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1 Supporting Information Wiley-VCH Weinheim, Germany

2 Kombinatorische und Hochdurchsatz-Technologien in der Materialforschung Wilhelm F. Maier,* Klaus Stöwe und Simone Sieg Selected Reviews The interested reader is pointed to a large number of review articles covering many areas of HTT. It has to be mentioned, that most review articles only cover a limited area and concentrate on the work of the authors. One on the first reviews appeared in [1] It reported on combinatorial development of molecular catalysts and the first inorganic catalysts, shortly followed by another one, [2] which contained a drawing of the first parallel polymerization reactor used to assay polymerization catalysts for ethylene polymerization. In 1999 a more comprehensive review [3] already covered about 207 publications on library design and preparation, electronic and magnetic materials, organic materials, polymers, zeolites, organic and polymeric catalysts, inorganic catalysts, electrocatalysts and new technologies for rapid screening of catalytic activity. The first special issue on combinatorial materials science [4] contains several smaller reviews. Also in 1999 I. Maxwell, T. Maschmeyer and coworkers reviewed combinatorial catalysis research and stressed the economic advantages of high speed screening. [5] S. Senkan reviewed in 2001 combinatorial heterogeneous catalysis. [6] At that time not only library design and synthesis as well as various screening technologies had been developed, but important theoretical considerations and technologies, such as genetic or evolutionary algorithms for catalyst development and discovery and data mining had already been applied. A more broader but not very detailed review on combinatorial methods in all areas of catalysis appeared in the same year. [7] HTE in oxidation catalysis has been covered by F. Schüth et al.. [8] Strategies for the search of new heterogeneous catalysts have been summarized by J. Scheidtmann et al.. [9] A general view on the importance of combinatorial materials development was put together by a group of selected scientists in 2000, published in 2001, which is certainly worth reading. [10] A collection of articles on combinatorial instrumentation, catalysis, electronic and magnetic materials was published as a result of the first Japan-US workshop on Combinatorial Materials Science and Technology. [11] This was followed in 2004 by a collection of articles

3 from the second Japan-US-workshop Combinatorial Materials Science and Technology. [12] In 2003 J. Cawse from GE edited a timely book on the theoretical implications of combinatorial and high-throughput research, [13] covering several aspects, such as design of experiment, multi-parameter optimisation strategies, descriptor generation and others. In the same year X. Xiang and I. Takeuchi edited a book on combinatorial materials science with detailed articles, mainly covering thin film materials research conducted in Japan and the US. [14] A short, but informative review of combinatorial methods for characterization of properties of polymers was presented by J.C. Meredith et al.. [15] A collection of articles on high-throughput analysis on optical methods, separation, mass spectrometry, sensors, magnetic, electric and thermal properties, libraries, data management and scale-up were published 2003 in the book edited by R. Potyrailo and E. Amis. [16] In 2004 A. Hagemeyer, P. Strasser and F. Volpe edited a book on high-throughput in chemical catalysis covering technologies, strategies and applications. [17] Selected articles on high-throughput in polymer science can be found in special issues edited in 2003 by U. Schubert and C. Kniep, [18] and in 2004 by U. Schubert and E. Amis. [19] In an article on HTT in polymer research the authors also present a collection of references documenting the application of combinatorial or high-throughput experiments as early as [20] A short, but informative review on combinatorial solid state chemistry of inorganic materials by I. Takeuchi and H. Koinuma mainly covered thin film materials, [21] emphasizing discoveries and new developments based on HTT. Preparation, characterization and applications of amorphous porous mixed oxides prepared by a large variety of sol-gel approaches have been reviewed by G. Frenzer and W. Maier. Special emphasis has been paid to the usefulness of the sol-gel synthesis to explore compositional parameter spaces practically limitless with the help of high throughput technologies. [22] Discovery of new materials and catalysts by HTT is the subject of a review by S. I. Woo et al.. [23] In a brief overview J. Lauterbach and coworkers in 2005 update the developments of HTT in catalysis. [24] The creative use of combinatorial approaches to the development of sensor polymers has been presented by R. Potyrailo. [25] An overview of successful strategies and technologies available for fast and accurate evaluation of structure-property relationships in biomaterials, material properties of thin film polymer libraries and of preparation and study of polymer based reverse micelles has been provided by M. Meier and U.S. Schubert. [26] Screening technologies applied to fuel cell developments have been summarized by J. Liu et al.. [27]

4 Reference List [1] W. H. Weinberg, B. Jandeleit, K. Self, H. Turner, Current Opinion in Solid State & Materials Science 1998, 3, [2] B. Jandeleit, H. W. Turner, T. Uno, J. A. M. Van Beek, W. H. Weinberg, CATTECH 1998, 2, [3] B. Jandeleit, D. J. Schaefer, T. S. Powers, H. W. Turner, W. H. Weinberg, Angewandte Chemie, International Edition 1999, 38, [4] Special Issue of: Biotechnology and Bioengineering, 61(4) (Ed.: P. Spellane) 1998, pp [5] P. P. Pescarmona, J. C. van der Waal, I. E. Maxwell, T. Maschmeyer, Catalysis Letters 1999, 63, [6] S. Senkan, Angewandte Chemie, International Edition 2001, 40, [7] A. Hagemeyer, B. Jandeleit, Y. Liu, D. M. Poojary, H. W. Turner, A. F. Volpe, W. Henry Weinberg, Applied Catalysis, A: General 2001, 221, [8] F. Schueth, O. Busch, C. Hoffmann, T. Johann, C. Kiener, D. Demuth, J. Klein, S. Schunk, W. Strehlau, T. Zech, Topics in Catalysis 2002, 21, [9] J. Scheidtmann, P. A. Weiss, W. F. Maier, Applied Catalysis, A: General 2001, 222, [10] available as Roadmap 2020: [11] Special Issue on the Proceedings of 1st Japan-US Workshop on Combinatorial Material Science and Technology held 1-3 October 2000 in Maui, Hawaii. (in: Appl. Surf. Sci., 2002; 189(3-4)), (Eds.: H. Koinuma, X. D. Xiang, T. Chikyow) 2002, 196 pages. [12] Combinatorial Material Science and Technology, CMST-2. (Proceedings of the Second Japan-US Workshop held in Winter Park, CO 9-11 December 2002.) (in: Appl. Surf. Sci., 2004; 223(1-3)), (Eds.: F. Tsui, J. Hewes) 2004, 267 pages. [13] Experimental Design for High Throughput Materials Development, (Ed.: J. N. Cawse) John Wiley & Sons, Chichester, UK 2003, 320 pages. [14] Combinatorial Materials Synthesis, (Eds.: X. D. Xiang, I. Takeuchi) Marcel Dekker Inc., Basel, CH 2003, 469 pages. [15] J. C. Meredith, A. Karim, E. J. Amis, MRS Bulletin 2002, 27, [16] High-Throughput Analysis: A Tool for Combinatorial Materials Science, (Eds.: R. A. Potyrailo, E. J. Amis) Kluwer Academic / Plenum Publishers, New York 2003, 638 pages.

5 [17] High Throughput Screening in Chemical Catalysis - Technologies, Strategies and Applications, (Eds.: A. Hagemeyer, P. Strasser, A. F. Volpe) Wiley-VCH, Weinheim 2004, 319 pages. [18] Special Issue of: Macromolecular Rapid Communications, 24(1) (Eds.: U. S. Schubert, C. S. Kniep) 2003, pp [19] Special Issue of: Macromolecular Rapid Communications, 25(1) (Eds.: U. S. Schubert, E. J. Amis) 2004, pp [20] R. Hoogenboom, M. A. R. Meier, U. S. Schubert, Macromolecular Rapid Communications 2003, 24, [21] H. Koinuma, I. Takeuchi, Nature Materials 2004, 3, [22] G. Frenzer, W. F. Maier, Annual Review of Materials Research 2006, 36, [23] S. I. Woo, K. W. Kim, H. Y. Cho, K. S. Oh, M. K. Jeon, N. H. Tarte, T. S. Kim, A. Mahmood, QSAR & Combinatorial Science 2005, 24, [24] R. J. Hendershot, C. M. Snively, J. A. Lauterbach, Chemistry - A European Journal 2005, 11, [25] R. A. Potyrailo, Angewandte Chemie, International Edition 2006, 45, [26] M. A. R. Meier, R. Hoogenboom, U. S. Schubert, Macromolecular Rapid Communications 2004, 25, [27] J. H. Liu, M. K. Jeon, A. Mahmood, S. I. Woo, Combinatorial amd High-Throughput Discovery and Optimization of Catalysts and Materials (Eds.: R. A. Potyrailo, W. F. Maier), CRC Taylor & Francis Group, Boca Raton, London, New York, 2006, pp

Combinatorial. materials synthesis by Ichiro Takeuchi 1*, Jochen Lauterbach 2, and Michael J. Fasolka 3

Combinatorial. materials synthesis by Ichiro Takeuchi 1*, Jochen Lauterbach 2, and Michael J. Fasolka 3 Combinatorial materials synthesis by Ichiro Takeuchi 1*, Jochen Lauterbach 2, and Michael J. Fasolka 3 The pace at which major technological changes take place is often dictated by the rate at which new