ECX LLC Bellingham, WA 98226

Transcription

1 CX LLC Bellingham, WA Carbnyl Assay Samples Reeived: 8/11/2015 Analysis Repr ( ) GC/MS Analysis (NT225) Diaeyl 2,3-Penanedine (aka Aeyl prpinyl) Aein (3-Hydrxy-2-Buanne) nhalpy Analyial, n. Phne: (919) / Fax: (919) / Capila Drive Durham, NC

2 erify ha he bes f my knwledge all analyial daa presened in his repr summary: Have been heked fr mpleeness Are aurae, errr-free, and legible Have been ndued in ardane wih apprved prl This analyial repr was prepared in Prable Dumen Frma (.PDF) and nains 11 pages. Repr ssued: 8/27/2015 A# Page 2 f 11

3 Summary f Resuls A# Page 3 f 11

4 Repr fr: CX LLC Prje Cde: Clien Prje: na Prje Sar Dae: 8/11/15 Analysis Mehd: NT225 nhalpy Cde Clien Sample D Diaeyl Cnenrains, ug/ml 2,3- Penanedine # Aein # mmral Fg - The Beas 34 J < 1.07 ND < 12 ND mmral Fg - Asensin 4.03 J mmral Fg - Awakening 2.46 J mmral Fg - Avaln < 1.13 ND < 1.07 ND < 12 ND mmral Fg - Legendary < 1.13 ND < 1.07 ND < 12 ND mmral Fg - nfinie Bliss < 1.13 ND < 1.07 ND < 12 ND #: Aein is als knwn as 3-hydrxy-2-buanne and 2,3-Penanedine is als knwn as aeyl prpinyl. ND: Nn Dee r analyial resul belw he MDL and is less han (<) he repred value. J: Resul is belw he lwer urve limi & abve he MDL and is nsidered esimaed value DAP arbs, TableCarbs Page 1 f 1 A# Page 4 f 11 8/27/ :45 AM

5 Narraive Summary A# Page 5 f 11

6 nhalpy Analyial Narraive Summary Cmpany CX LLC Clien Prj na Analys JM Jb # Parameers GC/MS Analysis # Samples 6 e-liquids Cusdy Carbnyls (NT225) Summer Mims reeived he samples n 8/11/15 afer being relinquished by CX LLC. The samples were reeived a ambien emperaure and in gd ndiin. On he sample Chain f Cusdy mmral Fg Asensin was lised wie bu he lab reeived ne sample eah f mmral Fg Asensin and mmral Fg Legendary. Prir, during, and afer analysis, he samples were kep under lk wih aess nly auhrized persnnel by nhalpy Analyial, n. The samples were analyzed fr diaeyl, 2,3-penanedine (aka aeyl prpinyl), and aein (aka 3-hydrxy-2-buanne) fllwing he analyial predures in nhalpy SOP NT225. A measured vlume f sample was mbined wih a measured vlume f aenirile. A measured amun f inernal sandard (buanedined6) was added and he vial apped and mixed hrughly mbine. An aliqu was hen analyzed quaniaively agains a linear alibrain urve using a GC/MS. The Agilen Tehnlgies Mdel 7890A Gas Chrmagraph mpa was equipped wih a 5975C Mass Seleive Deer and an apprpriae lumn fr hese analyses. QC Nes Repring Nes Qualiy nrl samples fr his prje me all aepane rieria unless herwise ned. Sample and alibrain urve hrmagrams are available upn reques. The resuls presened in his repr are represenaive f he samples as prvided he labrary. A# Page 6 f 11

7 General Repring Nes The fllwing are general repring nes ha are appliable all nhalpy Analyial, n. TSC daa reprs, unless speifially ned herwise. The arnym TSC represens nhalpy s Tba Smke Chemisry deparmen. The arnym MDL represens he Minimum Deein Limi. Belw his value, he labrary ann deermine he presene f he analye f ineres reliably. The arnym LOQ represens he Limi f Quaniain (aka Lwes Sandard Value r Lwer Curve Limi). Belw his value, he labrary ann quaniae he analye f ineres wihin he rieria f he mehd. The arnym ND fllwing a value indiaes a nn-dee r analyial resul belw he MDL. The leer J in he Qualifier r Flag lumn in he resuls indiaes ha he value is beween he MDL and he LOQ. The labrary an psiively idenify he analye f ineres as presen, bu he value shuld be nsidered an esimae. The leer in he Qualifier r Flag lumn in he resuls indiaes an analyial resul exeeding 100% f he highes alibrain pin. The assiaed value shuld be nsidered an esimae. The arnym DF represens Diluin Far. This number represens diluin f he sample during he preparain and/r analysis press. The analyial resul aken frm a labrary insrumen is muliplied by he DF deermine he final, undilued sample resul. The addiin f MS he Sample D represens a Marix Spike. An aliqu f an aual sample is spiked wih a knwn amun f analye s ha a peren revery value an be deermined. The MS analysis indiaes wha effe he sample marix may have n he arge analye, i.e. wheher r n anyhing in he sample marix inerferes wih he analysis f he analye(s). The addiin f MSD he Sample D represens a Marix Spike Dupliae. Prepared in he same manner as an MS, he use f dupliae marix spikes allws furher nfirmain f labrary qualiy by shwing he nsiseny f resuls gained by perfrming he same seps muliple imes. The Sample D LCS represens a Labrary Cnrl Sample. Clean marix (similar he lien sample marix) is prepared and analyzed by he labrary using he same reagens, spiking sandards, and predures used fr he lien samples. The LCS is used assess he nrl f he labrary s analyial sysem. A# Page 7 f 11

8 General Repring Nes (ninued) Signifian Figures: Where he repred value is muh greaer han uniy (1.00) in he unis expressed, he number is runded a whle number f unis raher han 3 signifian figures. Fr example, a value f 1, ug/ml is runded 1,456 ug/ml. There are fur signifian digis displayed, bu n nfidene shuld be plaed n mre han w signifian digis. Manual negrain: The daa sysems used fr pressing will flag manually inegraed peaks wih an M. There are several reasns a peak may be manually inegraed. These reasns will be idenified by he fllwing w-leer designains n sample hrmagrams, if prvided in he repr. The peak was n inegraed by he sfware N, he peak was inegraed inrrely by he sfware, r he wrng peak was inegraed by he sfware WP. These des will ampany he analys s manual inegrain samp plaed nex he mpund name n he hrmagram. The suffix Md signifies ha he mehd and/r SOP used has been mdified mee he needs f he analysis. A# Page 8 f 11

9 Sample Cusdy A# Page 9 f 11

10 G l8 d: e g O\; = >: 6; UGrO r u. rb F ;@!, > i= Xe 5 a dd e e*frg F sa= Ag g : rt?6 8 a!().ur,+ \r, e+, d 2 Fg.q : -.J.C z (, 'a - l ql 6l h l@ gls l e)l 3 l = e 8i = O!, ọ - N 4,, (,,. F z r <L F.= r,9, 6 -g J:.LO Y lg '.; r (, (! e g L =.. L ( ri (6.g g p J = LO )a 2(s m (,) L -. () r 6 -.) Ai (g =.g.s p :l U = lr) C ) L = ) (U L (f) C\i (d.6.d p J u = ro ). l< (s = <,) LL L =. 0) 6 TL a.) C\i!, (.g... ( (L J LU qg' -l J-G 6g).r- N (.q. (, ppp :lff f== r ru LO (U : L 6 r d J -r (h d(, 6 ) TL 6 =. ). ( (L (') i r (d.g.g ) O,.u) ).=, TL 6 r) r J H (1 s \ u 0 1,l \r^ ) ii L u lf r r (, sl (! J V + J - hj 2. d? h D6 h d J {r.,{ -a C> > -L (!. r j = =a N () r ) ) x N (n (l, U), (D (a N z d G a s 'a (! A# Page 10 f 11

11 This s The Las Page Of This Repr. A# Page 11 f 11