Period of validity: to date of issue:
|
|
- Vernon Armstrong
- 5 years ago
- Views:
Transcription
1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-RM according to the relevant clauses of ISO Guide 34: and DIN EN ISO/IEC 17025:2005 Period of validity: to date of issue: Holder of certificate: LGC GmbH Im Biotechnologiepark TGZ II, Luckenwalde Reference material producing in the fields: certified reference materials for organic neat compounds and salts thereof (e. g. pharmaceutically or forensically relevant substances); reference materials for organic neat compounds and salts thereof (e. g. pharmaceutically or forensically relevant substances); reference materials in form of solutions (e. g. pharmaceutically or forensically relevant substances) Abbreviations used: see last page The laboratory is permitted within the specified testing areas marked with *, without being required to inform and obtain prior approval from DAkkS: the modification, development and refinement of test methods. The listed test methods are exemplary. The laboratory maintains a current list of all test methods in a flexible scope of accreditation. This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/7
2 1 Certified reference materials for organic neat compounds and salts thereof (e. g. pharmaceutically or forensically relevant substances) Product Characteristic Range Pure Organic Substances Identity Relative uncertainty in % Method At least 4 of the following methods: FTIR-ATR, 1H NMR, 13C NMR, MS, melting point (capillary method, DSC), elemental analysis Assay > 95 % m/m 0,3 % Conformity of the test results within the limits of the measurement uncertainty of at least two methods: Titration, 100%-Method HPLC, 100%-Method DSC, carbon titration of the elemental analysis 2 Reference materials for organic neat compounds and salts thereof (e. g. pharmaceutically or forensically relevant substances) Product Characteristic Range Pure Organic Substances Relative uncertainty in % Identity Method Thorough identity checking by several of the following methods or comparison to an international accepted standard: FTIR-ATR, 1H NMR, 13C NMR, MS, melting point (capillary method, DSC), elementary analysis Assay > 90 % m/m < 2 % Assay detection by accredited absolute method or 100%- method (mass balance) with accredited (validated) testing methods Additional assay verification by an independent testing method Period of validity: to Translation 2/7
3 3 Reference materials in form of solutions of organic neat compounds and salts thereof (e. g. pharmaceutically or forensically relevant substances) Product Characteristic Range Method Solutions of pure organic substances Assay 0, g/l Gravimetric production with high precision weighing, on the basis of highly pure starting materials (characterised by quantitative analysis with accredited testing method like e.g. carbon titration of the elemental analysis, examined by 100% - impurities), verified by quantitative analysis (HPLC/GC) against external standard, contamination-free homogenisation and filling The determination of the reference values is based on the following test methods 1 Identity tests of organic compounds with melting point analysis (capillary method)* SOP EXAMPLES Product LGCQUANT Product LGCQUANT Melting Point Identity test of solid, organic pure substances by melting point measurement (capillary method) Identity test of Ethinylestradiol Identity test of Brotizolam 2 Identity tests and assay determinations of organic compounds with elementary analysis * SOP SOP Elemental Analysis Determination of C-, H- and N-content of liquid and solid organic pure substances using elemental analysis for the test on identity Elemental Analysis Content determination of liquid and solid organic pure substances using carbon titration of the elemental analysis Period of validity: to Translation 3/7
4 3 Identity tests and purity determinations of organic compounds with spectroscopy * SOP SOP IR Identity test of solid and liquid organic pure substances by infrared spectroscopy (FTIR-ATR) NMR Identity test of liquid and solid organic pure substances by 1H NMR spectroscopy and by 13C NMR spectroscopy 4 Purity and assay determinations of organic compounds with quantitative nuclear magnetic resonance (qnmr) * SOP SOP Quantitative NMR - Assay determination of solid and liquid organic pure substances Quantitative NMR Determination of residual solvent contents in pure organic compounds 5 Assay determinations of organic compounds with UV-Vis spectroscopy * SOP SOP , Annex 4 UV-Vis Spectrophotometry - Assay determination of organic substances Assay determination of ethanol in aqueous solution with UV/VIS Spectrophotometry via derivatisation with ADH and comparison to a standard 6 Identity tests and purity determinations of organic compounds with mass spectrometry* SOP SOP , Annex 3 MS Identity test of solid and liquid organic pure substances by mass spectrometry (ESI) Determination of the degree of deuteration of organic compounds with HRMS 7 Purity determinations of organic compounds with gravimetry * SOP TGA Determination of residual solvent content of solid organic pure substances by thermal gravimetric analysis Period of validity: to Translation 4/7
5 SOP SOP LOD Determination of residual solvent content of solid organic pure substances by Loss On Drying (LOD) Sulfated Ash Determination of inorganic components in organic pure substances as limit test by Sulphated Ash in a microwave oven 8 Purity and assay determinations of organic compounds in solution with titration * SOP SOP Titration Assay determination of solid and liquid organic pure substances (in solution) by potentiometric titration KFT Determination of water content up to a content of 20% in solid and liquid organic pure substances by Karl-Fischer-Titration - Testing Procedure 9 Purity and assay determinations of organic compounds with gas chromatographie (GC)* SOP SOP EXAMPLES Product LGCAMP Product LGCAMP GCMS-Headspace Residual solvent content in wt% in organic pure substances Purity and assay determinations of organic compounds with GC-MS Purity determination of 7-Aminonitrazepam 1.0 mg/ml in Acetonitrile Purity determination of Chlorpromazine Hydrochloride 1.0 mg/ml in Methanol (as free base) Period of validity: to Translation 5/7
6 10 Purity and assay determinations of organic compounds with HPLC * SOP EXAMPLES Produkt LGCQUANT Produkt LGCQUANT HPLC Purity determination of solid and liquid organic pure substances by HPLC (HPLC with UV-Detector) - Testing Procedure Purity determination of Methyl Parahydroxybenzoate Purity determination of Propyl Parahydroxybenzoate 11 Identity tests and purity determinations of organic compounds with differential scanning calorimetry (DSC) * SOP SOP DSC Purity determination of solid, temperature-stable, organic pure substances with a content >98.5% by DSC Melting Point Identity test of solid organic pure substances by melting point measurement (DSC) Pertinent documents: SOP SOP SOP SOP Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Chap Melting Point Identity test of solid organic pure substances by melting point measurement Method Development KFT - Determination of water content up to a content of 20% in solid and liquid organic pure substances by Karl-Fischer-Titration - Method Development HPLC Purity determination of solid and liquid organic pure substances by HPLC (HPLC with UV-Detector) Method Development HPLC Purity determination of solid and liquid organic pure substances by HPLC (HPLC with UV-Detector) - Method Validation Thermal Analysis - Thermogravimetry Microdetermination of water Coulometric Titration Loss on Drying Period of validity: to Translation 6/7
7 Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Kap Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Chap Ph. Eur. 7.2 Kap Ph. Eur. 7.2 Kap Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Chap Ph. Eur. 6.5 Chap Liquid Chromatography Gas Chromatography Thermal Analysis - DSC Potentiometric Titration Sulfated Ash NMR Spectroscopy Residual solvent per GC Headspace Absorption Spectrophotometry UV and Vis IR Spectroscopy Mass Spectrometry Melting Point Capillary Method Abbreviations used: DSC ESI FTIR-ATR GCMS HPLC NMR SOP Differential Scanning Calorimetry Electrospray-Ionisation Fourier Transform Infrared Spectroscopy Attenuated Total Reflectance Gas Chromatography-Mass Spectrometry High-Performance Liquid Chromatography Nuclear magnetic resonance Standard operation procedure at LGC GmbH Period of validity: to Translation 7/7
Annex to the Accreditation Certificate D-RM according to ISO Guide 34:2009 and DIN EN ISO/IEC 17025:2005
Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-RM-14176-01-00 according to ISO Guide 34:2009 and DIN EN ISO/IEC 17025:2005 Period of validity: 21.04.2017 to 04.08.2019 date
More informationCertificate of Analysis
Certificate of Analysis Reference Material - Primary Standard Product Name: Oxycodone 1.0 mg/ml in Methanol Catalogue Number: Lot Number: 37583 LGCAMP0672.10-01 CAS Number: 76-42-6 Molecular Formula: C
More informationCertificate of Analysis
Certificate of Analysis LGC Quality ISO Guide 34:2009 DAkkS D-RM-14176-01-00 ISO/IEC 17025:2005 DAkkS D-PL-14176-01-00 ISO 9001:2008 DQS 102448 QM08 Primary Reference Standard Tilidine Hydrochloride Hemihydrate
More informationCertificate of Analysis
Certificate of Analysis LGC Quality ISO Guide 34:2009 DAkkS D-RM-14176-01-00 ISO/IEC 17025:2005 DAkkS D-PL-14176-01-00 ISO 9001:2008 DQS 102448 QM08 Primary Reference Standard Granisetron Hydrochloride
More informationCertificate of Analysis
Certificate of Analysis Reference Material - Primary Standard Product Name: Metoprolol Tartrate 1.0 mg/ml in Methanol (as free base) Catalogue Number: LGCAMP0027.00-01 Lot Number: 8525 CAS Number: 56392-17-7
More informationCertificate of Analysis
Certificate of Analysis Reference Material - Primary Standard Product Name: LSD (Lysergic Acid Diethylamide) 1.0 mg/ml in Acetonitrile Catalogue Number: Lot Number: 16905 LGCAMP1346.00-11 O CAS Number:
More informationCertificate of Analysis
Certificate of Analysis LGC Quality ISO Guide 34:2009 DAkkS D-RM-14176-01-00 ISO/IEC 17025:2005 DAkkS D-PL-14176-01-00 ISO 9001:2008 DQS 102448 QM08 Primary Reference Standard Paracetamol H N Catalogue
More informationCertificate of Analysis
Certificate of Analysis Reference Substance Atorvastatin Calcium Catalogue Number: Lot Number: 55085 LGCFOR0400.00 Molecular Formula: 2C 33 H 34 FN 2 O 5 Ca Molecular Weight: 1155.34 CAS Number: [ 134523-03-8
More informationCertificate of Analysis
Certificate of Analysis Reference Substance N-Desmethylclobazam (Norclobazam) Catalogue Number: Lot Number: 16595 LGCFOR0910.01 Molecular Formula: C 15 H 11 ClN 2 O 2 Molecular Weight: 286.71 CAS Number:
More informationCertificate of Analysis
Certificate of Analysis Reference Substance Cefalexin Monohydrate Catalogue Number: Lot Number: 38530 LGCFOR0605.00 Molecular Formula: C 16 H 17 N 3 O 4 S H 2 O Molecular Weight: 365.40 CAS Number: [ 23325-78-2
More informationCertificate of Analysis
Certificate of Analysis Reference Substance Dehydronorketamine Hydrochloride Catalogue Number: Lot Number: 14579 LGCFOR0144.07 Molecular Formula: C 12 H 12 ClNO HCl Molecular Weight: 258.14 CAS Number:
More informationCertificate of Analysis
Certificate of Analysis Reference Substance Benzoic Acid Catalogue Number: Lot Number: 43480 LGCFOR0278.01 Molecular Formula: C 7 H 6 O 2 Molecular Weight: 122.12 CAS Number: [ 65-85-0 ] Long-term Storage:
More informationCertificate of Analysis
Certificate of Analysis Reference Standard 4,5α-Epoxy-14-hydroxy-3-methoxymorphinan-6-one Hydrochloride (Noroxycodone Hydrochloride) Catalogue Number: MM0672.03 Molecular Formula: C 17 H 19 NO 4 HCl Molecular
More information(RS)-2-(4-isobutyrylphenyl)propanoic acid Ibuprofen Impurity J
Reference Material Product Information Sheet Epichem's Quality System conforms to ISO9001:2015 as certified by ECAAS Pty Ltd - Certification number 616061. Name BP Name Synonym(s) O (RS)-2-(4-isobutyrylphenyl)propanoic
More informationAnnex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005
Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL-14468-01-00 according to DIN EN ISO/IEC 17025:2005 Period of validity: 26.07.2016 to 25.07.2021 Holder of certificate: Chemische
More informationIntroduction to Pharmaceutical Chemical Analysis
Introduction to Pharmaceutical Chemical Analysis Hansen, Steen ISBN-13: 9780470661222 Table of Contents Preface xv 1 Introduction to Pharmaceutical Analysis 1 1.1 Applications and Definitions 1 1.2 The
More informationAnnex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005
Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL-14435-01-00 according to DIN EN ISO/IEC 17025:2005 Period of validity: 06.10.2017 to 05.10.2022 Holder of certificate: Eurofins
More informationCertified Reference Material - Certificate of Analysis Methylone, Primary Standard
Certified Reference Material - Certificate of Analysis Methylone, Primary Standard Page 1 of 9 Catalog Number: O Lot: Expiration Date: Description: Packaging: Storage: Shipping: Intended Use: Instructions
More informationEgualen Sodium Granules
Egualen Sodium Granules Dissolution Weigh accurately an amount of Egualen Sodium Granules, equivalent to about 5 mg of egualen sodium (C 15 H 17 NaO 3 S 1/3 H2O) according to the labeled amount,
More informationFinal Report. Characterisation of Sample Report. Job No 2016/11/12-34 AS No. 1234A. Client Example Contact Sample. Signed Date 2017.
Final Report Title Characterisation of Job No 2016/11/12-34 AS No. 1234A Client Contact Sample Author report Signed Date 2017 Easy Reach Report 2017 v2.docx 1 of 33 Contents 1. Study Summary Page 3 2.
More informationCertificate of Analysis
Certificate of Analysis Bromazepam 7-Bromo-1,3-dihydro-5-(2-pyridinyl)-2H-1,4-benzodiazepin-2-one Catalog Number: Br Solution Lot: Expiration Date: Solvent: August 2015 Methanol Volume per Ampule: Not
More informationAnnex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005
Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL-14595-01-00 according to DIN EN ISO/IEC 17025:2005 Period of validity: 22.12.2017 to 13.10.2021 Holder of certificate: Forschungszentrum
More informationCertified Reference Material - Certificate of Analysis
Certified Reference Material - Certificate of Analysis Dehydroepiandrosterone 3-sulfate, Primary Standard D-065 Page 1 of 6 Catalog Number: D-065 Lot: H 3 C Expiration: Description: February 2019 Dehydroepiandrosterone
More informationCertified Reference Material - Certificate of Analysis
Certified Reference Material - Certificate of Analysis Amiodarone-D 4, Primary Standard A-83 Page 1 of 8 Catalog Number: A-83 Lot: Expiration: Description: Packaging: Storage: Shipping: Intended Use: Instructions
More informationSubstance Characterisation for REACH. Dr Emma Miller Senior Chemist
Substance Characterisation for REACH Dr Emma Miller Senior Chemist Submission of a REACH registration dossier, either as a lead registrant or a joint registrant Submission of an Inquiry to ECHA Submission
More informationOndansetron Hydrochloride Tablets
Ondansetron Hydrochloride Tablets Dissolution Perform the test with 1 tablet of Ondansetron Hydrochloride Tablets at 50 revolutions per minute according to the Paddle method, using 900 ml of water
More informationPHENYLEPHRINE HYDROCHLORIDE CERTIFIED REFERENCE MATERIAL
PHENYLEPHRINE HYDROCHLORIDE CERTIFIED REFERENCE MATERIAL OH H 3 C H N OH HCl LOT #: BCBD1315V Fluka No. 11529 NOMINAL WT: 500 mg CERTIFICATE VALIDITY DATE: 12. October 2010 VERSION: BCBD1315V-1 Note: Certificates
More informationAnalytical Strategy: HS 2014 Rafael Hodel, Stefanie Jucker. Quality Control: Quantitative Nuclear Magnetic Resonance
Analytical Strategy: HS 2014 Rafael Hodel, Stefanie Jucker Quality Control: Quantitative Nuclear Magnetic Resonance Quality Control (QC) - Why? 1) Purchasing raw materials and educts Did we get what we
More informationCertificate of Analysis
Certificate of Analysis ISO GUIDE 34 ANAB Cert# AR-1470 ISO/IEC 17025 ANAB Cert# AT-1467 ATROPINE SULFATE CERTIFIED REFERENCE MATERIAL CERTIFIED PURITY: 99.9%, U crm = ±0.2% k = 2 (Mass Balance/anhydrous
More informationCertificate of Analysis
Certificate of Analysis ISO GUIDE 34 ACLASS Cert# AR-1470 ISO/IEC 17025 ACLASS Cert# AT-1467 AMOXICILLIN TRIHYDRATE CERTIFIED REFERENCE MATERIAL HO O H H N H S CH 3 3H 2 O NH 2 N CH 3 COOH CERTIFIED PURITY:
More informationADVANTAME. Not less than 97.0% and not more than 102.0% on the anhydrous basis. Sweetener, flavour enhancer
ADVANTAME SYNONYMS INS No. 969 Prepared at the 80 th JECFA (2015), published in FAO JECFA Monographs 17 (2015), superseding tentative specifications prepared at 77 th JECFA (2013). An ADI of 0-5 mg/kg
More informationLUMEFANTRINUM LUMEFANTRINE
July 2008 LUMEFANTRINE: Final text for addition to The International Pharmacopoeia (July 2008) This monograph was adopted at the Forty-second WHO Expert Committee on Specifications for Pharmaceutical Preparations
More informationCertificate of Analysis
Certificate of Analysis E-903 Page 1 of 7 8-Chloro-6-pentadeuterophenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine Catalog umber: E-903 Cl Solution Lot: Expiration Date: Solvent: August 2016 Methanol
More informationASPIRIN (ACETYLSALICYLIC ACID) CERTIFIED REFERENCE MATERIAL
ASPIRIN (ACETYLSALICYLIC ACID) CERTIFIED REFERENCE MATERIAL HO O O CH 3 O LOT #: BCBD0724V Fluka No. 01478 NOMINAL WT: 1 g CORRESPONDES TO RTC LOT: P500003 CERTIFICATE VALIDITY DATE: 20. October 2011 VERSION:
More informationCOMMON PAPER (FIRST SEMESTER) (ALL BRANCHES) I/II M.PHARMACY ADVANCED INSTRUMENTAL METHODS OF ANALYSIS (THEORY)
COMMON PAPER (FIRST SEMESTER) (ALL BRANCHES) MPH 101 (T) I/II M.PHARMACY ADVANCED INSTRUMENTAL METHODS OF ANALYSIS (THEORY) Unit : 1 : UV.VISIBLE SPECTROSCOPY : Brief review of electromagnetic spectrum
More information1-(2-METHOXYPHENYL)PIPERAZINE Latest revision: June 27, 2005
1-(2-METHOXYPHENYL)PIPERAZINE Latest revision: June 27, 2005 HN O N 1. SYNONYMS CFR: N/A CAS #: Base: 35386-24-4 Hydrochloride: 5464-78-8 Other Names: 2-MeOPP 2-Methoxyphenylpiperazine 2. CHEMICAL AND
More informationM Phil Chemistry. Duration 1 Year. Course I Semester
M Phil Chemistry Duration 1 Year Course I Semester Paper Paper Detail Marks Theory and Sessional MCH 01 Analytical methodologies and methods 100 70&30 (industrial tour & its report writting) MCH 02 Research
More information高等食品分析 (Advanced Food Analysis) I. SPECTROSCOPIC METHODS *Instrumental methods: 1. Spectroscopic methods (spectroscopy): a) Electromagnetic radiation
*Instrumental methods: 1. Spectroscopic methods (spectroscopy): a) Electromagnetic radiation (EMR): γ-ray emission X-Ray absorption, emission, fluorescence and diffraction Vacuum ultraviolet (UV) absorption
More informationBUFOTENINE Latest Revision: August 16, 2005
BUFOTENINE Latest Revision: August 16, 25 H N HO N CH 3 CH 3 1. SYNONYMS CFR: Bufotenine CAS #: Base: 487-93-4 Other Names: N,N-dimethylserotonin, 5-hydroxy-N,N-dimethyltryptamine, mappine 2. CHEMICAL
More informationDedicated solvents for Headspace GC
Dedicated solvents for Headspace GC Dr. Frank Michel sigma-aldrich.com sigma-aldrich.com/analytical Headspace GC - Basics Analysis of headspace above an (aqueous) sample: Gas and vapors are analyzed Injection
More informationADVANTAME (TENTATIVE)
ADVANTAME (TENTATIVE) SYNONYMS INS No. 969 New tentative specifications prepared at the 77th JECFA (2013) and published in FAO JECFA Monographs 14 (2013). An ADI of 0-5 mg/kg body weight was established
More informationHigh-pressure qnmr spectroscopy in condensed- and gas-phase towards determination of impurities and compositions of gas mixtures
13.10.2016 High-pressure qnmr spectroscopy in condensed- and gas-phase towards determination of impurities and compositions of gas mixtures Klas Meyer, Heinrich Kipphardt, Michael Maiwald Online NMR Spectroscopy
More informationRosemary extract liquid
EUROPEAN COMMISSION DIRECTORATE-GENERAL JOINT RESEARCH CENTRE Institute for Reference Materials and Measurements Community Reference Laboratory - Feed Additives Authorisation Evaluation Report of the Community
More informationSupplementary Information
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2015 Supplementary Information Synthesis of hydrocarbon-soluble, methyl-substituted highly branched
More informationInstrumental Chemical Analysis
L1 Page1 Instrumental Chemical Analysis Dr. Ahmad Najjar Philadelphia University Faculty of Pharmacy Department of Pharmaceutical Sciences 2 nd semester, 2016/2017 L1 Page2 Course Syllabus Course title:
More informationFlk = Acy + Cy z. Discover the perfect formula Fluka Reagents. Fluka TM Accuracy Consistency AUTHENTIC
Flk = Acy + Cy z Fluka TM Accuracy Consistency QUALITY ASSURED AUTHENTIC BY HONEYWELL Discover the perfect formula Fluka Reagents Honeywell now delivers Fluka premium grade inorganic reagents worldwide
More informationSTS Directory Accreditation number: STS 0038
International standard: ISO/IEC 17025:2005 Swiss standard: SN EN ISO/IEC 17025:2005 SQTS Swiss Quality Testing Services Grünaustrasse 23 Postfach 702 8953 Dietikon Route de l Industrie 61 Postfach 135
More informationThe Uncertainty of Reference Standards
2009 Cerilliant Corporation The Uncertainty of Reference Standards A Guide to Understanding Factors Impacting Uncertainty, Uncertainty Calculations and Vendor Certifications Authors: Ning Chang PhD, Isil
More informationThe Uncertainty of Reference Standards A Guide to Understanding Factors Impacting Uncertainty, Uncertainty Calculations, and Vendor Certifications
The Uncertainty of Reference Standards A Guide to Understanding Factors Impacting Uncertainty, Uncertainty Calculations, and Vendor Certifications Kevin Gates, Ning Chang, Isil Dilek, Huahua Jian, Sherri
More informationQuestions on Instrumental Methods of Analysis
Questions on Instrumental Methods of Analysis 1. Which one of the following techniques can be used for the detection in a liquid chromatograph? a. Ultraviolet absorbance or refractive index measurement.
More informationp-methoxyamphetamine Latest Revision: May 16, 2013
p-methoxyamphetamine Latest Revision: May 16, 2013 1. SYNONYMS CFR: p-methoxyamphetamine (PMA) CAS #: Base: 23239-32-9 Hydrochloride: 3706-26-1 Other Names: Phenethylamine, p-methoxy-alpha-methyl-, (+/-)-
More information2,5-DIMETHOXY-4-IODOPHENETHYLAMINE Latest Revision: August 22, 2005
2,5-DIMETHOXY-4-IODOPHENETHYLAMINE Latest Revision: August 22, 2005 1. SYNONYMS CFR: CAS #: Other Names: Not Available Base: Not Available Hydrochloride: 69587-11-7 4-Iodo-2,5-dimethoxyphenethylamine 4-Iodo-2,5-dimethoxybenzeneethanamine
More informationSelective Formation of Benzo[c]cinnoline by Photocatalytic Reduction of 2,2 Dinitrobiphenyl with TiO 2 and UV light irradiation
Electronic Supplementary Material (ESI) for Chemical Communications. This journal is The Royal Society of Chemistry 2015 Content: Selective Formation of Benzo[c]cinnoline by Photocatalytic Reduction of
More informationCalibration and Purity Assessment in Chemical Analysis
Better Standards, Better Life! Calibration and Purity Assessment in Chemical Analysis 25 November 2010 Hun-Young So Philosophical question Q: What makes metrology in chemistry so unique? A: Definition
More informationQuality? Who Decides? Mitzi M. Rettinger Vice President, Sales & Marketing Cerilliant Corporation Round Rock, TX
Quality? Who Decides? Mitzi M. Rettinger Vice President, Sales & Marketing Cerilliant Corporation Round Rock, TX Harmonize Methods by Raising the Bar on Calibrators A significant contributor to variability
More informationPhiladelphia University Faculty of Pharmacy Department of Pharmaceutical Sciences First (Fall) semester, 2011/2012. Course code:
Philadelphia University Faculty of Pharmacy Department of Pharmaceutical Sciences First (Fall) semester, 2011/2012 Course syllabus Course title: Pharmaceutical Instrumental Analysis Course level: Third
More informationCHEMISTRY TESTING IN THIS SECTION
CHEMISTRY TESTING ANSI/AAMI/ISO standards and FDA guidelines emphasize the importance of material characterization. Materials or processing aids used in the manufacture of products should be identified
More informationAnnex to the Accreditation Certificate D-K according to DIN EN ISO/IEC 17025:2005
Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-K-15133-02-00 according to DIN EN ISO/IEC 17025:2005 Period of validity: 24.01.2018 to 23.01.2023 Holder of certificate: Hexagon
More informationTechniques useful in biodegradation tracking and biodegradable polymers characterization
Techniques useful in biodegradation tracking and biodegradable polymers characterization Version 1 Wanda Sikorska and Henryk Janeczek 1 Knowledge on biodegradable polymers structures is essential for the
More informationVALLIAMMAI ENGINEERING COLLEGE SRM Nagar, Kattankulathur
VALLIAMMAI ENGINEERING COLLEGE SRM Nagar, Kattankulathur 603 203 DEPARTMENT OF ELECTRONICS AND INSTRUMENTATION ENGINEERING QUESTION BANK V SEMESTER EI6501 Analytical Instruments Regulation 2013 Academic
More informationCHEMISTRY. CHEM 0100 PREPARATION FOR GENERAL CHEMISTRY 3 cr. CHEM 0110 GENERAL CHEMISTRY 1 4 cr. CHEM 0120 GENERAL CHEMISTRY 2 4 cr.
CHEMISTRY CHEM 0100 PREPARATION FOR GENERAL CHEMISTRY 3 cr. Designed for those students who intend to take chemistry 0110 and 0120, but whose science and mathematical backgrounds are judged by their advisors
More informationWork carried out in the Czech Republic
CENTRAL INSTITUTE FOR SUPERVISING AND TESTING IN AGRICULTURE NATIONAL REFERENCE LABORATORY Department of Testing Plant Protection Product Work carried out in the Czech Republic (version for CIPAC website)
More informationThe Use of the ACQUITY QDa Detector for a Selective, Sensitive, and Robust Quantitative Method for a Potential Genotoxic Impurity
The Use of the ACQUITY QDa Detector for a Selective, Sensitive, and Robust Quantitative Method for a Potential Genotoxic Impurity Janet Hammond Waters Corporation, Wilmslow, UK APPLICATION BENEFITS High
More informationCHMC 16 Instrumental Analysis (Syllabus)
CHMC 16 Instrumental Analysis (Syllabus) Course Description CHMC16 is a laboratory course designed to compliment CHMC11 (Principles of Analytical Instrumentation). This course will provide a practical
More informationDEPARTMENT OF ELECTRONICS AND INSTRUMENTATION ENGINEERING SRM NAGAR, KATTANKULATHUR-603203 EI 2302 ANALYTICAL INSTRUMENTS QUESTION BANK UNIT I COLORIMETRY AND SPECTROPHOTOMETRY Part A 1. State Lambert
More informationScheme 1: Reaction scheme for the synthesis of p(an-co-mma) copolymer
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Design and Development of Poly (acrylonitrile-co-methyl methacrylate) Copolymer to Improve
More informationEFAVIRENZ Final text for addition to The International Pharmacopoeia
Document QAS/05.145/FIAL March 07 EFAVIREZ Final text for addition to The International Pharmacopoeia This monograph was adopted at the Fortieth W Expert ommittee on Specifications for Pharmaceutical Preparations
More informationCertificate of analysis Certified reference material code: CRM-00-GTX1&4
Certificate of analysis Certified reference material code: CRM-00-GTX1&4 Name: Gonyautoxin-1 and Gonyautoxin-4 in 0.003 M HCl aq. Batch: 15-001 Description: This Certified Reference Material (CRM) is a
More informationI/II M.PHARMACY (1 st Semester)
1.1 T : ADVANCED INSTRUMENTAL METHODS OF ANALYSIS 1. UV-VISUAL SPECTROSCOPY : Brief review of electromagnetic spectrum, UV-Visual range, energy-wavelength-color relationship. Interaction of electromagnetic
More informationFACULTY OF PHARMACY. M. Pharmacy I Semester (Suppl.) Examination, November 2015 (Common To All) Subject: Pharmaceutical Analytical Techniques
M. Pharmacy I Semester (Suppl.) Examination, November 2015 (Common To All) Subject: Pharmaceutical Analytical Techniques Code No. 6001 / S Note: Answer any Five questions. All questions carry equal marks.
More informationSince 1988 High Force Research has worked with organizations operating in practically all end use sectors requiring chemical synthesis input, and
Since 1988 High Force Research has worked with organizations operating in practically all end use sectors requiring chemical synthesis input, and offers a range of services allied to new product development
More informationSECOBARBITAL Latest Revision: February 15, 1999
SECOBARBITAL Latest Revision: February 15, 1999 1. SYNONYMS CFR: Secobarbital CAS #: Free acid: 76-73-3 Sodium salt: 309-43-3 Other Names: 5-(1-Methylbutyl)-5-(2-propenyl)-2,4,6-(1H,3H,5H)-pyrimidinetrione
More informationSpectroscopy and Chromatography
Spectroscopy and Chromatography Introduction Visible light is one very small part of the electromagnetic spectrum. The different properties of the various types of radiation depend upon their wavelength.
More informationการใช REFERENCE STANDARDS ในการควบค มค ณภาพยา
การใช REFERENCE STANDARDS ในการควบค มค ณภาพยา น ดาพรรณ เร องฤทธ นนท ส าน กยาและว ตถ เสพต ด กรมว ทยาศาสตร การแพทย 23 ส งหาคม 2549 23.08.49 BDN 1 Definition Pharmaceutical Reference Standards A substance
More informationLa RMN quantitative appliquée aux petites molécules
La RMN quantitative appliquée aux petites molécules Fabrice Moriaud - Applications Development - Fällanden 30ème Réunion d Utilisateurs RMN Bruker December 9, 2016 1 Covered in this presentation Quantification
More informationHigh Purity Chromasolv Solvents
Research Chemicals High Purity Chromasolv Solvents Part of Honeywell Research Chemical s Exclusive Riedel-de Haën Brand Portfolio The Chromasolv family of solvents are used in a variety of analytical applications
More information3-Fluoromethcathinone Latest Revision: March 29, 2013
3-Fluoromethcathinone Latest Revision: March 29, 2013 1. GENERAL INFORMATION IUPAC Name: 1-(3-fluorophenyl)-2-methylaminopropan-1-one CFR: Not Scheduled (3/2013) CAS #: 1049677-77-1 Synonyms: Source: Appearance:
More informationBENZYLPIPERAZINE Latest Revision: June 1, 2005
BENZYLPIPERAZINE Latest Revision: June 1, 2005 HN N 1. SYNONYMS CFR: Schedule I CAS #: 2759-28-6 Stride II: Other Names: N-Benzylpiperazine 1-Benzylpiperazine N-Benzylpiperazine 1-(phenylmethyl)piperazine
More informationBRIEFING. (EXC: K. Moore.) RTS C Propylparaben C 10 H 12 O Benzoic acid, 4 hydroxy, propyl ester; Propyl p hydroxybenzoate [ ].
BRIEFING Propylparaben. The European Pharmacopoeia is the coordinating pharmacopeia for the international harmonization of the compendial standards for the Propylparaben monograph, as part of the process
More informationTraceability, validation and measurement uncertainty 3 pillars for quality of measurement results. David MILDE
Traceability, validation and measurement uncertainty 3 pillars for quality of measurement results David MILDE Traceability Validation Measurement Uncerainty Outline Introduction to 3 pillars Recommended
More informationThe Claviature of Gas Analysis
The Claviature of Gas Analysis Mass spectrometric gas analysis for quality assurance of gases and gas mixtures High purity and special gases are becoming increasingly important in the development of modern
More informationAPPLICATION NOTE. Investigation of Alkali Salts with the STA 449 F5 Jupiter. Dr. Alexander Schindler and Dr. Michael Schöneich.
APPLICATION NOTE Investigation of Alkali Salts with the STA 449 F5 Jupiter Dr. Alexander Schindler and Dr. Michael Schöneich Introduction While analytical techniques such as EDX or ICP-MS provide a detailed
More informationTips & Tricks GPC/SEC: Quantify and Get More Than Molar Mass Averages
Tips & Tricks GPC/SEC: Quantify and Get More Than Molar Mass Averages Daniela Held, PSS Polymer Standards Service GmbH, Mainz, Germany Gel permeation chromatography/size-exclusion chromatography (GPC/SEC)
More informationBenchtop NMR Combined with GC/MS Confirms Identity of Forensic Case Sample
APPLICATION NOTE Benchtop NMR Combined with GC/MS Confirms Identity of Forensic Case Sample No. AN52889 Authors: Dean Antic, Ph.D., Thermo Fisher Scientific, San Jose, CA, USA WanLi Wei, Senior Engineer,
More informationDRAFT. Category A Category B Category C Infrared Spectroscopy Capillary Electrophoresis Color Tests
Appendix A: Properties for the Validation Process DRAFT Categories of Analytical Techniques: The following listings of methods or instrumental techniques are from category A, B or C of the Recommended
More informationInternational interlaboratory study of forensic ethanol standards
International interlaboratory study of forensic ethanol standards Bernard King and Richard Lawn LGC, Queens Road, Teddington, Middlesex, UK TW11 0LY. E-mail: bmjk@lgc.co.uk Received 18th January 1999,
More informationCYCLOSERINE Final text for addition to The International Pharmacopoeia. (November 2008) CYCLOSERINUM CYCLOSERINE
December 2008 CYCLOSERINE Final text for addition to The International Pharmacopoeia (November 2008) This monograph was adopted at the Forty-third WHO Expert Committee on Specifications for Pharmaceutical
More informationCouplings / Gas Analysis
Couplings / Gas Analysis General With the coupling of a thermal balance and a gas analyzer like a FTIR spectrometer (Fourier Transform Infrared) or a Quadrupole-Mass-Spectrometer a very powerful analytical
More information(DCHE21) ASSIGNMENT - 1 M.Sc. (Second) DEGREE EXAMINATION, MAY 2019 Second Year CHEMISTRY Analytical Chemistry MAXIMUM : 30 MARKS ANSWER ALL QUESTIONS
ASSIGNMENT - 1 Analytical Chemistry (DCHE21) Q1) State and explain Beer s Law mention its limitations. Q2) Write the basic instrumentation, principle and applications of nephelometry. Q3) Define Fluorescence
More informationSupplementary Information
Facile Preparation of Fluorovinylene Aryl Ether Telechelic Polymers with Dual Functionality for Thermal Chain Extension and Tandem Crosslinking Scott T. Iacono, Stephen M. Budy, Dirk Ewald, and Dennis
More informationHydrophobic Ionic Liquids with Strongly Coordinating Anions
Supporting material Hydrophobic Ionic Liquids with Strongly Coordinating Anions Hasan Mehdi, Koen Binnemans*, Kristof Van Hecke, Luc Van Meervelt, Peter Nockemann* Experimental details: General techniques.
More informationElectronic Supporting Information
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 2017 Electronic Supporting Information Designing the thermal behaviour of aqueous biphasic systems
More informationAdvanced Pharmaceutical Analysis
Lecture 2 Advanced Pharmaceutical Analysis IR spectroscopy Dr. Baraa Ramzi Infrared Spectroscopy It is a powerful tool for identifying pure organic and inorganic compounds. Every molecular compound has
More informationTAAQI - Advanced Instrumental Techniques of Chemical Analysis
Coordinating unit: Teaching unit: Academic year: Degree: ECTS credits: 2018 205 - ESEIAAT - Terrassa School of Industrial, Aerospace and Audiovisual Engineering 714 - ETP - Department of Textile and Paper
More informationUncover the insight with Hyphenation. Gerlinde Wita October 2015
Uncover the insight with Hyphenation Gerlinde Wita October 2015 Let s start from the beginning Outline Material Characterization at PerkinElmer Thermal Analysis DSC, TMA, DMA, TGA - And some examples Hyphenation
More informationLIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (LC/MS) Presented by: Dr. T. Nageswara Rao M.Pharm PhD KTPC
LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (LC/MS) Presented by: Dr. T. Nageswara Rao M.Pharm PhD KTPC INTRODUCTION Principle: LC/MS is a technique that combines physical separation capabilities of liquid
More informationRubber compounding ingredients Sulfenamide accelerators Test methods
Provläsningsexemplar / Preview INTERNATIONAL STANDARD ISO 11235 Second edition 2016-01-15 Rubber compounding ingredients Sulfenamide accelerators Test methods Ingrédients de mélange du caoutchouc Accélérateurs
More informationii) Describe the various types of detectors used in IR spectroscopy.
(DCHE 21) ASSIGNMENT - 1, DEC - 2014. PAPER - V : ANALYTICAL 1) Describe a method for the determination of manganese in complex matrices. 2) Describe the instrumentation and working principles of IR. 3)
More informationPOLYMERIZATION REACTION MONITORING FOR PSA PRODUCTION USING AN ATR-FTIR PROBE
POLYMERIZATION REACTION MONITORING FOR PSA PRODUCTION USING AN ATR-FTIR PROBE Renata Jovanović, Doctoral student, Department of Chemical Engineering, University of Ottawa, Ottawa, Canada, (jovanovi@genie.uottawa.ca)
More informationAquagent. The Scharlau comprehensive pyridine-free solutions range for a reliable Karl Fischer Titration
The Scharlau comprehensive pyridine-free solutions range for a reliable Karl Fischer Titration Karl Fischer titration is a well known and globally accepted method for water determination since the beginning
More information