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1 Product Information: COA: Sample ID: D Type: Concentrate/Extract Lot Number: 700mg Hemp oil Storage conditions: 4 C Customer: Sunshine Global Sample size: 15 ml 150 South Pine Island Rd, #300 Sampled by: Customer Plantation, FL Date Sampled: - License Number: - Sampling Location: - Date Accepted: 02/19/2017 Total CBD mg THC 0.0% Microbial Pesticides Mycotoxins Total Terpenes 0.10% Residual Solvents Heavy Metals 1. Cannabinoid profile: Analysis Method: SOP.T SOP.T QA Testing mg/g CBDV 0.00 CBDA 0.00 CBGA 0.00 CBG 0.00 CBD THCV 0.00 CBN 0.00 Total THC THC THCa CBC mg/g Page 1
2 2. Pesticides: Passed. Analysis Method: SOP.T , SOP.T Pesticide ppb Pesticide ppb None detected None detected Abbreviations: ppb = Parts Per Billion 3. Residual Solvents: Passed Analysis Method: SOP.T Analyte ppm Analyte ppm None detected Abbreviations: ppm = Parts Per Million 4. Contaminant Analysis: Passed Microbial Analysis Method: SOP.T Escherichia Coli (Limit: Absent in 1g) Salmonella (Limit: Absent in 1g) Aspergillus fumigatus (Limit: Absent in 1g) Aspergillus flavus (Limit: Absent in 1g) Aspergillus niger (Limit: Absent in 1g) Aspergillus terreus (Limit: Absent in 1g) 5. Mycotoxins Analysis: Passed. Analysis Method: SOP.T , SOP.T Aflatoxins Aflatoxins B1, B2, G1, G2 (Limit 20 µg/kg) 2.86 µg/kg Ochratoxins Ochratoxins A (Limit 20 µg/kg) 0.00 µg/kg 6. Heavy Metals: Passed. Analysis Method: SOP.T , SOP.T Metal ppm Metal ppm Arsenic (As) Lead (Pb) Cadmium (Cd) Mercury (Hg) Abbreviations: ppm = Parts Per Million 7. Terpenes screening: Analysis Method: SOP.T Analyte % Analyte % alpha-pinene ( ) 0.01 Terpinolene ( )) 0.01 Camphene ( ) 0.00 Linalool ( ) 0.01 beta-myrcene ( ) 0.02 (-)-Isopulegol ( ) 0.00 (-)-beta-pinene ( ) 0.00 Geraniol ( ) 0.00 delta-3-carene ( ) 0.00 trans-caryophellene 0.01 alpha-terpinene ( alpha-humulene ( ) Page 2
3 Ocimene ( ) 0.02 cis-nerolidol 0.00 d-limonene ( ) 0.01 trans-nerolidol 0.00 Ocimene (mixture of isomers) 0.00 (-)-Guaiol ( ) ,8-Cineole (Eucalyptol) ( ) 0.00 (-)-Caryophyllene oxide ( ) 0.00 gamma-terpinene ( ) 0.01 (-)-alpha-bisabolol ( ) Details of testing: 8.1. Cannabinoid Profile Test Results Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T for sample prep and Shimadzu High Sensitivity Method SOP.T for analysis. LOQ for all cannabinoids is 1 mg/l) Pesticide Analysis Pesticide screening is performed using LC-MS (Non-Volatile Pesticides) and GC-MS (Volatile Pesticides) which can screen down to below single digit ppb concentrations for regulated pesticides. Currently we analyze for 66 pesticides. (Method: SOP.T Sample Preparation for Pesticides Analysis via LCMSMS and GCMS, SOP.T Procedure for Pesticide Quantification Using LCMS, and SOP.T Procedure for Volatile Pesticide Quantification Using GCMS) Pesticides Edible Products Dried Flowers All Other Processed Pesticides Edible Products Dried Flowers Page 3 All Other Processed Abamectin B1a Imazalil Acephate Imidacloprid Acequinocyl Kresoxim-methyl Acetamiprid Malathion Aldicarb Metalaxyl Azoxystrobin Methiocarb Bifenazate Methomyl Bifenthrin Methyl parathion Boscalid Myclobutanil Carbaryl Naled Carbofuran Oxamyl Chlorantraniliprole Paclobutrazol Chlorfenapyr MGK Chlorpyrifos Permethrin Clofentezine Phosmet Cyfluthrin Piperonyl butoxide Cypermethrin Prallethrin Daminozide Propiconazole DDVP (Dichlorvos) Propoxur Diazinon Pyrethrins Dimethoate Pyridaben Ethoprophos Spinosad Etofenprox Spiromesifen Etoxazole Spirotetramat Fenoxycarb Spiroxamine Fenpyroximate Tebuconazole Fipronil Thiacloprid Flonicamid Thiamethoxam Fludioxonil Trifloxystrobin Hexythiazox
4 8.3. Residual Solvents Analysis Residual solvent screening is performed using GC-MS which can detect below single digit ppm concentrations for residual solvents. Currently we analyze for 29 residual solvents. (Method: SOP.T Residual Solvent Analysis vis GC/MS) Residual Solvents CAS No. Action Level for Medical Goods 1,2-Dichloroethane ,1-Dichloroethene ,1,1-Trichloroethane Acetone Acetonitrile Benzene Butane Carbon Tetrachloride Chlorobenzene Chloroform Cyclohexane Ethanol Ethyl acetate Ethyl ether Ethylene glycol Ethylene oxide Formamide Heptane Hexane Isopropyl alcohol Methanol Methylene chloride Naphtha Pentane Petroleum ether Propane Trichloroethylene Toluene Total xylenes (ortho-, meta-, para-) Microbial Test Results Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoids purification. (Method SOP.T ) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails the microbiological-impurity testing Mycotoxins Analysis Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using VICAM AflaTest and OchraTest analysis. (Method: SOP.T for sample prep and SOP.T for analysis, LOQ for Aflatoxins 2 ppb and for Ochratoxins 3ppb). Total Aflatoxins (Aflotoxin B1, B2, G1, G2) must be <20µg/Kg of substance. Ochratoxins must be <20µg/Kg of substance. Page 4
5 8.6. Heavy Metals Analysis Heavy Metals screen is performed using ICP-MS (Inductively Coupled Plasma Mass Spectroscopy) which can screen down to below single digit ppb concentrations for regulated heavy metals using Method SOP.T Sample Preparation for Heavy Metals Analysis via ICP-MS and SOP.T Heavy Metals Analysis via ICP-MS. Heavy Metal Action Lavel for Medical Edible Products, Suppositories, Sublingual Products, and other Manufactured Products (µg/g) Action Level for All Inhaled Medical Goods (µg/g) Action Level for Topical and Transdermal Medical Goods (µg/g) Cadmium Lead Arsenic Mercury Terpenes screening Terpenoid profile screen is performed using GC-MS QP-2020 with Headspace Sampler (Gas Chromatography Mass Spectroscopy) which can screen down to below single digit ppb concentrations terpenes using Method SOP.T Terpenoid Analysis Via GC-MS. Sample lot approved by: Jorge Segredo Date: 02/21/2018 Jorge Segredo Lab Director Page 5
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