The Use of COMSOL Multiphysics for Studying the Fracture Pressure of Rectangular Micro-Channels Embedded in Thin Silicon Substrates

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The Use of COMSOL Multiphysics for Studying the Fracture Pressure of Rectangular Micro-Channels Embedded in Thin Silicon Substrates Kaitlin Howell 1, H. Georgiou 2, A. Mapelli 3, P. Petagna 3, G. Romagnoli 3 1 George Mason University, Fairfax, VA, USA; EPFL, Lausanne, Switzerland 2 Cyprus University of Technology (C.U.T), Limassol, Cyprus, EU 3 CERN - The European Organization for Nuclear Research, Geneva, Switzerland, EU 24-Oct-13 Kaitlin.Howell@epfl.ch 1

Micro-fluidic silicon devices are being developed and studied for high energy physics applications at CERN since 2009. distribution manifolds 280 µm deep fluidic inlets 1.6 mm 150 microchannels 200 x 70 µm pitch 400 µm Introduction fluidic outlets 1.6 mm recollection manifolds 280 µm deep Figure 1: Microchannel Cooling Plate 24-Oct-13 Kaitlin.Howell@epfl.ch 2

The amount of material in the sensing area must be minimized. Silicon sensor (200 µm) Bump bonds (50 µm) Electronics chips (100 µm) Figure 1: Particle Physics Detector Setup Introduction A.Mapelli Silicon cooling plate (150 µm) Micro-channels (70x200 µm) Silicon membranes (30 µm) submitted to internal fuidic pressure Figure 2: Microcooling Device Thermally Connected to a Detector 24-Oct-13 Kaitlin.Howell@epfl.ch 3

Cover height (variable) Silicon Pyrex Geometry of Pressure Test Samples and Comsol Models Silicon Channel width (variable) Cover height (variable) Channel width (variable) Pyrex Figure 3: Schematic of Geometries for Pressure Test Samples and Comsol Models 24-Oct-13 Kaitlin.Howell@epfl.ch 4

Experimental Testing for Fracture Pressure Figure 4: Sample after Silicon Fracture Figure 5: Qualitative View of Silicon Fracture Figure 6: Sample after Pyrex-silicon Delamination Fracture Figure 7: Qualitative View of Pyrex-silicon Bonding Fracture Fabricated pressure test samples with simple microchannel geometry. Introduced internal hydraulic pressures until fracture of silicon or Pyrex-silicon bonding interface. 24-Oct-13 Kaitlin.Howell@epfl.ch 5

Comsol Models Structural Mechanics Module One 3D, two 2D models Parameters: Cover height of silicon Channel width Pressure Materials: Pyrex, silicon Conditions: Union between Pyrex and silicon Fillet at bottom of channel Physics generated mesh - Finer Pressure load on all sides of channel Symmetry to create half device Fixed contact on ends of device, top/bottom free Results: J-integral calculations at corners of channel, von Mises stress Figure 8: 3D Model with von Mises Stress Figure 9: 2D Model with J-Integral Contours 24-Oct-13 Kaitlin.Howell@epfl.ch 6

Analytical Formula and J-Integral Analytical model is based off a clamped plate model for channel-like cavities. If J-integral values were greater than analytically calculated critical strain energy release rate, fracture. Integration contour is square with 5µm. Figure 10: 2D Model with J-Integral Contour Equation 1: Analytical Formula for Critical Strain Energy Release Rate [2] Equation 2: J-Integral for Comsol Model [3] 24-Oct-13 Kaitlin.Howell@epfl.ch 7

Fracture pressure (bar) 275 Channel Height Vs. Fracture Pressure Channel Width of 500 µm 250 225 200 175 150 Pyrex-Silicon Delamination Fracture Initial Results 125 100 75 50 25 Silicon Fracture Experiment COMSOL J-Integral 0 0 25 50 75 100 125 150 175 200 225 Channel Height (µm) Figure 11: Results of Comsol Models versus Experimental Testing with a Channel Width of 500µm 24-Oct-13 Kaitlin.Howell@epfl.ch 8

Conclusions and Future Goals Initial Comsol results correlate well to experimental results. Will conduct full parametric analysis of cover height versus channel width versus pressure with Comsol models. Fine tune J-integral 2D model for better accuracy and precision. Create a technique to predict fracture conditions and behavior of future micro-channel devices. 24-Oct-13 Kaitlin.Howell@epfl.ch 9

References [1] A.Francescon, A.Mapelli, G.Nuessle, P.Petagna, A.Pezous, P.Renaud, G.Romagnoli Application of Micro-channel Cooling to the Local Thermal Management of Detectors Electronics for Particle Physics Microelectronics Journal 44 (2013), pp. 612-618 DOI information: 10.1016/j.mejo.2013.03.012 [2] Örjan Vallin, Kerstin Jonsson, Ulf Lindberg, Adhesion quantification methods for wafer bonding, Materials Science and Engineering: R: Reports, Volume 50, Issues 4 5, 30 December 2005, Pages 109-165, ISSN 0927-796X, 10.1016/j.mser.2005.07.002. [3] COMSOL; Single Edge Crack, Model Documentation 24-Oct-13 Kaitlin.Howell@epfl.ch 10