Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005
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1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005 Period of validity: to Holder of certificate: Chemische Fabrik Budenheim KG Budenheim Analytics Rheinstraße 27, Budenheim Tests in the fields: selected physical, physico-chemical, chemical and microbiological analyses of phosphates and phosphoric acid; selected physical, physico-chemical and chemical analyses of water; selected physico-chemical analyses of meat and meat products; selected analyses of powders Abbreviations used: see last page Within the given testing field marked with *), the testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, the free choice of standard or equivalent testing methods. The listed testing methods are exemplary. The testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, to use standards or equivalent testing methods listed here with different issue dates. The testing laboratory maintains a current list of all testing methods within the flexible scope of accreditation. This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/6
2 1 Analyses of phosphates and phosphoric acid 1.1 Determination of content in phosphates by titration * Ph. Eur. 8.5/0116 Ph. Eur. 8.5/0981 Ph. Eur. 8.5/1052 FCC 9th Edition Quantitative analysis in calcium hydrogen phosphate dihydrate (harmonised USP, EP, JP); titration Quantitative analysis in calcium hydrogen phosphate, anhydrous (harmonised USP, EP, JP); titration Quantitative analysis in tricalcium phosphate; titration Quantitative analysis in di- and triphosphates in accordance with FCC; titration 1.2 Determination of loss on drying and ignition in phosphates by gravimetry * Ph. Eur Ph. Eur Determination of loss on drying Determination of loss on ignition in accordance with the monographs 1.3 Determination of bacteria, yeasts and moulds in phosphates using cultural microbiological methods * Ph. Eur , Method B Ph. Eur , Method B Ph. Eur , Method B Determination of total aerobic microbial count in non-sterile products (TAMC) Determination of total yeast and mould count in non-sterile products (TYMC) Determination of specific microorganisms in non-sterile products E. coli, Pseudomonas aeruginosa, Staphylococcus aureus, Salmonella Period of validity: to Translation - 2/6
3 1.4 Determination of trace elements in phosphates and phosphoric acid using atomic absorption spectrometry (flame AAS) * DIN EN ISO DIN E DIN E Water quality Determination of calcium and magnesium Atomic absorption spectrometric method Determination of potassium by atomic absorption spectrometry (AAS) using an air-acetylene flame Determination of sodium by atomic absorption spectrometry (ASS) using an air-acetylene flame 1.5 Determination of elements in phosphates and phosphoric acid DIN EN ISO E DIN EN ISO DIN EN ISO E In-house method FE In-house method AS Water quality Determination of selected elements by inductively coupled plasma optical emission spectroscopy (ICP- OES) Water quality Application of inductively coupled plasma mass spectrometry (ICP/MS) Part 2: Determination of selected elements including uranium isotopes Water quality Determination of mercury Method using atomic fluorescence spectrometry Photometric determination of iron in phosphoric acid, Na, K and NH4 phosphates Photometric determination of arsenic in phosphoric acid and phosphates 1.6 Determination of content using X-ray spectroscopic analysis DIN X-ray spectrometry X-ray emission and X-ray fluorescence analysis (XRF) Part 2: Definitions and basic principles for measurements, calibration and evaluation of results Period of validity: to Translation - 3/6
4 1.7 Physical, physico-chemical and chemical analyses of phosphates and phosphoric acid DIN EN ISO Corrigendum DIN EN 1484 (H 3) ASU L In-house method HPIC1 In-house method HPIC In-house method HPIC In-house method ph-pot Oscillation-type density meters Part 1: Laboratory instruments Water analysis Guidelines for the determination of total organic carbon (TOC) and dissolved organic carbon (DOC) (Modification: application on matrix phosphates and phosphoric acid, here determination of DOC only) Detection of condensed phosphates in meat and meat products (Modification: application on matrix phosphate mixtures) Ion chromatographic determination of pyrophosphates in orthophosphates Ion chromatographic determination of orthophosphates and pyrophosphates in tripolyphosphates Ion chromatographic determination of orthophosphates and tripolyphosphates in pyrophosphates Potentiometric ph Measurement in aqueous phosphate solutions and suspensions 2 Selected analyses of meat and meat products ASU L ASU L Analysis of foodstuffs Determination of total phosphorus content in meat and meat products Photometric method Detection of condensed phosphates in meat and meat products Period of validity: to Translation - 4/6
5 3 Analysis of water 3.1 Determination of indicators in water by electrode measurement * DIN EN ISO (C 5) DIN EN (C 8) Water quality Determination of ph Water quality Determination of electrical conductivity 3.2 Determination of indicators in water by titration * DIN H DIN H Water hardness Determination of acid and base-neutralising capacities 3.3 Selected physico-chemical and chemical analyses DIN EN ISO (D 20) DIN EN ISO (E 22) DIN EN 1484 (H 3) DIN ISO (H 45) Water quality Determination of dissolved anions by liquid chromatography of ions Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate (Modification: here only chloride, nitrate, phosphate and sulfate) Water quality Determination of selected elements by inductively coupled plasma optical emission spectroscopy (ICP- OES) Water analysis Guidelines for the determination of total organic carbon (TOC) and dissolved organic carbon (DOC) (Modification: here determination of TOC only) Water quality Determination of the chemical oxygen demand index (ST-COD) Small-scale sealed tube method Period of validity: to Translation - 5/6
6 4 Selected analyses of powders ISO ISO DIN ISO Determination of the specific surface area of solids by gas adsorption BET method Particle size analysis Laser diffraction methods Test sieves Technical requirements and testing Part 1: Test sieves of metal wire cloth Abbreviations used: ASU BET DIN EN HPIC ISO OES Ph. Eur. TAMC TYMC Official Collection of Methods of Analysis on the basis of 64 Lebensmittel-, Bedarfsgegenstände und Futtermittelgesetzbuch (German Food and Feed Act, LFGB) BET method by Brunauer, Emmett und Teller Deutsches Institut für Normung (German Institute for Standardization) European standard High pressure ionic chromatography International Standards Organisation optical emission spectrometry Pharmacopoeia Europaea Total aerobic microbial count Total yeast and mould count Period of validity: to Translation - 6/6
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