Plasma Source Mass Spectrometry
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1 Plasma Source Mass Spectrometry Developments and Applications Edited by Grenville Holland Department of Geological Sciences, University of Durham, Durham, UK Scott D. Tanner PE-Sciex, Concord, Ontario, Canada ^&- THE ROYAL ggf SOCIETY OF ^g>, CHEMISTRY ijgjgjgg^ Information ^?J5^ Services
2 Contents Generation and transport of ions: ICP-MS from Single drops and microsecond time scales to practical measurements 1 /. W. Olesik, J. A. Kinzer andm. P. Dziewatkoski Ion optics for ICP-MS: modeling, intuition or blind luck 13 Scott D. Tanner Interface studies in the ICP-MS spectrometer 28 P. Turner, T. Merren, J. Speakman and C. Haines A Computer Simulation of the current distribution in an electron multiplier 35 J. H. Batey andm. Liezers The effect of high uranium matrix concentration on plasmascreen torch: an evaluation of the improvement of iron analysis in actinide Compounds 44 F. Pilon, D. Koller anda. Raith A routine approach to the multielement analysis of small sample volumes by ICP Mass Spectrometry 51 R. J. Thomas, T. J. Gluodenis Jr., S. A. Beres ande. R. Denoyer Simultaneous reduction of polyatomic ion interferences in quadrupole ICP-MS using ultrasonic nebulization and directed optimization 61 J. L. M. de Boer Early results for the direct analysis of concentrated acids by ICP-MS using a desolvated micro-concentric nebulizer 70 D. R. Wiederin, P. Krause, R. Hutton, B. Grote and C. W. McLeod Spectral interpretation and survey analysis in ICP-MS 77 E. H. van Veen andm. T. C. deloos-vollebregt A study of random and systematic errors for the determination of molybdenum by inductively coupled plasma source mass spectrometry using on-line isotope dilution analysis 85 /. M. Marchante-Gayön, J. I. Garcia Alonso anda. Sanz-Medel
3 viii Plasma Source Mass Spectrometry: Developments and Applications Quality control in the multi-element analysis of foods using ICP-MS 95 M. J. Baxter, H. M. Crews, P. Robb andp. R. Strutt Coupling of GC with ICP-MS for trace metal speciation 109 T. De Smaele, L. Moens andr. Dams On-line Separation and determination of bromate in waters using flow injection inductively coupled plasma mass spectrometry 124 A. R. Elwaer, C. W. McLeod, K. C. Thompson and D. Wiederin Speciation of protein-bound cadmium in biological materials by size-exclusion and reversed-phase HPLC with ICP-MS detection 131 /. Szpunar, H. Chassaigne, O. F. X. Donard, J. Bettmer and R. Lobinski Rapid on-line Separation and determination of arsenic (III) and (V) in waters by inductively coupled plasma mass spectrometry 145 A. G. Cox, C. W. McLeod, M. Nishikawa andd. Wiederin Determination of As, Hg and Se in coals by means of FI-HG- ICP-MS. Comparison with other techniques 152 M. Bettinelli, S. Spezia, U. Baroni and G. Bizzari Microcolumn field sampling for determination and speciation of organo-tin in seawater 159 G. D. Woods, C. W. McLeod, K. Kawabata, S. Nagaoka, H. Okochi anda. Otsuki Microcolumn preconcentration and flow injection ICP-mass spectrometry for determination of plutonium in seawater: initial studies 166 A. E. Eroglu, C. W. McLeod, K. S. Leonard andd. McCubbin Gold determination in human blood serum by flow injection inductively coupled plasma mass spectrometry 175 G. Doner, C. W. McLeod andd. Bax Determination of Butyltin Compounds by means of hydride generation-cold trapping-gas chromatography coupled to ICP-MS detection 182 E. Segovia Garcia, J. I. Garcia Alonso anda. Sanz-Medel
4 Contents Flow injection sorbent extraction preconcentration for ICP mass spectrometry with ultrasonic nebulisation and membrane desolvation 192 R. Ma, C. W. McLeod and K. C. Thompson Uranium in urine and serum of "normal" populations: a FIAS- ICP-MS study 202 A. Lorber, L. Halicz, Z. Karpas, E. Elish, J. Roiz andr. Marko Multielement characterisation of lichens and vegetable materials by ICP-MS 211 M. Bettinelli, S. Spezia, U. Baroni and G. Bizzari Plant material decomposition methods and determination of selected elements by ICP-MS Elan E. Curdovä, J. Szdkovd, R. Koplik and M. Suchänek Glow discharge optical emission spectrometry: use of plasma sources in characterisation of electronic materials and devices 231 /. M. Dharmadasa, M. Ives, C. Breen, G. Hill, C. C. Button, J. S. Roberts and M. Hopkinson Contamination of drinking water caused by mixer taps 240 P. Fecher, A. Nagengast and R.Sperk Determination of rare earth elements in Antarctic lakes and streams of varying ionic strengths 253 E. Y. Graham, L. A. Ramsey, W. B. Lyons andk. A. Welch Assessment of the potential risks of landfills by determination of trace metals in groundwater by ICP-MS 263 A. Ulrich, H.-R. Zweifel and A. C. Johnson Simultanous quantification of et- and ß-emitting radionuclides in concrete samples by inductively coupled plasma mass spectrometry (ICP-MS) 271 M. Rupprecht and T. Probst Application of ICP-MS to steel samples 284 K. Pettersen and I. Gustavsson lx
5 x Plasma Source Mass Spectrometry: Developments and Applications Determination of arsenic in solid extracts using high resolution inductively coupled plasma mass spectrometry (HR-ICP-MS) 291 T. Prohaska, C. Latkoczy, G. Stingeder and W. W. Wenzel New instrumental developments and analytical applications in ICP-MS 298 N. Jakubowski andd. Stuewer Author Index 313 Subject Index 316 Reference Index 324
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