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1 Certificate of Alysis Certificate Number Client Earth Science Partnership 33 Cardiff Road Taffs Well Cardiff CF15 7RB 03-Apr-17 Our Reference Client Reference Order No Contract Title Description Date Received Date Started Date Completed Test Procedures Notes d Prince Charles Hospital 66 Soil samples. Wednesday, March 22, 2017 Wednesday, March 22, 2017 Monday, April 3, 2017 Identified by prefix DETSn (details on request). This report supersedes Extra testin. Opinions and interpretations are outside the scope of UKAS accreditation. This certificate is issued in accordance with the accreditation requirements of the United Kindom Accreditation Service. The results reported herein relate only to the material supplied to the laboratory. Observations and interpretations are outside the scope of ISO This certificate shall not be reproduced except in full, without the prior written approval of the laboratory. Approved By Rob Brown Business Maer Derwentside Environmental Testin Services Limited Unit 2, Park Road Industrial Estate South, Consett, Co Durham, DH8 5PY Tel: Pae 1 of 11.
2 Summary of Asbestos Alysis Lab No Sample ID Material Type Result Comment* Alyst HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert HDP SOIL Amosite Small bundle of Amosite Steven Lambert HDP SOIL Amosite bundles of Amosite fibres Steven Lambert HDP SOIL Amosite Amosite present as fibre bundle Steven Lambert HDP03A 1.20 SOIL Amosite Small bundle of Amosite Steven Lambert HDP SOIL Chrysotile Bundle of Chrysotile Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert HDP SOIL Amosite bundles of Amosite fibres Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Chrysotile Bundles of Chrysotile and bundles of Steven Lambert Amosite HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundle of Amosite Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundle of Amosite Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert Pae 2 of 11
3 Summary of Asbestos Alysis Lab No Sample ID Material Type Result Comment* Alyst HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL Amosite Small bundles of Amosite Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP30A 0.75 SOIL Amosite Small bundle of Amosite Steven Lambert HDP31A 0.50 SOIL Amosite Amosite present in visable insulation Steven Lambert and fibre bundles HDP31A 1.00 SOIL Amosite Amosite present as fibre bundles Steven Lambert HDP32A 0.05 SOIL NAD none Steven Lambert HDP32A 0.30 SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert HDP SOIL NAD none Steven Lambert Crocidolite = Blue Asbestos, Amosite = Brown Asbestos, Chrysotile = White Asbestos. Anthophyllite, Actinolite and Tremolite are other forms of Asbestos. Samples are alysed by DETSC 1101 usin polarised liht microscopy in accordance with HSG248 and documented in-house methods. NAD = No Asbestos Detected. Where a sample is NAD, the result is based on alysis of at least 2 sub-samples and should be taken to mean 'no asbestos detected in sample'. Key: * -not included in laboratory scope of accreditation. Pae 3 of 11
4 Summary of Asbestos Quantification Alysis Lab No Sample ID HDP01 HDP02 HDP02 HDP03 Depth Sample Type SOIL SOIL SOIL SOIL Samplin Date 09-Mar Mar Mar Mar-17 Samplin Time Total Mass% Asbestos (a+b+c) DETSC 1102 Mass % Gravimetric Quantification (a) DETSC 1102 Mass % Detailed Gravimetric Quantification (b) DETSC 1102 Mass % Quantification by PCOM (c) DETSC 1102 Mass % Potentially Respirable Fibres (d) DETSC 1102 Fibres/ Breakdown of Gravimetric Alysis (a) Mass of Sample Breakdown of Detailed Gravimetric Alysis (b) % Amphibole bundles in sample Mass % % Chrysotile bundles in sample Mass % Breakdown of PCOM Alysis (c) % Amphibole fibres in sample Mass % % Chrysotile fibres in sample Mass % Breakdown of Potentially Respirable Fibre Alysis (d) Amphibole fibres Fibres/ Chrysotile fibres Fibres/ % asbestos in Asbestos Containin Materials (ACMs) is determined by Recommended sample size for quantification is approximately 1k # denotes deviatin sample Pae 4 of 11
5 Summary of Asbestos Quantification Alysi Lab No Sample ID Depth Sample Type Samplin Date Samplin Time Total Mass% Asbestos (a+b+c) DETSC 1102 Mass % Gravimetric Quantification (a) DETSC 1102 Mass % Detailed Gravimetric Quantification (b) DETSC 1102 Mass % Quantification by PCOM (c) DETSC 1102 Mass % Potentially Respirable Fibres (d) DETSC 1102 Fibres/ Breakdown of Gravimetric Alysis (a) Mass of Sample Breakdown of Detailed Gravimetric Alysis (b) % Amphibole bundles in sample Mass % % Chrysotile bundles in sample Mass % Breakdown of PCOM Alysis (c) % Amphibole fibres in sample Mass % % Chrysotile fibres in sample Mass % Breakdown of Potentially Respirable Fibre Alysis (d) Amphibole fibres Chrysotile fibres Fibres/ Fibres/ HDP03A HDP04 HDP05 HDP SOIL SOIL SOIL SOIL 08-Mar Mar Mar Mar < < < % asbestos in Asbestos Containin Materials (ACMs) is determined by Recommended sample size for quantification is approximately 1k # denotes deviatin sample Pae 5 of 11
6 Summary of Asbestos Quantification Alysi Lab No Sample ID Depth Sample Type Samplin Date Samplin Time Total Mass% Asbestos (a+b+c) DETSC 1102 Mass % Gravimetric Quantification (a) DETSC 1102 Mass % Detailed Gravimetric Quantification (b) DETSC 1102 Mass % Quantification by PCOM (c) DETSC 1102 Mass % Potentially Respirable Fibres (d) DETSC 1102 Fibres/ Breakdown of Gravimetric Alysis (a) Mass of Sample Breakdown of Detailed Gravimetric Alysis (b) % Amphibole bundles in sample Mass % % Chrysotile bundles in sample Mass % Breakdown of PCOM Alysis (c) % Amphibole fibres in sample Mass % % Chrysotile fibres in sample Mass % Breakdown of Potentially Respirable Fibre Alysis (d) Amphibole fibres Chrysotile fibres Fibres/ Fibres/ HDP06 HDP07 HDP08 HDP SOIL SOIL SOIL SOIL 07-Mar Mar Mar Mar < < <0.001 <0.001 % asbestos in Asbestos Containin Materials (ACMs) is determined by Recommended sample size for quantification is approximately 1k # denotes deviatin sample Pae 6 of 11
7 Summary of Asbestos Quantification Alysi Lab No Sample ID Depth Sample Type Samplin Date Samplin Time Total Mass% Asbestos (a+b+c) DETSC 1102 Mass % Gravimetric Quantification (a) DETSC 1102 Mass % Detailed Gravimetric Quantification (b) DETSC 1102 Mass % Quantification by PCOM (c) DETSC 1102 Mass % Potentially Respirable Fibres (d) DETSC 1102 Fibres/ Breakdown of Gravimetric Alysis (a) Mass of Sample Breakdown of Detailed Gravimetric Alysis (b) % Amphibole bundles in sample Mass % % Chrysotile bundles in sample Mass % Breakdown of PCOM Alysis (c) % Amphibole fibres in sample Mass % % Chrysotile fibres in sample Mass % Breakdown of Potentially Respirable Fibre Alysis (d) Amphibole fibres Chrysotile fibres Fibres/ Fibres/ HDP16 HDP17 HDP22 HDP SOIL SOIL SOIL SOIL 17-Mar Mar Mar Mar < < < <0.001 <0.001 < <0.001 <0.001 <0.001 % asbestos in Asbestos Containin Materials (ACMs) is determined by Recommended sample size for quantification is approximately 1k # denotes deviatin sample Pae 7 of 11
8 Summary of Asbestos Quantification Alysi Lab No Sample ID Depth Sample Type Samplin Date Samplin Time Total Mass% Asbestos (a+b+c) DETSC 1102 Mass % Gravimetric Quantification (a) DETSC 1102 Mass % Detailed Gravimetric Quantification (b) DETSC 1102 Mass % Quantification by PCOM (c) DETSC 1102 Mass % Potentially Respirable Fibres (d) DETSC 1102 Fibres/ Breakdown of Gravimetric Alysis (a) Mass of Sample Breakdown of Detailed Gravimetric Alysis (b) % Amphibole bundles in sample Mass % % Chrysotile bundles in sample Mass % Breakdown of PCOM Alysis (c) % Amphibole fibres in sample Mass % % Chrysotile fibres in sample Mass % Breakdown of Potentially Respirable Fibre Alysis (d) Amphibole fibres Chrysotile fibres Fibres/ Fibres/ HDP26 HDP30A SOIL 09-Mar-17 SOIL 16-Mar < < Insulation < HDP31A 0.50 SOIL 16-Mar LFAD % asbestos in Asbestos Containin Materials (ACMs) is determined by Recommended sample size for quantification is approximately 1k # denotes deviatin sample Pae 8 of 11
9 Summary of Asbestos Quantification Alysi Lab No Sample ID Depth Sample Type Samplin Date Samplin Time Total Mass% Asbestos (a+b+c) DETSC 1102 Mass % Gravimetric Quantification (a) DETSC 1102 Mass % Detailed Gravimetric Quantification (b) DETSC 1102 Mass % Quantification by PCOM (c) DETSC 1102 Mass % Potentially Respirable Fibres (d) DETSC 1102 Fibres/ Breakdown of Gravimetric Alysis (a) Mass of Sample Breakdown of Detailed Gravimetric Alysis (b) % Amphibole bundles in sample Mass % % Chrysotile bundles in sample Mass % Breakdown of PCOM Alysis (c) % Amphibole fibres in sample Mass % % Chrysotile fibres in sample Mass % Breakdown of Potentially Respirable Fibre Alysis (d) Amphibole fibres Chrysotile fibres Fibres/ Fibres/ HDP31A 1.00 SOIL 16-Mar Insulation % asbestos in Asbestos Containin Materials (ACMs) is determined by Recommended sample size for quantification is approximately 1k # denotes deviatin sample Pae 9 of 11
10 Information in Support of the Alytical Results Contract Prince Charles Hospital Containers Received & Deviatin Samples Lab No Sample ID Date Sampled Containers Received HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP03A 1.20 SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L Holdin time exceeded for tests Ippropriate container for tests Pae 10 of 11
11 Information in Support of the Alytical Results Contract Prince Charles Hospital Holdin time exceeded for tests Ippropriate container for tests Lab No Sample ID Date Sampled Containers Received HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP30A 0.75 SOIL PT 1L HDP31A 0.50 SOIL PT 1L HDP31A 1.00 SOIL PT 1L HDP32A 0.05 SOIL PT 1L HDP32A 0.30 SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L HDP SOIL PT 1L Key: P-Plastic T-Tub DETS cannot be held responsible for the interity of samples received whereby the laboratory did not undertake the samplin. In this instance samples received may be deviatin. Deviatin Sample criteria are based on British and Intertiol standards and laboratory trials in conjunction with the UKAS note 'Guidance on Deviatin Samples'. All samples received are listed above. However, those samples that have additiol comments in relation to hold time, ippropriate containers etc are deviatin due to the reasons stated. This means that the alysis is accredited where applicable, but results may be compromised due to sample deviations. If no sampled date (soils) or date+time (waters) has been supplied then samples are deviatin. However, if you are able to supply a sampled date (and time for waters) this will prevent samples bein reported as deviatin where specific hold times are not exceeded and where the container supplied is suitable. Disposal From the issue date of this test certificate, samples will be held for the followin times prior to disposal :- Soils - 1 month, Liquids - 2 weeks, Asbestos (test portion) - 6 months Pae 11 of 11
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