name _A.D _A.D _A.D _A.D.D.D.D.D.D.D File path: E E E E DA DA CA CA DA DA Project Misc.info Operator: Method: MSD_ARO MSD_ARO MSD_ARO MSD_ARO MSD_ARO MSD_ARO MSD_ARO MSD_ARO MSD_ARO Amounts:
36 Aromatic biomarkers, Well /- compound amounts ng/mg
37 Aromatic biomarkers, Well /- compound amounts ng/mg EOM or peak heights Compound amounts Sample name: N -MN -MN -EN
38 Aromatic biomarkers, Well /- compound amounts ng/mg
39 Aromatic biomarkers, Well /- compound amounts ng/mg
40 Aromatic biomarkers, Well /- compound amounts ng/mg EOM or peak heights Compound amounts Sample name: ,+,+,-dmp,+,+,+, -DMP,+,+,-DMP,-DMP,-DMP,+,+, -DMP,-DMP Retene Peak heights Sample name: ,+,+,-dmp,+,+,+,-dmp,+,+,-dmp,-dmp,-dmp,+,+,-dmp,-dmp Retene Page
41 Compound amounts Aromatic biomarkers, Well /- compound amounts ng/mg EOM or peak heights Sample name: TA TA STA RTA/STA STA RTA RTA Peak heights Sample name: TA TA STA
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