2D Simulations and Electro-Thermal Analysis of Micro-Heater Designs Using COMSOL TM for Gas Sensor Applications

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Presented at the COMSOL Conference 2010 India 2D Simulations and Electro-Thermal Analysis of Micro-Heater Designs Using COMSOL TM for Gas Sensor Applications Presented By Velmathi.G, Ramshanker.N and Mohan.S Department of Instrumentation and Applied Physics, Indian Institute of Science, Bangalore velmathi@isu.iisc.ernet.in

Integrated micro structure of a Gas sensor

Gas sensors are the devices which hdetermine the information about the gas present and its concentration in an ambient gas atmosphere. Miniaturized Second gas sensors level with a low power consumption for the detection ec of Third various level gases such as CO,LPG and H 2 is svey very essential for a wide range of applications. The Micro-heater is the main component tin gas sensors to make the sensing layer more sensitive and selective. Which is also a most power consuming part in gas sensors. Hence perfect design and fabrication of Micro-heater is an important aspect.

Micro-heaters in gas sensors are basically resistive beams which can attain a temperature of 300 o C - 400 o C due to joule heating, when sufficient voltage is applied across them. The design Second of micro-heaters level is optimized for low power consumption low thermal mass Better temperature uniformity across the device enhanced thermal isolation from the surroundings

Micro-Heater patterns The Plane plate with central square hole Double spiral Honeycomb S-shape Fan shape Meander

Electro Thermal Mathematical modeling of microheater In Joule heating, the temperature increases due to the resistive heating from the electric current. The electric potential V is the solution variable in the Conductive Second Media level DC application mode. The generated Third resistive level heat Q is proportional to the square of the magnitude Fourth of the level electric current density J. Current density, in»fifth turn, level is proportional to the electric field, which equals the negative of the gradient of the potential V In our Simulations we assume the temperature and potential gradients in the z-direction (perpendicular to the heater plane) are small in comparison to the gradients in x- y plane. There by reducing the problems to two dimensions. This is a reasonable assumption given the relative dimensions of the structure; the thickness being much smaller than the length or width.

Over a range of Third temperatures level the electric conductivity σ is a function of temperature T according Fourth to: level where σ 0 is the conductivity at the reference temperature T 0. α is the temperature coefficient of resistivity, which describes how the resistivity varies with temperature. A typical value for platinum copper is 0.00385 per o C

The coefficient of proportionality is the electric resistivity ρ = 1/σ, which is also the reciprocal of the temperature- dependent Click electric to edit conductivity Master text σ = σ(t). styles Combining these facts gives Second the fully level coupled relation. The equations Fourth have been levelsolved under Dirichlet, Neumann, and mixed boundary»fifth conditions level numerically using the Finite Element Method (FEM) when the Electro-Thermal module dl is selected din COMSOL TM.

Meshing optimization The optimized meshing for the simulation is determined Third by level performing an independent grid study Fourth to minimize level the modeling error. When the change in the solution between subsequent stages of meshing refinement is considered to be negligible, g the lower but still sufficient, mesh resolution is kept.

Material properties of layers used in the MEMS micro-heater structure Material (Si) (Si x N y ) (SiO 2 ) (Pt) Thermal Conductivity (W/mK) 157 22 14 1.4 73 Young s Modulus (GPa) 190 290 73 170 Poisson s s Ratio 017 0.17 024 0.24 020 0.20 039 0.39 Thermal expansion Fourth (1/K) level2.33e-6 2.33e-6 0.55e-6 8.9e-6 Density (kg/m 3 ) 2.32e3 3.1e3 2.2e3 2.145e4 Heat Capacity (J/kg o C) 700 600-800 730 130

Square plate with center hole

Double Spiral Shape

Honey Comb structure

S-Shape structure

Fan shape

Meander structure

FABRICATION PROCESS STEPS (1) Thermally grown SiO 2 on Si Substrate (2) Si 3 N 4 deposition on top side (3) Pt heater deposition (4) Si 3 N 4 deposition over Pt heater (5) contact pad open (6) back side window open (7) Backside etching using TMAH Photograph of Gold wire bonded, packed micro-heater

SL.N o Heater pattern Power consumption for 400 O CinmW 1. Double Spiral 9.56 2. Fan Third Shape level 15.94 3. S-Shape 17.50 4. Meander pattern 20.00 5. Honeycomb structure 6. Square with center hole 140.63 787.50

So taking (R= W i+1 / W i) as an important variable the double spiral pattern is designed within the area of 500µm X 500µm The pattern Click to is fabricated edit Master with text membrane styles at the back and tested for its heating profile SEM image of Fabricated Micro-heater Image of Fabricated Micro-heater in Surface Profilometer TMAH etched Membrane

Gold Wire Bonded Heater

Thermal Imaging The ThermaCAM P65 delivers unmatched temperature measurement accuracy. A thermal sensitivity of 0.08 C results in clear noise-free images (320 x 240 pixels). A low thermal sensitivity not only offers you the possibility to see the smallest of temperature changes. It also means you get crisp, very detailed high-resolution images which cannot be obtained by less sensitive cameras. How it Works? The FLIR P65 uses an advanced, highly-sensitive detector for non-contact scanning across wide areas. Second Camera level controls and software make it easy to quickly scan for emissivity and object Third temperature level differencesdifferences that can signal trouble in building envelopes and infrastructure FLIR thermal image @ 0.06V applied voltage. ThermaCAM P65

Practical Data Thermal analysis of Micro-heater Resistance-temperature dependence for the determination of temperature (RT) R sensor =Ro(1+α T) Where T = T sensor T amb Ro is the sensor Third resistance level in ohms at T = T amb, α is Temperature coefficient of resistance (TCR) in o C-1 voltage temperature 0.020074 50.66 0.029974 101.32 0.040104 172.24 0.04976 253.29 0.060008 377.12 0.070045 506.58 FLIR thermal image @ 0.06V applied voltage. 0.079998 628.16 COMSOL simulated Result

Click to edit Acknowledgements Master text styles The authors are thankful to NPMASS for funding this activity Third and level Ministry of Communication and Information Technology for providing the funds for setting up Center»Fifth of level Excellence in Nanoelectronics facility at IISc.