ANNUAL REPORT ANALYSES OF OFFICIAL FERTILIZER SAMPLES

Transcription

1 AGRICULTURAL EXPERIMENT STATION UNIVERSITY OF KENTUCKY-COLLEGE OF AGRICULTURE REGULATORY BULLETIN No. 305 ANNUAL REPORT ANALYSES OF OFFICIAL FERTILIZER SAMPLES JULY 2007 JUNE 2008 D r e a m C h a l l e n g e S u c c e e d UNIVERSITY OF KENTUCKY COLLEGE OF AGRICULTURE An Equal Opportunity University AGRICULTURAL EXPERIMENT STATION DIVISION OF REGULATORY SERVICES LEXINGTON, KENTUCKY

2 DIVISION OF REGULATORY SERVICES KENTUCKY AGRICULTURAL EXPERIMENT STATION William O. Thom, Director D. L. Terry, Coordinator, Fertilizer Regulatory Program Henry Spencer, Auditor INSPECTION STAFF Steve McMurry Coordinator, Field Inspection Staff Mark Barrow Dewey Coffey John W. Flood Brad Johnston Noel Johnston David Mason Warren Pinkston Terry Prather Jesse Whitehouse LABORATORY STAFF Melton Bryant and Sharon Webb Coordinators, Chemical Laboratories Gary Coleman Wayne Ingram Keith Erny David Harover Ellen Perry Robert Kiser Garland McKee Paul Wilson Debra Sipe David Tompkins Lancao Zhang ADMINISTRATIVE STAFF Tony Benge, Computer Systems Manager III Kellye Gaither, Senior Systems Analyst Programmer This report was compiled and prepared by D. L. Terry with the assistance of the Inspection, Laboratory, and Administrative Staffs.

3 Table of Contents INTRODUCTION... 1 EXPLANATION OF TABLES... 1 INVESTIGATIONAL ALLOWANCES... 4 MONETARY PENALTIES MAXIMUM CHLORINE GUARANTEE FOR TOBACCO FERITLIZERS COMMERCIAL FERTILIZER VALUES FOR CALENDAR YEARS 2007 AND KENTUCKY OFFICIAL NPK SAMPLES FOR SUMMARY OF CERTAIN SAMPLE CHARACTERISTICS COMBINED BY FORM AND BY TYPE KENTUCKY OFFICIAL NPK SAMPLES FOR SUMMARY OF CERTAIN SAMPLE CHARACTERISTICS BY FORM AND BY TYPE TOTAL FERTILIZER SUMMARY- JULY 2007 JUNE TABLE 1. RESULTS OF TOTAL NITROGEN (N), AVAILABLE PHOSPHATE (P2o5) SOLUBLE POTASH (K2O), AND EXCESS CHLORINE (XS CL) ANALYSES OF OFFICIAL FERTILIZER SAMPLES TABLE 2. RESULTS OF THE ANALYSES OF CERTAIN OFFICIAL SAMPLES FOR SECONDARY AND MINOR ELEMENTS, WATER INSOLUBLE NITROGEN (WIN), COATED SLOW RELEASE ((CSRN) AND OCCLUDED SLOW RELEASE NITROGEN (OSRN) TABLE 3. COMPANIES REGISTERED or LISCENSED TO SELL IN KENTUCKY: as of June 30,

4 REGULATORTY BULLETIN INTRODUCTION This bulletin presents the results of the analysis of 2,798 official samples of commercial fertilizer taken during the period of July 1, 2007 through June 30, 2008 by the field inspection staff. The samples represented approximately 60,000 tons of fertilizer out of the approximately 846,000 tons sold during this period. The Laboratory made 2,464 nitrogen, 2,080 phosphorus, 2,249 potassium and 1,396 chloride, secondary and minor element and certain other analyses on these samples. The results of N, P 2 O 5, K 2 O, and maximum chloride analyses of samples of mixed fertilizers and fertilizer materials and certain statistical analyses are in Table 1. Table 2 contains the results of secondary and minor element and certain other analyses and Table 3 is a listing of companies or licensees registered or licensed to sell fertilizer in Kentucky as of June 30, Table 1. EXPLANATION OF TABLES Sample Data Every official fertilizer sample taken during the year is listed in this table alphabetically by registrant and by GRADE within a registrant s listing. GRADE: The registrant s whole number guarantee is expressed as the grade: N - P 2 O 5 - K 2 O. For custom mixes with fractional guarantees this represents the whole number part of the guarantee. NUM: A Laboratory number (NUM) is assigned each sample and is the only code used by the laboratory to identify a sample. + : A (+) beside a NUM indicates that the sample was analyzed for one or more of the following tests: secondary or minor element, water insoluble nitrogen (win), coated slow release (CSRN), or occluded slow release nitrogen (OSRN) and the results are in Table 2 N, P 2 O 5, K 2 O: These are the results of the chemical analyses of each sample for total Nitrogen (N), available phosphate (P 2 O 5 ) and soluble potash (K 2 O). XS CL: Each sample with a maximum chlorine guarantee was analyzed for chloride. If it exceeded the guarantee (XS CL), an asterisk (*) appears in this column.

5 2 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY RV: The relative value (RV) of a NPK fertilizer is a comparison of its found value with its guaranteed value. An example calculation follows: A fertilizer is guaranteed to contain 6% N, 24% P 2 O 5, and 24% K 2 O. A Guaranteed Value and a Found Value are computed for the fertilizer by using the following example commercial values: N - $4.00, P 2 O 5 - $3.80, and K 2 O (Non-Tobacco) - $1.60. The Guaranteed Value is calculated as follows: Element Guaranteed,% Unit Value Value N 6.0 X 4.00 = P 2 O X 3.80 = K 2 O 24.0 X 1.60 = Total Guaranteed Value The same procedure is followed for the Found Value, thus Element Found, % Unit Value Value N 5.9 X 4.00 = P 2 O X 3.80 = K 2 O 23.9 X 1.60 = Total Found Value The relative value (RV) is then computed by dividing the Found Value by the Guaranteed Value and multiplying by 100. RV = (153.42/153.6) X 100 = 99.9% The RV is rounded to the nearest whole percent before being printed in the bulletin. * : Those results marked with an asterisk (*) are deficient under the criteria stated in the investigational allowances section of this bulletin. Occasionally an analysis may be found that appears to be inconsistent in its marking. For example, two samples that are guaranteed 10% P 2 O 5 may both be shown as containing 9.1%. One of these may have an asterisk (*) and the other may not. There are two situations which may cause this apparent discrepancy:

6 REGULATORTY BULLETIN (1) The investigational allowances are applied by computer to the laboratory analyses before the found analyses are rounded to the nearest tenth of a percent and printed. In the above example, if the laboratory found 9.09% for one sample and 9.13% for the other, only the first one would be marked (*) as deficient. (2) The grade as printed is the largest whole number in the guarantee of each ingredient, that is, any decimal is dropped before the table is printed. For example, a custom-mixed lot of fertilizer may be guaranteed 11.9% P 2 O 5 and 11.2% K 2 O. The grade would be printed However, the investigational allowances are applied on the basis of the 11.9% and 11.2% guarantees. If this custom mixed fertilizer analyzed 10.9% P 2 O 5 and 10.9% K 2 O, only the 10.9% P 2 O 5 would be marked (*) because it is below the 11.9% guarantee by more than the investigational allowance. TYPE: The codes for type are: BLEND - A fertilizer made by physically mixing two or more fertilizer materials or non-fertilizer ingredients. It does not include custom mixes. MNFR - An ammoniated-granulated fertilizer made by chemically mixing and/or reacting fertilizer materials. MAT - A fertilizer material such as muriate of potash. CM - A custom-mixed blended fertilizer. FORM: The column headed FORM indicates whether the fertilizer was in bags, bulk, or in Liquid form when sampled. Statistical Analyses -- In the body of the table there is a brief statistical analysis: (1) When one grade of a company was sampled 5 or more times or (2) when 10 or more total samples were obtained from a company. The terms used are self explanatory; however, the following additional explanation is considered helpful. CV is the coefficient of variation found by dividing the standard deviation by the average analysis and multiplying by 100. Deficiency Rate is calculated by dividing the number of samples with one or more deficiencies in N, P 2 O 5, K 2 O or RV by the total number of samples and multiplying by 100. Tables 2 and 3 - Self Explanatory

7 4 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY INVESTIGATIONAL ALLOWANCES Primary Nutrients A fertilizer shall be deemed deficient if the analysis of an official sample for any primary nutrient is below the guarantee by an amount exceeding the values in the following schedule. Guaranteed % Total Nitrogen (N) % Available Phosphate (P 2 O 5 ) % Soluble Potash (K 2 O) % 05 or less or more For guarantees not listed, calculate the appropriate value by interpolation.

8 REGULATORTY BULLETIN For these investigational allowances to be applicable, the recommended AOAC International procedures for obtaining, preparing, and analyzing samples must be used. These are described in the current edition of Methods of Analysis published by the, AOAC International. 481 North Frederick Avenue, Suite 500, Gaithersburg, MD In evaluating replicate data, Table 19, page 935, Journal of the Association of Official Analytical Chemists, Volume 49, No. 5, October, 1966, should be followed. Secondary and micro nutrients shall be deemed deficient if the analysis of an official sample for any of these elements is below the guarantee by an amount exceeding the values in the following schedule. Secondary and Micro Nutrients Element Calcium Magnesium Sulfur Boron Molybdenum Chlorine Copper Iron Manganese Sodium Zinc Investigation Allowances 0.2 unit + 5% of guarantee 0.2 unit + 5% of guarantee 0.2 unit + 5% of guarantee unit + 15% of guarantee unit + 30% of guarantee unit + 10% of guarantee unit + 10% of guarantee unit + 10% of guarantee unit + 10% of guarantee unit + 10% of guarantee unit + 10% of guarantee The maximum allowance when calculated in accordance to the above shall be one (1) percentage point. Relative Value (RV) and Maximum Chlorine (XSCL) The investigational allowance for relative value (RV) is three (3) percentage points. The investigational allowance for maximum chlorine is 0.5 percentage point.

9 6 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY MONETARY PENALTIES Monetary penalties for deficiencies in any test are assessed according to the following schedule. PRIMARY NUTRIENTS AND RV Number of Investigational Allowance Penalty Schedule Below Guarantee < 2 Equal to the Monetary Value of the Deficiency > 2 < 3 Two (2) Times the Monetary Value of the Deficiency > 3 Three (3) Times the Monetary Value of the Deficiency If the relative value (RV) is greater than or equal to 97%, then the penalties calculated from the above schedule may be reduced according to the following schedule: Number of Investigational Allowances Below Guarantee No more than one (1) deficiency that is less than or equal to two (2) investigational allowances No more than one (1) deficiency that is greater than two (2) but less than three (3) investigational allowances Two (2) deficiencies that are less than three (3) investigational allowances; or, no more than one (1) deficiency that is equal to or greater than three (3) but less than four (4) investigational allowances Penalty Adjustment Penalty adjusted to zero Value of Overages may adjust up to 100% of the Value of the Deficiencies Value of Overages may adjust up to 75% of the Value of the Deficiencies When a fertilizer is subject to a penalty from both a primary nutrient deficiency and a relative value deficiency, only the larger penalty shall apply; however, in no case shall the penalty exceed the total value of the fertilizer.

10 REGULATORTY BULLETIN Penalties for deficiencies in secondary and minor elements and for excess chlorine in tobacco fertilizer shall be calculated from the following schedules. SECONDARY AND MINOR ELEMENTS Number of Investigational Allowances Below Guarantee Penalty Schedule < 2 Equal to the Monetary Value of the Deficiency > 2 Two (2) Times the Monetary Value of the Deficiency EXCESS CHLORINE IN TOBACCO FERTILIZERS Number of Investigational Allowances Above Maximum Chlorine Guarantee Penalty Schedule < 2 Equal to the difference in the Soluble Potash for Tobacco Unit Value and the Non-Tobacco Soluble Potash Unit Value. > 2 Two Times the Difference in the Soluble Potash for Tobacco Unit Value and the non-tobacco Soluble Potash Unit Value. Any penalty assessed for a deficiency in N, P 2 O 5, K 2 O, or RV shall be added to any penalty assessed for a deficiency in the secondary and minor elements or excess in chlorine and the total shall be paid by the registrant to the consumer of the lot of fertilizer represented by the sample within three months after the date of notice from the Director, receipts taken therefore and promptly forwarded to the Director. If said consumer cannot be found, the amount of the penalty payments shall be paid to the Kentucky Agricultural Experiment Station within three months after the date of the notice from the Director to the registrant and set aside (1) for purchase of equipment for the sampling, handling, analyzing and reporting of results of analyses of official samples and (2) for the education of the Kentucky fertilizer industry on the newest methods in manufacturing blended fertilizers. If the lot of fertilizer is on hand at a retail location the penalty payments assessed under this section shall be used to reduce the retail price of the fertilizer if it is to be relabeled and sold. In no case shall the total penalties assessed exceed the retail value of the fertilizer.

11 8 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY MAXIMUM CHLORINE GUARANTEE FOR TOBACCO FERTILIZERS All fertilizers, except bagged, sold for or represented for use on field crop tobacco shall, in addition to the other guarantees specified by 12 KAR Chapter 4, state a maximum chlorine guarantee not to exceed 50 lb. per acre chlorine (equivalent to 100 lb. of muriate of potash per acre) in the following format: Chlorine (Cl) Maximum 50 lb./acre The maximum chlorine guarantee shall be: Placed below the Guaranteed Analysis as required by 12 KAR 4:090 and prominently and conspicuously displayed on the invoice or shipping ticket that accompanies bulk sales. The invoice or shipping ticket shall state the rate of application expressed in lb./acre of the blended fertilizer. The provisions of this administrative regulation shall not apply to fertilizers for use on plant beds.

12 REGULATORTY BULLETIN COMMERCIAL FERTILIZER VALUES FOR CALENDAR YEARS 2007 AND 2008 Under provision of Chapter of the Kentucky Law of 1995 the following unit values were used in assessing penalties for deficient fertilizer. Nutrient Dollars/Unit (20 lbs.) Total Nitrogen (N) $8.39 $11.81 Avail. Phosphate (P 2 O 5 ) $8.61 $15.66 Soluble Potash (K 2 O) Tobacco (Low CL) $7.50 $9.49 Non-Tobacco $4.27 $6.93 Calcium (Ca) $6.01 $11.50 Magnesium $11.52 $13.19 Sulfur (S) $5.39 $5.51 Boron (B) $66.25 $67.10 Copper (Cu) $ $ Iron (Fe) $7.63 $12.45 Manganese (Mn) $22.90 $20.68 Molybdenum (Mo) $18.05 $18.05 Zinc (Zn) $31.52 $35.65 These values are statewide averages taken from a survey conducted in December of the preceding year. No attempt was made to distinguish between bag, bulk or liquid; or, blends and manufactured products.

13 10 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY SUMMARY Kentucky Official NPK Samples for Summary of Certain Sample Characteristics Combined By Form and By Type Samples Samples Tons Tons Sampled Sample RV FORM TYPE Number % of Total Sampled % of Total Def. Rate, % MEAN BAG BLENDED GRADE , BAG MANUFACTURED BAG MATERIAL BULK BLENDED GRADE BULK MANUFACTURED BULK MATERIAL , BULK CUSTOM MIX 1, , LIQUID BLENDED GRADE LIQUID MANUFACTURED LIQUID MATERIAL , LIQUID CUSTOM MIX SUMMARY 2, , Kentucky Official NPK Samples for Summary of Certain Sample Characteristics By Form and By Type No. N Tests N Test P Tests P Test K Tests K Test Sample RV Ave Lot Size Total Tons FORM TYPE Samples Sum Def. Rate Sum Def. Rate Sum Def. Rate Def. Rate,% MEAN Per Smp Sampled BAG ,526 BULK. 1,949 1, , , ,774 LIQUID BLENDED GRADE ,796 MANUFACTURED ,001 MATERIAL ,848 CUSTOM MIX 1,297 1, , , ,137 NPK SAMPLES ONLY 2,759 2, , , ,782 ALL SAMPLES 2,798 2, , , ,985

14 REGULATORTY BULLETIN Monday, December 08, 2008 TOTAL FERTILIZER SUMMARY DIVISION OF REGULATORY SERVICES UNIVERSITY OF KENTUCKY From July, 2007 To June, 2008 CONTAINER USE TOTAL BAG BULK LIQUID FARM NON-FARM MULTI-NUTRIENT 248, , , , , ,312.5 NITROGEN 374, , , , , PHOSPHATE 3, , , POTASH 180, , , , ORGANICS 20, , , , , SEC/MICRO 2, , , MISCELLANEOUS 19, , , , , TOTAL 848, , , , , ,359.24

15 12 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY TABLE 1. Results Of Total Nitrogen (N), Available Phosphate Acid (P2O5), Soluble Potash (K2O), And Excess Chloride (XS CL) Analyses Of Official Fertilizer Samples. Deficiencies in N,P205, K20, and RV and excessive chloride are noted with an asterisk(*). A(+) by the sample number indicates that there is an entry for this sample in Table 2. AG DISTRIBUTORS, INC. NASHVILLE TN Mat Bulk Mat Bulk Mat Bulk Blend Bag Blend Bag * Blend Bag Mat Bulk Blend Bag Blend Bag Mat Bulk Mat Bulk Blend Bag Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 5.88 % AG/GRO FERTILIZER CO. (HILL ST.) WINCHESTER KY Mat Bulk Blend Bag Blend Bag * Blend Bag * 8.92 * 89 * Blend Bag * * Blend Bag Blend Bag * Blend Bag Blend Bag Blend Bag Blend Bulk Statistical Analysis for Grade : Number of Samples This Grade : 5 Average Analysis : CV, % Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag

16 REGULATORY BULLETIN AG/GRO FERTILIZER CO. (HILL ST.) WINCHESTER KY Blend Bag * Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag * * 96 * Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag * * Blend Bulk Blend Bag Blend Bag Blend Bag Statistical Analysis for Grade : Number of Samples This Grade : 18 Average Analysis : CV, % Blend Bag Blend Bag Blend Bag * * * Blend Bag Blend Bag Statistical Analysis for Grade : Number of Samples This Grade : 5 Average Analysis : CV, % Blend Bag Blend Bag Blend Bag Blend Bag * Blend Bag Blend Bag CM Bulk Blend Bag Mat Bulk * Blend Bag Blend Bulk Blend Bag Blend Bag Blend Bag

17 14 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY AG/GRO FERTILIZER CO. (HILL ST.) WINCHESTER KY Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Statistical Analysis for Grade : Number of Samples This Grade : 13 Average Analysis : CV, % Blend Bag Blend Bag Mat Bag Mat Bag Mat Bag Mat Bag Mat Bag Mat Bag Statistical Analysis for Grade : Number of Samples This Grade : 6 Average Analysis : CV, % Mat Bag Mat Bag Mat Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % AG/GRO FERTILIZER CO. (PEND. ST.) WINCHESTER KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk

18 REGULATORY BULLETIN AG/GRO FERTILIZER CO. (PEND. ST.) WINCHESTER KY ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % AGRI-CHEM, INC. (HERN) HERNDON KY CM Bulk CM Bulk AGRI-CHEM, INC. (HOPK) HOPKINSVILLE KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk AGRI-CHEM, INC. (PRIN) PRINCETON KY CM Bulk CM Bulk AGRI-CHEM, INC. (TRENT) TRENTON KY CM Bulk CM Bulk * CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % AGRIENERGY RESOURCES PRINCETON IL Blend Liq Blend Liq Blend Liq Blend Liq Blend Liq

19 16 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY AGRIENERGY RESOURCES PRINCETON IL Blend Liq Blend Liq AGRILIANCE, LLC/WINFIELD SOLUTIONS ST. PAUL MN Blend Bag * * Blend Bag * * Blend Bag Blend Bag * * 93 * Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % AGRIPORT TERMINAL EDDYVILLE KY Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Statistical Analysis for Grade : Number of Samples This Grade : 7 Average Analysis : CV, % * 106 CM Bulk CM Bulk Mat Bulk Mat Bulk CM Bulk CM Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk

20 REGULATORY BULLETIN AGRIPORT TERMINAL EDDYVILLE KY Statistical Analysis for Grade : Number of Samples This Grade : 9 Average Analysis : CV, % CM Bulk CM Bulk Mat Liq Mat Liq Mat Liq Mat Liq Mat Liq Mat Liq Statistical Analysis for Grade : Number of Samples This Grade : 6 Average Analysis : CV, % ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 3.23 % AGRIUM ADVANCED TECHNOLOGIES US INC REESE MI Mnfr Bulk Mat Bag Mat Bag Mnfr Bag Mnfr Bag AGRIUM U.S. INC. (DENV) DENVER CO Mnfr Bulk Mnfr Bag Mnfr Bag Mnfr Bag Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk

21 18 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY AGRIUM U.S. INC. (DENV) DENVER CO Mat Bulk Mat Bulk Statistical Analysis for Grade : Number of Samples This Grade : 15 Average Analysis : CV, % ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % AGRO CULTURE LIQUID FERT. ST. JOHNS MI Blend Liq Blend Liq Blend Liq Blend Liq Blend Liq Blend Liq AGRO DISTRIBUTION, LLC HARDINSBURG KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Statistical Analysis for Grade : Number of Samples This Grade : 6 Average Analysis : CV, % ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % ALLEN COUNTY FARMERS SERVICE SCOTTSVILLE KY CM Bulk CM Bulk CM Bulk CM Bulk

22 REGULATORY BULLETIN ALLEN COUNTY FARMERS SERVICE SCOTTSVILLE KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % ALLEN COUNTY FEED & SEED, INC. SCOTTSVILLE KY CM Bulk CM Bulk * * CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % ALLENSVILLE CROP SVC. ALLENSVILLE KY CM Bulk * 106 CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % ANDERSON CO FARM SVC LAWRENCEBURG KY Mat Bulk Mat Bulk

23 20 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY ANDERSON CO FARM SVC LAWRENCEBURG KY Mat Bulk BALLARD COUNTY COOPERATIVE LA CENTER KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk BANDANA AG INC. BANDANA KY Mat Bulk Mat Bulk * CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Statistical Analysis for Grade : Number of Samples This Grade : 6 Average Analysis : CV, % * 100 CM Bulk Mat Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % BICKETT AGRI CTR. CENTRAL CITY KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk * 103 CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk

24 REGULATORY BULLETIN BICKETT AGRI CTR. CENTRAL CITY KY Statistical Analysis for Grade : Number of Samples This Grade : 7 Average Analysis : CV, % Mat Liq ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 9.09 % BLOOMFIELD FERTILIZED CHEM CO., INC BLOOMFIELD KY Mat Bulk * CM Bulk CM Bulk CM Bulk CM Bulk Mat Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Mat Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 7.69 % BLUEGRASS SEED/FERT INC. BARDSTOWN KY Mat Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Mat Bulk CM Bulk CM Bulk CM Bulk Mat Bulk

25 22 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY BLUEGRASS SEED/FERT INC. BARDSTOWN KY ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % BRYANT, OTIS & SON CANEYVILLE KY CM Bulk CM Bulk CM Bulk CM Bulk * CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % C & F FARM SUPPLY, INC. HISEVILLE KY Mat Bulk Mat Bulk Mat Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Statistical Analysis for Grade : Number of Samples This Grade : 5 Average Analysis : CV, % Mat Bulk CM Bulk Mat Bulk

26 REGULATORY BULLETIN C & F FARM SUPPLY, INC. HISEVILLE KY ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % CAMERON CHEMICALS, INC. PORTSMOUTH VA Blend Bulk Blend Bulk CAMPBELLSVILLE CROP SVC. CAMPBELLSVILLE KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk * CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % CECILIA FARM SVC INC. CECILIA KY Mat Bulk Mat Bulk CM Bulk Mat Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Mat Bulk

27 24 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY CECILIA FARM SVC INC. CECILIA KY ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % CEN FARMERS SUP. OF GREEN GREENSBURG KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Statistical Analysis for Grade : Number of Samples This Grade : 5 Average Analysis : CV, % CM Bulk CM Bulk CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % CHEMSICO, DIV OF UNITED INDUSTRIES ST. LOUIS MO * 9.31 * 8.40 * 78 * Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag * 9.02 * * Blend Bag Blend Bag * 8.93 * * Blend Bag * 91 * Blend Bag * * 89 * Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag

28 REGULATORY BULLETIN CHEMSICO, DIV OF UNITED INDUSTRIES ST. LOUIS MO * 113 Blend Bag * 8.13 * 8.01 * 82 * Blend Bag * 8.91 * 89 * Blend Bag Blend Bag * 7.34 * * Blend Bag * Blend Bag Blend Bag Blend Bag * 7.09 * 8.28 * 79 * Blend Bag Blend Bag Blend Bag * 7.32 * 89 * Blend Bag Blend Bag Blend Bag * Blend Bag * * Blend Bag * Blend Bag * 7.58 * 7.91 * 73 * Blend Bag Statistical Analysis for Grade : Number of Samples This Grade : 33 Average Analysis : CV, % Mnfr Bag Blend Bag * * * Blend Bag Blend Bag Blend Bag Blend Bag Blend Bag * * Mnfr Bag Statistical Analysis for Grade : Number of Samples This Grade : 6 Average Analysis : CV, % * 94 * Blend Bag * * Blend Bag Blend Bag Blend Bag Mnfr Bag Mnfr Bag Blend Bag Mnfr Bag Blend Bag Mnfr Bag Blend Bag * * 89 * Blend Bag Blend Bag Blend Bag

29 26 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY CHEMSICO, DIV OF UNITED INDUSTRIES ST. LOUIS MO * 102 Blend Bag ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % CLEMENTS AG SUPP. SPRINGFIELD KY Mat Bulk CM Bulk Mat Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Mat Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % CNI AGRIMINERALS, LLC ALBANY GA Mat Bag Mat Bag CORBIN FARM & GARDEN CTR. CORBIN KY Blend Bag Blend Bag * 8.51 * * Blend Bag Blend Bag Blend Bag CROP PRODUCTION SVC INC (CADIZ) CADIZ KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk

30 REGULATORY BULLETIN CROP PRODUCTION SVC INC (CADIZ) CADIZ KY ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % CROP PRODUCTION SVC INC (CLA) CLARKSON KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Statistical Analysis for Grade : Number of Samples This Grade : 5 Average Analysis : CV, % CM Bulk CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % CROP PRODUCTION SVC INC (CLA) CLAY KY * CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Statistical Analysis for Grade : Number of Samples This Grade : 5 Average Analysis : CV, % CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk

31 28 ANALYSIS OF OFFICIAL FERTILIZER SAMPLES IN KENTUCKY JULY CROP PRODUCTION SVC INC (CLA) CLAY KY ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = % CROP PRODUCTION SVC INC (FANC) FANCY FARM KY CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk CM Bulk Statistical Analysis for Grade : Number of Samples This Grade : 6 Average Analysis : CV, % * 101 CM Bulk CM Bulk ALL SAMPLES,%GUAR ALL SAMPLES,CV % NUMBER OF ANALYSIS Deficiency Rate = 0.00 % CROP PRODUCTION SVC INC (GAL) GALESBURG IL Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk

32 REGULATORY BULLETIN CROP PRODUCTION SVC INC (GAL) GALESBURG IL Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Statistical Analysis for Grade : Number of Samples This Grade : 31 Average Analysis : CV, % Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mnfr Liq Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Statistical Analysis for Grade : Number of Samples This Grade : 6 Average Analysis : CV, % Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk Mat Bulk