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1 1 MINISTRY OF ENVIRONMENT, FORESTS & CLIMATE CHANGE (CENTRAL POLLUTION CONTROL BOARD) NOTIFICATION New Delhi, the 24 th October, 2016 Legal/42(3)/87. In exercise of the powers conferred under sub-section (3) of Section 16 and sub-section (2) of Section 17 read with sub-section (4) of Section 4 of the Water (Prevention and Control of Pollution) Act, 1974 (Act 6 of 1974) alongwith rule 28 of the Water (Prevention and Control of Pollution) Rules, 1975, and under sub-section (3) of Section 16 of Air (Prevention and Control of Pollution) Act, 1981 (Act 14 of 1981), the Central Pollution Control Board has established the Board s Laboratories at the places mentioned in Schedule I. 2. The fee payable to the Central Pollution Control Board Laboratories in respect of each report of analysis of various analytical parameters and sampling charges for the water, wastewater, soil, hazardous waste, air / fugitive emissions, source emission, noise monitoring, auto exhaust monitoring and ambient air quality monitoring shall be as per Schedule II: Schedule of sampling and analysis charges for Environmental Samples. 3. The fee prescribed under Schedule II will be subject to revision.

2 2 THE GAZETTE OF INDIA : EXTRAORDINARY [PART III SEC. 4] 4. This notification shall come into force w.e.f SCHEDULE I SCHEDULE OF BOARD S LABORATORIES Place Address 1. Delhi `Parivesh Bhawan East Arjun Nagar Delhi Kolkata Zonal Office East 502, Southend Conclave 1582, Rajadanga Main Road Kolkata West Bengal 3. Vadodara Zonal Office West Parivesh Bhawan Opp. VMC Ward Office 10 Subhanpura Vadodara Gujarat 4. Lucknow Zonal Office North Ground Floor, PICUP Bhawan Vibhuti Khand, Gomtinagar Lucknow Uttar Pradesh 5. Bengaluru Zonal Office South 1 st & 2 nd Floors, Nisarga Bhavana A-Block, Thimmaiah Main Road, 7 th D Cross Opp. Pushpanjali Theatre Shivanagar Bengaluru Karnataka 6. Bhopal Zonal Office - Central 3 rd Floor, Sahkar Bhawan North T. T. Nagar Bhopal Madhya Pradesh 7. Shillong Zonal Office North East "TUM-SIR". Lower Motinagar Near Fire Brigade H.Q. Shillong Meghalaya

3 III 3 SCHEDULE OF SAMPLING AND ANALYSIS CHARGES FOR ENVIRONMENTAL SAMPLES SCHEDULE-II Note : (Applicable w.e.f. July 1, 2016) (i) This schedule supersedes all schedules of sampling and analysis charges notified earlier as such earlier schedules stand cancelled & withdrawn. (ii) 50% discount on analytical charges shall be applicable for the samples forwarded from North-Eastern states. A. SAMPLING CHARGES (I) Sampling charges for Ambient Air/Fugitive emission samples Type of sampling 1. Air Monitoring (a) Sampling (upto each 8 hrs) for suspended particulate matter and gaseous pollutants Note: (II) (b) (c) Sampling (24 hrs) for suspended particulate matter and gaseous pollutants Sampling of Volatile Organic Compounds (VOCs)/ Benzene Toluene Xylene (BTX) (d) Sampling of Poly Aromatic Hydrocarbons (PAHs) (e) Sampling (24 hrs using PUF HVS) of Ambient Air for Dioxin- Furan (PCDDs-PCDFs) congeners (i) Transportation charges will be separate as per actual basis. (ii) Sample analysis charges of respective parameters are separate as per list. Source Emission Monitoring/Sampling charges Type of sampling 1. Source Emission Monitoring (a) Sampling/measurement of Velocity, Flow rate, temperature and molecular weight of Flue Gas (each specific location/each sample in duplicate for the mentioned parameter) (b) Sampling of SO 2 /NO (c) Sampling of Volatile Organic Compounds (VOCs)/ Benzene Toluene Xylene (BTX) (d) Sampling of Poly Aromatic Hydrocarbons (PAHs) (e) Note : (i) (ii) Sampling of emission from stationary source for Dioxin-Furan (PCDDs-PCDFs) congeners using Manual Sampling Kit Transportation charges will be separate as per actual basis. Sample analysis charges of respective parameters are separate as per list (III) Noise Monitoring

4 4 THE GAZETTE OF INDIA : EXTRAORDINARY [PART III SEC. 4] Type of sampling 1. Noise Monitoring (a) First Monitoring (b) Each Subsequent Monitoring within same premises (c) For 08 hours Continuous Monitoring or more Note : (i) (ii) Transportation charges will be separate as per actual basis. Sample analysis charges of respective parameters are separate as per list. (IV) Sampling charges for water & wastewater samples 1. 2 Type of sampling GRAB SAMPLING: 1) Grab sampling/sample/place 2) For every additional Grab sampling/same place COMPOSITE SAMPLING: ) Composite sampling/source/place upto 8 hrs do - upto 16 hrs do - upto 24 hrs ) For every additional composite sampling/same place but different source upto 8 hrs do - upto 16 hrs do - upto 24 hrs Flow Rate measurement/source - once Note : - do - - every additional (i) Transportation charges will be separate as per actual basis. (ii) Sample analysis charges of respective parameters are separate as per list. (V) 1. Note : Sampling charges for Soil samples Type of sampling Grab sampling/sample/place For additional Grab sampling/same place (i) Transportation charges will be separate as per actual basis. (ii) Sample analysis charges of respective parameters are separate as per list. (VI) Hazardous Waste Sample collection charges at the premises of Industry/Import site/disposal site

5 III 5 Type of sampling 1 Integrated sample collection charges B. ANALYSIS CHARGES (I) Analysis charges of Ambient Air/ Fugitive Emission Samples 1 Ammonia Analysis using dragger (per tube) Benzene Toluene Xylene (BTX) Carbon Monoxide Chlorine Fluoride (gaseous) Fluoride (particulate) Hydrogen Chloride Hydrogen Sulphide Lead & Other metals (per metal) As mentioned in respective group at Clause NO Ozone Poly Aromatic Hydrocarbons (PAHs) As mentioned in respective group at Clause Suspended Particulate Matter (SPM) Particulate Matter (PM 2.5 ) Respirable Suspended Particulate Matter (PM 10 ) Sulphur Dioxide Volatile Organics Carbon Trace Metals on air filter paper using EDXRF Aluminium, Antimony, Arsenic, Barium, Bromine, Cadmium, Calcium, Cesium, Chlorine, Chromium, Cobalt, Copper, Gallium, Germanium, Gold, Iodine, Iron, Lanthanum, Lead, Magnesium, Manganese, Molybdenum, Nickel, Palladium, Phosphorous, Potassium, Rubidium, Rutherfordium, Per filter paper Selenium, Silicon, Silver, Sodium, Strontium, Sulphur, Tellurium, Tin, Titanium, Tungsten, Vanadium, Ytterbium, and Zinc. 20 Water Extractable ions in Air Particulate Matter using Ion Chromatograph (IC) (i). Processing / Pretreatment Charge per Sample (Filter Paper) (ii). Cations (Na +, NH 4 +, K +, Ca +2 & Mg +2 ) and Anions (F -, Br -, Cl -, NO 3 -, NO 2 -, SO 4-2 & PO 4-3 ) (for 12 ions) 21 Organic and Elemental Carbon (OC/EC) on quartz filter paper Sample processing and analysis for Dioxin-Furan (PCDDs-PCDFs) congeners (Isotope Dilution method using GC-HRMS) (II) Analysis Charges for Source Emission

6 6 THE GAZETTE OF INDIA : EXTRAORDINARY [PART III SEC. 4] 1 Acid Mist Ammonia Carbon Monoxide Chlorine Fluoride (Gaseous) Fluorides (Particulate) Hydrogen Chloride Hydrogen Sulphide Oxides of Nitrogen Oxygen Polycyclic Aromatic Hydrocarbons (Particulate) As mentioned in respective group at Clause Suspended Particulate Matter Sulphur Dioxide Benzene Toluene Xylene (BTX) Volatile Organic Compounds (VOCs) Sample processing and analysis for Dioxin-Furan (PCDDs-PCDFs) congeners (Isotope Dilution method using GC-HRMS) (III) Ambient Air Quality Monitoring using on-line monitoring instruments by Mobile Van 1 PM 10, PM 2.5, SO 2, NOx, SPM, CO along with Meteorological data viz. temperature, Humidity, Wind speed, Wind direction per hour (minimum charges Rs.15,000/-) + Rs.50.00/km run of the van for 24 hours monitoring (IV) Auto Exhaust Monitoring - One time checking of vehicular exhaust 1 Carbon Monoxide % 2 Hydrocarbon, PPM 3 Smoke Density, HSU As per rate notified by Transport Department (V) Analysis charges of Water & Wastewater samples

7 III 7 PHYSICAL PARAMETERS 1 Conductivity Odour Sludge Volume Index (V.I.) Solids (dissolved) Solids (fixed) Solids (volatile) Suspended Solids Temperature Total Solids Turbidity Velocity of Flow (Current Meter) Velocity of Flow (other) CHEMICAL PARAMETERS Inorganic 1 Acidity Alkalinity Ammonical Nitrogen Bicarbonates Biochemical Oxygen Demand (BOD) Bromide Calcium (titrimetric) Carbon Dioxide Carbonate Chloride Chlorine Demand Chlorine Residual Chemical Oxygen Demand (COD) Cyanide Detergent Dissolved Oxygen Fluoride H. Acid Hardness (calcium) Hardness (total) Iodide Nitrate Nitrogen Nitrite Nitrogen Percent Sodium Permanganate Value ph Phosphate (ortho) Phosphate (total) Salinity

8 8 THE GAZETTE OF INDIA : EXTRAORDINARY [PART III SEC. 4] 30 Sodium Absorption Ratio (SAR) Settlable Solids Silica Sulphate Sulphide Total Kjeldahl Nitrogen (TKN) Urea Nitrogen Cations (Na +, NH + 4, K +, Ca +2 & Mg +2 ) and Anions (F -, Br -, Cl -, NO - 3, NO - 2, SO -2 4 & PO -3 4 ) in surface & ground water sample using Ion (for 12 ions) Chromatograph Metals Processing / pre-treatment Charge per Sample Aluminium Antimony Arsenic Barium Beryllium Boron Cadmium Chromium Hexavalent Chromium Total Cobalt Copper Iron Lead Magnesium Manganese Mercury (Processing & Analysis) Molybdenum Nickel Potassium Tin Selenium Silver Sodium Strontium Vanadium Zinc Organics Organo Chlorine Pesticides (OCPs) Processing / pretreatment Charge per Sample Aldrin Dicofol Dieldrin Endosulfan-I Endosulfan-II Endosulfansulfate

9 III 9 7 Heptachlor Hexachlorobenzene (HCB) Methoxy Chlor o,p-ddt p,p -DDD p,p -DDE p,p -DDT α-hch β-hch γ-hch δ-hch Organo Phosphorous Pesticides (OPPs) Processing / pretreatment Charge per Sample Chlorpyriphos Dimethoate Ethion Malathion Monocrotophos Parathion-methyl Phorate Phosphamidon Profenophos Quinalphos Synthetic Pyrethroids (SPs) Processing / pretreatment Charge per Sample Deltamethrin Fenpropethrin Fenvalerate α-cypermethrin β-cyfluthrin λ-cyhalothrin Herbicides Processing / pretreatment Charge per Sample Alachlor Butachlor Fluchloralin Pendimethalin Polycyclic Aromatic Hydrocarbons (PAHs) Processing / pretreatment Charge per Sample Acenaphthene Acenaphthylene Anthracene Benz(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(e)pyrene

10 10 THE GAZETTE OF INDIA : EXTRAORDINARY [PART III SEC. 4] 45 Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Perylene Phenanthrene Pyrene Polychlorinated Biphenyls (PCBs) Processing / pretreatment Charge per Sample Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Tri Halo Methane (THM) Processing / pre-treatment Charge per Sample Bromodichloromethane Bromoform Chloroform Dibromochloromethane Other Organic Parameter 67 Adsorbable Organic Halogen (AOX) Tanin / Lignin Oil & Grease Phenol Total Organic Carbon (TOC) Volatile Organic Acids BIOLOGICAL TEST 1 Bacteriological Sample Collection Benthos Organism Identification & Count (each sample) Benthos Organism Sample collection Chlorophyll Estimation E. Coli (MFT technique) E. Coli (MPN technique) Faecal Coliform (MFT technique) Faecal Coliform (MPN technique) Faecal Streptococci (MFT technique) Faecal Streptococci (MPN technique) Plankton Sample collection

11 III Plankton (Phytoplankton) count Plankton (Zooplankton) count Standard Plate Count Total Coliform (MFT technique) Total Coliform (MPN technique) Total Plate Count Toxicological - Bio-assay (LC 50 ) Toxicological - Dimensionless toxicity Test Note : (i) (ii) Sampling charges for water and waste water samples are separate as specified in clause A (IV), but subject to minimum of Rs.700/- irrespective of number of samples. Transportation charges are separate on actual basis. (VI) Analysis charges of Soil/Sludge/Sediment/Solid waste samples 1 Ammonia Bicarbonates Boron Calcium Calcium Carbonate Cation Exchange Capacity (CEC) Chloride Colour Electrical Conductivity (EC) Exchangeable Sodium Percentage (ESP) Gypsum Requirement H. Acid Heavy Metal As mentioned in respective group at Clause 5.0 Trace Metals using ED-XRF Aluminium, Antimony, Arsenic, Barium, Bromine, Cadmium, Calcium, Cesium, Chlorine, Chromium, Cobalt, Copper, Gallium, Germanium, Gold, Iodine, Iron, Lanthanum, Lead, Magnesium, 14 Manganese, Molybdenum, Nickel, Palladium, Phosphorous, Potassium, Rubidium, Rutherfordium, Selenium, Silicon, Silver, Sodium, Strontium, Sulphur, Tellurium, Tin, Titanium, Tungsten, Vanadium, Ytterbium and Zinc, per sample. 15 Magnesium Mechanical soil analysis (soil texture) Nitrate Nitrite Nitrogen available Organic Carbon/Matter (chemical method)

12 12 THE GAZETTE OF INDIA : EXTRAORDINARY [PART III SEC. 4] 21 Polycyclic Aromatic Hydrocarbons (PAHs) As mentioned in respective group at Clause Polychlorinated Biphenyls (PCBs) As mentioned in respective group at Clause Pesticides As mentioned in respective group at Clause ph Phosphorous (available) Phosphate (ortho) Phosphate (total) Potash (Available) Potassium Sodium Absorption Ratio (SAR) in Soil extract Sodium Soil Moisture Sulphate Sulphur Total Kjehldhal Nitrogen (TKN) TOC Total water soluble salts Water Holding capacity Sample processing and analysis for Dioxin-Furan (PCDDs-PCDFs) congeners (Isotope Dilution method using GC-HRMS) (VII) Analysis charges for Hazardous Waste samples 1 Preparation of Leachate (TCLP extract/water Extract) Determination of various parameters in Leachate As mentioned in respective group at Clause Flash point/ignitibility Reactivity Corrosivity Measurement of Toxicity - LC Dimensionless Toxicity Total Organic Carbon Absorbable Organic Halogen (AOX)

13 III 13 (VIII) AQC Participation Fees: to be charged by CPCB from respective SPCB s/pcc s or Recognized laboratory for Analytical Quality Control exercise (AQC) samples. 1 Laboratories of Govt./Semi Govt./ Public Sector Undertaken/ Autonomous bodies Private Sector Laboratories P.SINGH PARIHAR, Chairman [ADVT.-III/4/Exty./176/17] Note: The principal notification was published in the Gazette of India vide O. 296(E), dated , and thereafter amended vide O. 389(E) dated , O. 390(E), dated , O. 1218(E), dated and Legal/42(3)/87 dated Uploaded by Dte. of Printing at Government of India Press, Ring Road, Mayapuri, New Delhi and Published by the Controller of Publications, Delhi

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