Sciences and Analyses of Materials Department Surface Treatment Unit Centre de Recherche Public Gabriel Lippmann Belvaux - Luxembourg
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1 Sciences and Analyses of Materials Department Surface Treatment Unit Centre de Recherche Public Gabriel Lippmann Belvaux - Luxembourg
2 Surface Treatment Unit, UTS BRIEF history : : launched of the TRASU project (FNR) 08/2007 : creation of a Surface Treatment Unit 2013 : the group is constituted of 14 people SCIENTIFIC topics : Surface Treatment Unit Presentation (6 permanent researchers, 2 Post-Doc, 6 PhD) Study of the interaction mechanisms between a non thermal plasma and surfaces to engineer new surface treatments TECHNOLOGY activities : Plasma Enhancement Chemical Vapour Deposition (low to atmospheric pressure) Physical Vapour Deposition (magnetron sputtering) International collaborations : - 2 PhD Université de Lorraine (IJL) - 1 PhD Université de Toulouse (Laplace) - 1 PhD Université de Liège - 1 PhD Université de Bruxelles - 1 PhD Université de Mayence
3 Plasma Surface applications Atmospheric processes Grafting of functional molecules 1 to 80 nm thickness Plasma Organic contaminations Biomolécule decontamination 0,020 to 10 µm Thickness : 5 nm 5 µm Deposition of layer(s) Ultimate cleaning Low pressure plasma processes
4 Diffusion barrier layers Hydrophylic, super-hydrophobic surfaces Corrosion protection coatings Thermal reversible adhesion Photocatalytic surfaces Antibacterial surface Hard coatings Sensoring packaging coatings Adhesion interlayer Bacterial surface décontamination 3D plasma coaters Ultimate cleaning surface Roll-to roll equipments Flat substrate coater
5 Atmospheric pressure plasma processes - facilities Different plasma sources : Direct plasma DBD, remote plasma with DBD, Microwaves, arc discharges Realization of surface treatment on different substrate shapes 1D 2D 3D Flat substrate continuous deposition Object + Robot 300x200mm on wire (0.1 à 5 mm) 300x200x 300mm (IST) (AcXys)
6 Low pressure plasma processes - facilities PVD Magnetron sputtering : - Generators available : DC, pulsed DC, RF, HIPIMS - Codeposition - multilayers ( 2 to 4 targets) - Metallic, oxide, nitride or carbide coatings Realization of surface treatment on different substrate shapes 1D 2D 3D Flat substrate Continuous deposition on wires Object 50x50mm 0.1 à 2 mm 100x100x 150mm
7 Analysis of materials and surfaces A unique set of dedicated scientific instruments A long-time and proven experience in the characterization Elemental/molecular composition Of all materials For all types of investigations 8.00E+04 Materials identification (phase, particles, defects, coatings ) Structural analysis Physical/functional properties With the highest performances With the highest performances NanoSIMS SEM (EDS) XPS SC ultra-sims FE-SEM (EDS,WDS) XRD CMS TEM (EDS,EELS) FTIR/microscopy ToF-SIMS FE-AES RAMAN And direct access (SAM s scientists) to: Confocal microscopy, FTMS, ICP-MS, GC-MS, LC-MS Counts / s 9.00E E E E E C1s C1s peak O-C=O 1 PET C-O Binding Energy (ev) C-C (cycle)
8 Analysis of materials and surfaces Analysis of materials and surfaces National Platform NanoSIMS
9 LEA - LIPES : Laboratoire Européen Associé Contrat entre IJL Univ. de Lorraine CNRS CRPGL Thématique : Interactions entre le Plasma et l extrême surface Projets en commun entre les deux laboratoires : - 4 thèses depuis 2010 Formation Plasma-surface pour jeunes chercheurs : - 3 jours/an depuis 3 ans avec entre participants 1. Introduction to plasma physics and its applications 2. Plasma-surface interaction 3. Plasma diagnostics 4. Surface structuring by plasma 5. Surface functionalizations by plasma 6. Molecular simulation of particule-surface interactions Surface Treatment Unit Presentation
10 NanoBeams PhD School NanoBeams PhD School : nanoanalysis using finely focused ion and electron beams ( - Ion/Matter interactions (atomic collisions, scattering and stopping powers, sputtering and secondary particle emission, ) - Electron/Matter interactions - Instrumentation : geometrical and charged particle optics - Nanoanalysis using finely focused ion and electrons beam - Dynamic SIMS (different modes of analysis, applications) - Static SIMS - TEM - Auger Training organized every year, next session from November 11 to 15, 2013 Surface Treatment Unit Presentation
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