SCHEDULE OF INORGANIC CHEMISTRY PRACTICALS B.Sc (Biotech.) Sem-I July-August, 2014
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1 SCHEDULE OF INORGANIC CHEMISTRY PRACTICALS B.Sc (Biotech.) Sem-I July-August, 2014 Turn I : Determine the value of x n a sample of Na 2 S 2 O 3.XH 2 O 6.2 g of which are dissolved/litre. Gven N/ 40 Iodine solution. : N/ 40 Iodine solution, Na 2 S 2 O 3. Turn II : The given solution has been prepared by dissolving 6.2g of M 2 s 2 O 3.5H 2 O per litre of the solution. Determine Volumetrically the atomic weight of the metal. : N/ 40 Iodine solution Turn III : Determine Volumetrically value of molecule of water of crystallization in Mohr s salt. 19.6g of which have been dissolved per litre of solution provided N/ 20 K 2 Cr 2 O 7. : Mohr s salt:(nh 4 ) 2 SO 4. FeSo 4. 6H 2 O,Potassium Dichromate (K 2 Cr 2 O 7 ). Turn IV : To the given solution has been prepared by mixing FeSo 4. 7H 2 O and anhydrous Fe2(so 4 ) 3. Determine volumetrically the %age composition of mixture you are provided with N/ 20 k 2 cr 2 O 7 solution. : N/ 20 k 2 cr 2 O 7, Feso 4. 7H 2 O and anhydrous ferric sulphate Turn V : Determine volumetrically the %age purity of given solution Mohr s salt. 21g of which have been dissolved per litre of given solution. Provided N/ 20 KMNO 4. : Mohr s salt:(nh 4 ) 2 SO 4. feso 4. 6H 2 O.
2 September-November 2014 Turn VI : Determine volumetrically value of water of crystallization in Mohr s salt. 19.6g of which have been dissolved per litre of solution provided N/ 20 KMNO 4. : KMNO 4, Mohr s salt, Dil.H 2 SO 4. Turn VII : The given sample was prepared by dissolved 10g of CaCo 3 in Dilhcl and diluting the volume to 1L. Determine volumetrically the % of ca 2+ ions in the sample. : CaCo 3,EDTA,dil.Hcl. Turn VIII : To Determine volumetrically the %age purity of given Sample of the Magnesum sulphate 27g of which are dissolved per litre of given solution provided 1M EDTA solution. : EDTA solution, MgSo 4 (27g) Turn IX : Determine the value of x in a sample of Na 2 S 2 O 3.XH 2 O 6.2 g of which are dissolved/litre. Gven N/ 40 Iodine solution. : N/ 40 Iodine solution, Na 2 S 2 O 3. Turn X : Determine Volumetrically value of molecule of water of crystallization in Mohr s salt. 19.6g of which have been dissolved per litre of solution provided N/ 20 K 2 Cr 2 O 7. Turn XI : Mohr s salt:(nh 4 ) 2 SO 4. feso 4. 6H 2 O, N/ 20 (K 2 Cr 2 O 7 ) solution. : To Determine volumetrically the %age purity of given Sample of the Mgso 4.27g of which are dissolved per litre of given solution provided 1M EDTA solution. : EDTA solution, MgSo 4. Turn XII : The given solution has been prepared by dissolving 6.2g of the M 2 S 2 O 3.5H 2 O pe litre of the solution. Determine volumetrically the atomic weight of the metal. : N/ 40 Iodine solution, M 2 S 2 O 3.5H 2 O.
3 Schedule of organic chemistry practical B.Sc(Bio-tech) Sem-I July-August, 2014 Turn I : To analyse the given organic compound by ignition test and solubility test. Turn-II : To analyse the given organic compound for aldehyde group. Turn-III : To analyse the given organic compound for ketone group. Turn-IV : To analyse the given organic compound for carbohydrate group Turn v To analyse the given orgnic compound for aromatic hydrocarbon Turn-VI : Preparation of derivative for aldehyde group. September to November, 2014 Turn-VII : Preparation of derivative for ketone group. Turn-VIII : prepration of derivative for carbohydrate group. Turn-IX : prepration of derivative for aromatic hydrocarbon Turn-X : To analyse the unknown organic compound and prepare its derivative. Turn-XI : To analyse the given unknown organic compound and prepare Its derivative. Turn-XII : To analyse the given unknown organic compound and prepare its derivative.
4 Schedule of organic chemistry practical B.Sc(Bio-tech) Sem-II January to Febrary, 2015 Turn I : To analyse the given mixture by physical examination, dry heating test, charcoal cavity and cobalt nitrate test. Turn II : To analyse the given mixture by flame test and Borax Bead test. Turn III : To analyse the given mixture by dilh 2 SO 4 test conc H 2 SO 4 independent acid radcial. Turn IV : To analyse the given mixture for acid radcial by confirmatory test. Turn V : To analyse the given mixture for basic radicals of group 0 And 1. Turn VI : To analyse the given mixture for basic radicals of group 2. March-April 2015 Turn VII : To analyse the given mixture for basic radicals of group 3. Turn VIII : To analyse the given mixture for basic radicals of group 4. Turn IX : To analyse the given mixture for basic radicals of group 5. Turn X : To analyse the given mixture for basic radicals of group 6. Turn XI : To analyse the given mixture for acid radical and basic radicals. Turn XII : To analyse the given mixture for acid radical and basic radicals.
5 Schedule of organic chemistry practical B.Sc(Bio-tech) Sem-II January to Febrary, 2015 Turn-I :To analyse the given organic compound by ignition test and : solubility test. Turn-II : Preparation of L.E. and detection of special element (N,S or Halogen) Turn-III :To analyse the given organic compound for carboxylic acid group. Turn-IV :To analyse the given organic compound for phenolic group. Turn-V Turn-VI :To analyse the given organic compound for amine group. :To analyse the given organic compound for amide group. March to April 2015 Turn-VII : Preparation of derivative for carboxylic acid group. Turn-VIII : Preparation of derivative for phenolic group. Turn-IX : Preparation of derivative for amine group. Turn-X : Preparation of derivative for amide group. Turn-XI : To analyse the unknown organic compound and prepare its derivative. Turn-XII : To analyse the given unknown organic compound and prepare Its derivative.
6 Schedule of Physical Chemistry Practical BSC. (Biotechnology) Sem III July to August 2014 Turn 1:- Determine the surface tension of a given liquid by drop weight method using stalgmometer : Acetone, Ethanol, Propanol, Butanol. Turn 2:- Determine the surface tension of given liquid by drop number method. :- Acetone, Ethanol, Propanol, Butanol. Turn 3:- To determine the viscosity of liquid using viscometer. :- Acetone, Ethanol, Propanol, Butanol. Turn 4:- To verify Lambert-Beers law for solution of K 2 Cr 2 O 7 in H 2 O. :-K 2 Cr 2 O 7. Turn 5:- To verify Lambert-Beers Law for solution of COCl 2.5H 2 O in H 2 O :- COCl 2.5H 2 O Turn 6:- Determine ph of Buffer solution and strength of HCl by titrating it against standard solution of NaOH. :- NaOH, Buffer solution, HCl September to November 2014 Turn7:- determine the normality and strength of acetic acid with ph meter and Determine the ionization constant of a weak acid ie.. CH 3 COOH :- CH 3 COOH. Turn8:- Study of distribution law of Benzoic Acid between Benzene and water. :- Benzoic acid, Benzene. Turn 9 :- Study of distribution law by iodine distribution between water and CCl 4. standard solution NA 2 S 2 o 3. :- CCl 4, Na 2 S 2 O 3, Iodine solution Turn 10:- Determine composition of HCL and CH 3 COOH in the given solution ph metrically. :- HCl, CH 3 COOH Turn 11:- Determine the surface tension of given liquid by drop number method. :- Acetone, Ethanol, Propanol, Butanol. Turn 12:- To determine the viscosity of given liquid by viscometer. :- Acetone, Ethanol, Propanol, butanol
7 Schedule of physical chemistry practical B.Sc(Bio-tech) Sem-IV January to Febrary, 2015 Turn 1 :To determine refractive index of given liquid and calculate their specific and molar refraction. : Acetone,distilled water. Turn 2 : Determine the %age composition of an unknown mixture of benzene and acetone with the help of abb s refractometer. : Acetone,distilled water benzene. Turn 3 : Determine the %age composition of an optically active solution. : Sugar solution. Turn 4 : To determine the enthalpy of neutralization of a strong acid(hcl) and a strong base calorimetrically. : HCl, NaoH. Turn 5 : To Determine the enthalpy of neutralization of weak acid with a strong base calorimetrically. : CH 3 COOH,NaoH Turn 6 : Determination oh Heat of solution of KCl,NH 4 Cl,KNO 3. : KCl,NH 4 Cl,KNO 3. March to April, 2015 Turn 7 : To determine the specific conductance and equivalent conductance of a given electrolyte at different dilutions. : HCl Solution. Turn 8 : To Determine the strength of given solution of H 2 o by titration against NaoH. : Oxalic acid, N/10 HCl solution. Turn 9 : To determine the strength of acetic acid solution by titrating It against N/2 standard solution by NaoH. : oxalic acid,acetic acid,naoh Turn 10: Precipatation titration of Na 2 So 4 vs. Bacl 2. : Na 2 So 4, Bacl 2. Turn 11: Determination of adsorption isotherm of oxalic acid on charcoal. : oxalic acid. Turn 12: Determination of heat of solution of KCL,NH 4 Cl,KNO 3. : KCL,NH 4 Cl,KNO 3.
8 Turn 1 Turn 2 Turn 3 Turn4 Turn5 Cl2 and that of Schedule of Chemistry Practical s B.Sc(Bio Tech ) Sem- V July to August 2014 : Record its IR spectra diethylether, ethyl acetate and butanone. : spectra diethylether, ethyl acetate and butanone : Convert cyclohexanone to cyclohexanol and hydrazine of cyclohexanone. Compare UV vis and IR spectra of product with that of starting material. : cyclohexanol. : Preparation of [Fe(PY)4(NCS)2] and its IR characteristics. : Pyridine, ammonium thiocyanate. : Take commercial sample of methed arrange and record it UV-vis and fluarescene spectra under neutral, acidic and basic medium and make comparison. : Methylarrange. : Synthesis and electronic spectral studies of d-d bands of [Ni(NH3)6] [Ni(en)3] Cl2 Complete a compression of their electronic spectra with [Ni(H2o)6]Cl2 for the conclusion of100q valve. : [Ni(NH3)6] Cl2, [Ni(en)3] Cl2. September to November 2014 Turn 6 : To Verify Beer-Lambert Low For KMnO4/K2Cr2O7 and determine concentration of given KMnO4/ K2Cr2O7 Solution. : KMnO4, K2Cr2O7. Turn 7 : Record its IR spectra diethylether, ethyl acetate and butanone. Turn 8 : spectra diethylether, ethyl acetate and butanone : Convert cyclohexanone to cyclohexanol and hydrazine of cyclohexanone. Compare UV vis and IR spectra of product with that of starting material. : cyclohexanol. Turn 9 : Preparation of [Fe(PY)4(NCS)2] and its IR characteristics.
9 Turn10 Turn11 Turn12 Cl2 and with that of : Pyridine, ammonium thiocyanate. : Take commercial sample of methed arrange and record it UV-vis and fluarescene spectra under neutral, acidic and basic medium and make comparison. : Methylorange. : Take To verify beer-lambert law for KMnO4/K2Cr2O7 and determine concentration of given KMnO4/K2Cr2O7 Solution. : KMnO4, K2Cr2O7. : Synthesis and electronic spectral studies of d-d bands of [Ni(NH3)6] [Ni(en3)6] Cl2 Complete a compression of their electronic spectra [Ni(H2o)6]Cl2 for the conclusion of100q valve. : [Ni(NH3)6] Cl2, [Ni(en)3] Cl2
10 Schedule of chemistry practical B.Sc(Bio-tech) Sem-VI January to Febrary, 2015 Turn 1 : Recard the H NMRspectra of ethylacctate and ethylacetoacetate (In cdcl 3 or ccl 4 )and shows the presence of tantomeric structure. : Cdcl 3, ethylacctate,ethylacetoacetate Turn 2 : Prepration of Benzilic acid from Benzaldehyde (Green- Chemistry experiment) : Benzaldehyde Turn 3 : Seperate the components of spinach using column chromatography. : Spinach leaves,alumina Turn 4 : Prepare p-nitoacetanilide and make comparison of H NMR spectra data of aniline acetanilide (starting material) and p- nitroacetanilide (poduct). : acetanilide Turn 5 : Compare IR and HNMR spectra of aspirin : Aspirin,cdcl 3 Aim : Compare IR and H NMR spectra of salicyclic acid : Salicyclic acid,cdcl 3 March-April 2015 Turn 7 : Preparation of Benzilic acid from Benzaldehyde. : Benzaldehyde. Turn 8 : Separate the components of spinach leaves using column chromatography. : spinach leaves,alumina Turn 9 : Record the H NMR spectra of ethylacetate and ethyacctocetate (in cdcl 3 or ccl 4 )and show the presence of tantomeric structure.
11 : cdcl3, ethylacetate or ethyacctocetate. Turn 10 : Compare the IR and H NMR spectra of aspirin. : Aspirin Turn 11 : Compare the IR and H NMR spectra of solicyclic acid. : salicyclic acid, cdcl 3 Turn 12 : Prepare p-nitoactavlide and make comparison of H NMR spectra Data of aniline,acetanilide (starting material) and p- nitroacetaanilide). : acetanilide
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