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CHEM. RES. CHINESE UNIVERSITIES 2008, 24(6), 1 8 Volume Contents of Chem. Res. Chinese U. to Vol.24 Volume Contents of Chemical Research in Chinese Universities to Vol.24(2008) Articles Sonochemical Preparation of Micro- and Nanometer Cu 2 O WANG Ling, ZHANG Xiao-xia, YUAN Hong-ming, CHEN Yan, DONG Zhong-ping, PANG Guang-sheng and FENG Shou-hua * (1) 1 Synthesis, Crystal Structure, and Catalytic Performance of 2,6-Bis[1-(2,4,6-trimethylphenylimino)ethyl]pyridine Nickel(II) Complex FAN Rui-qing *, YANG Yu-lin and LÜ Zhi-wei (1) 4 Novel Strategy for Synthesis of High Quality CdTe Nanocrystals in Aqueous Solution YAN Yu-xi, MU Ying *, FENG Guo-dong, ZHANG Lei, ZHU Lin-lin, XU Ling, YANG Rui and JIN Qin-han * (1) 8 Synthesis, DNA-binding, and Photocleavage of 2,3-Di-2-pyridylquinoxaline-silver(I) Complex WANG Xiu-li *, FANG Jia-ni, BI Yan-feng, LIN Hong-yan and LIU Guo-cheng (1) 15 Synthesis, Characterization, and Electrochemical Property of Nanometer Porphyrin Dimer ZHENG Wen-qi, SHAN Ning and WANG Xing-qiao * (1) 20 Immunosensor Based on Surface Plasmon Resonance for Antigen Recognition JIN Wei, MU Ying *, ZOU Xiang-yu and JIN Qin-han * (1) 24 First-order Derivative Spectrophotometry for the Determination of Vitamin C in Medicament MENG Qing-fan, TENG Le-sheng, JIANG Chao-jun, AN Jin-shuang, LI Lei, LU Jia-hui and TENG Li-rong * (1) 29 Synthesis and Herbicidal Activity of Novel Sulfonylureas Containing Thiadiazol Moiety GUO Wan-cheng, LIU Xing-hai, LI Yong-hong, WANG Su-hua and LI Zheng-ming * (1) 32 Tetramethylguanidium Lactate Ionic Liquid: Catalyst-free Medium for Michael Addition Reaction LIANG Da-peng, XIN Xin, DUAN Hai-feng, YIN Yan-zhen, GAO Han, LIN Ying-jie * and XU Jia-ning (1) 36 Synthesis and Anti-tumor Activity of Novel Amide Derivatives of Ursolic Acid LIU Dan, MENG Yan-qiu *, ZHAO Juan and CHEN Li-gong (1) 42 Synthesis and Biological Evaluation of Novel Tricyclic Oximino Derivatives as Antitumor Agents GUO Shu-chun, ZHAO Yan-fang, LI Rong-dong, XIE Li-jun, YANG You-bin and GONG Ping * (1) 47 Sulfonyl Imidazoles as Reagents for the Preparation of Sulfonates and Sulfonamides REN Yu-jie *, GUI Bin, WU Hai-xia and SUN Xiao-bin (1) 54 Novel Method for the Enantioselective Synthesis of β-lactams YUAN Qing, JIAN Shan-zhong and WANG Yan-guang * (1) 58 Effects of Siqi Decoction on Concentration of Nitric Oxide and Activity of Nitric Oxide Synthase in Blood Serum of Rats with Myocardial Ischemia SU Yan-bin,LI Zheng-qiang *,SU Yan-wen and ZHANG Fen-rong (1) 65 Molecular Design and Immunogenicity of a Multiple-epitope FMDV Antigen and DNA Vaccination MA Ming-xiao, JIN Ning-yi *, LIU Hui-juan, ZHENG Min, YIN Ge-fen, TIAN Ming-yao, JIN Ming-lan, LU Hui-jun, SHEN Guo-shun, ZHU Guang-ze, JIN Hong-tao, JIN Kuo-shi and ZHANG Ying-jiu (1) 69 Translational Enhancer of Tobacco mosaic virus Enhancing Expression of Hepatitis B Surface Antigen in Transgenic Panax ginseng C. A. Meyer Callus GAO Zheng-lun, SHENG Jun *, HAO Shu-mei, LIU Dan, LIU Xiao-yu, JI Hai-bin, LI Juan and ZHANG Xian-ping (1) 75 Effects of Vitamin E on the Activities of Protective Enzymes and Membrane Lipid Peroxidation in Leymus Chinensis under Drought Stress GU Jie, LIU Gong-she *, GUO Juan and ZHANG Jin (1) 80 Transferrin and Its Isoforms from Normal Human Serum Revealed by Several Analytical Techniques ZHUO Hui-qin, HUANG He-qing *, JIN Hong-wei and HUANG Lin (1) 84 Natural Compound Curcumin Corrects the Gating Defect of G551DMutant Cystic Fibrosis Trans- membrane Conductance Regulator HAO Li-ming, LIU Xin, XU Li-na, ZHU Na, LIN Sen, HOU Shu-guang, ZHOU Na, SHI De-cheng, SHANG De-jing, MA Tong-hui * and YANG Hong * (1) 92

2 CHEM. RES. CHINESE UNIVERSITIES Vol.24 Kinetics and Mechanism of the Photo-oxidation of Thiophene by O 2 Adsorbed on Molecular Sieves ZHAO Di-shun *, LI Fa-tang, ZHOU Er-peng and SUN Zhi-min (1) 96 Effect of 3-Amino-5-mercapto-1,2,4-triazole on Electroless Nickel Deposition LIU Hai-ping, LI Ning *, BI Si-fu, LI De-yu and ZOU Zhong-li (1) 101 New Chiral Calixarene Derivatives: Syntheses and Their Chiral Recognition Toward Amino Acids by UV-Vis Spectroscopy GU Jin-ying, HE Wan-ping, SHI Xian-fa * and JI Liang-nian (1) 106 Mechanistic Aspects of Monomer, Polymer Formation, and Synthesis of PQ-Alt-Dialkyl-fluorene Conjugated Copolymer Muddasir Hanif, LU Ping, ZHENG Yan, LI Mao, XIE Zeng-qi, MA Yu-guang *, LI Di and LI Jing-hong (1) 110 Poly(vinylidene fluoride)/clay Nanocomposites by Melt Compounding SONG Yu-ming, ZHAO Zhu-di *, YU Wen-xue, ZHENG Wei-tao, LI Bo, YANG Xiao-wei and CHEN Xin-fang (1) 116 Synthesis and Spectroscopic Properties of a Series of New tetra-substituted Metal Phthalocyanines YU Hai-ling, YANG Jin, FU Qiang *, MA Ji-cheng and LI Wei-li (2) 123 New Inorganic-organic Hybrid Compound Containing One Dimensional Keggin Polyoxometalate [SiW 11 O 39 Co] 6 Chains: Preparation, Characterization and Application in Chemically Bulk-modified Electrode WANG Xiu-li *, LIN Hong-yan, LIU Guo-cheng, CHEN Bao-kuan and BI Yan-feng (2) 129 Synthesis of ZrSiO 4 and Coesite in SiO 2 -ZrO 2 System Under High Pressure XUE Yan-feng, XU Da-peng *, ZHANG Guang-qiang, ZHOU Xian-feng, DING Zhan-hui, LIU Xiao-mei and SU Wen-hui (2) 135 Aptamer-based Electrochemical Biosensors for Highly Selective and Quantitative Detection of Adenosine ZHENG Fan, WU Zai-sheng, ZHANG Song-bai, GUO Meng-meng, CHEN Chen-rui, SHEN Guo-li * and YU Ru-qin (2) 138 Simple, Selective, and Sensitive Spectrophotometric Method for Determination of Trace Amounts of Nickel(II), Copper(II), Cobalt(II), and Iron(III) with a Novel Reagent 2-Pyridine Carboxaldehyde Isonicotinyl Hydrazone Sajid H. Guzar and JIN Qin-han * (2) 143 Quality Analysis of Herbal Medicine Products Prepared from Herba Sarcandrae by Capillary Electrophoresis with Electrochemical Detection ZHOU Xiao-guang, SUN Jin-ying, ZHU De-rong, YUAN Bai-qing and YOU Tian-yan * (2) 148 Adsorption of Human Serum Albumin onto PVA-coated Affinity Microporous PTFE Capillary JIN Gu *, YAO Qi-zhi and ZHANG Lei (2) 154 Qualitative and Semi-quantitative Analysis of Quaternary Alkaloids in Coptis-scute Herb Couple by Electrospray Mass Spectrometry LI Wei, SONG Feng-rui, LIU Zhi-qiang * and LIU Shu-ying (2) 162 Component Analysis and Free Radicals Scavenging Activity of Physalis alkekengi L. Polysaccharide CHENG Ying-kun, LI Lei, MENG Zhao-kun, HOU A-li, WU Yu-jie and TENG Li-rong * (2) 167 New Active Organic Substance in Oyster Shell Capable of Scavenging Oxygen Free Radicals with High Efficiency MA Jian-hua * (2) 171 Diels-Alder Addition of Dicyclopentadiene with Cyclopentadiene in Polar Solvents ZHANG Xiang-wen, JIANG Qiang, XIONG Zhong-qiang, ZOU Ji-jun *, WANG Li and MI Zhen-tao (2) 175 Organometallic Gold(III) Derivatives with Anionic Oxygen Ligands-mononuclear Hydroxo, Alkoxo, and Acetato Complexes: Synthesis and Spectral Study Prithwiraj Byabartta * (2) 180 Activation of CFTR-mediated Cl Transport by Magnolin JIN Ling-ling, LIU Xin, SUN Yan, LIN Sen, ZHOU Na, XU Li-na, YU Bo, HOU Shu-guang and YANG Hong * (2) 187 Expression, Purification and Spectral Characterization of p21 Waf1/Cip1 SHI Qiao-yun, ZHENG Yong-chen, REN Jin-song * and QU Xiao-gang (2) 192 Preparation, Characterization, and in vitro Release of Biodegradable Erythromycin-gelatin Microspheres WANG Fei, LIU Pai, JIANG Dan, LIU Cheng-bai, ZHANG Feng-chun and CHEN Xia * (2) 196 Natural Compound Curcumin a Channel Potentiator Rather Than a Corrector of the Defective Intracellular Processing of F 508 Mutant Cystic Fibrosis Transmembrane Conductance Regulator LIU Xin, GUAN Li, HE Cheng-yan, ZHANG Xiao-jing, XU Li-na, SHANG De-jing, MA Tong-hui * and YANG Hong * (2) 200

No.6 Volume Contents of Chemical Research in Chinese Universities to Vol.24(2008) 3 Osmotic Regulation of Betaine Content in Leymus chinensis Under Saline-alkali Stress and Cloning and Expression of Betaine Aldehyde Dehydrogenase(BADH) Gene CUI Xi-yan, WANG Yong and GUO Ji-xun * (2) 204 Nonisothermal Kinetics of Dehydration Process of [Sm(m-ClBA) 3 phen] 2 2H 2 O and [Sm(p-ClBA) 3 phen] 2 2H 2 O REN Ning, WANG Xi-e, ZHANG Jie, ZHANG Jian-jun *, XU Su-ling and ZHANG Hai-yan (2) 210 Resistivity-Temperature Behavior of CB-Filled HDPE Foaming Composites LI Ji-xin, ZHANG Guo *, LI Zhuo-shi, WANG Xin-lei and LIU Xiu-qi (2) 215 Theoretical Studies on Structures and Properties of Endohedral Fullerenes Complexes: XH n @C32(X=F, O, N, C; n=1 4) CHANG Ying-fei, HONG Bo, SUN Li-li, TANG Shu-wei and WANG Rong-shun * (2) 220 Quasi-Classical Trajectory Study of the Chemical Reaction Ca+CH 3 I ZHANG Zhi-hong, CHEN Mao-du * and CONG Shu-lin (2) 223 Cerium Salt Promoted Homocoupling Reaction of Dialkylanilines in Water YANG Xiang-hua, LU Wen-chao, LIAO Qian and XI Chan-juan * (2) 226 Immobilization and Properties of Lipase from Candida rugosa on Electrospun Nanofibrous Membranes with Biomimetic Phospholipid Moities HUANG Xiao-jun *, YU An-guo, GE Dan and XU Zhi-kang (2) 231 Mixed Pyridine-phenol Boron Complex Encapsulated in Polymer/Silica Hybrid Sol-gel Matrix DONG Wei, TANG Jun * and WANG Yue (2) 238 Theoretical Study on the Conformational Conversion of 1,3-Dioxane Inside a Capsular Host WANG Ju, YANG Zuo-yin, WANG Xiu-li, ZHANG Jing-chang and CAO Wei-liang * (2) 241 Preparation, Structure and Properties of 3D Supramolecular Architecture, on the Basis of Hydrogen Bonds and π-π Stacking Between 2D Layers, with Windmill Building Blocks YU Li-qiong, HUANG Ru-dan *, CHI Ying-nan and HU Chang-wen * (3) 251 Synthesis, Crystal Structure and Electrochemistry of Two Complexes (YL n ) 3+ [PW 12 O 40 ] 3 (L=Me 2 SO, Me 2 NCHO) HAN Qiu-xia, WANG Chun-zhang, MA Jian-ru, NIU Jing-yang * and WANG Jing-ping (3) 255 A Facile Solvothermal Synthesis of Monodisperse Ni Nanoparticles YU Peng-fei, CUI Bin *, ZHANG Yan and SHI Qi-zhen (3) 260 A New Maleamide Bridged Carbazole Chromogenic-sensor Based on Proton Transfer Signaling Mode WANG Yue-hong, LIN Hai, SHAO Jie and LIN Hua-kuan * (3) 263 Synthesis and Optical Properties of Ce-doped ZnO YANG Jing-hai *, GAO Ming, ZHANG Yong-jun, YANG Li-li, LANG Ji-hui, WANG Dan-dan, WANG Ya-xin, LIU Hui-lian, FAN Hou-gang, WEI Mao-bin and LIU Fu-zhu (3) 266 Studies on the Components of Crude and Processed Fructus Corni by ESI-MS n ZHOU Li-li, WU Guo-guang, LIU Zhi-qiang * and LIU Shu-ying (3) 270 Rapid Extraction and Analysis of Essential Oil from Cinnamomum Cassia Presl. WANG Lu, WANG Zi-ming, LI Tie-chun, ZHOU Xin, DING Lan and ZHANG Han-qi * (3) 275 Evaluation and QSAR Study of Joint Toxicity of Substituted Phenols and Cadmium to Photobacterium phosphoreum SU Li-min, YUAN Xing, MU Chun-fang, YAN Ji-chang * and ZHAO Yuan-hui (3) 281 Degradation of Phenol by Hydroxyl Radicals on Different Coating Lead Dioxide Electrodes LIU Miao *, TANG Yi-nan, WANG Li, HU Yan-dong, JIAO Xin-qian and HUANG Wen-peng (3) 285 Synthesis, Crystal Structure and Biological Activity of Novel Dichloroacetyl Oxazolidine Herbicide Safeners FU Ying, FU Hong-gang *, YE Fei, WEN Xiao-tian and JIANG Ling-xue (3) 291 Synthesis, Crystal Structure and Biological Activity of 2-Chloro-N-{2-fluoro-5-[N-(phenylsulfonyl) phenylsulfonamido]phenyl}benzamide LI Wen-ming, WANG Jian-guo *, LI Zheng-ming and SONG Hai-bin (3) 295 Structure and Biological Activities of Novel Triazole Compounds Containing 1,3,4-Oxadiazole Ring XU Liang-zhong *, BI Wen-zhao, SHANG Yu-qing, ZHAI Zhi-wei and YI Xu (3) 299 New Macrocyclic Diamide from Rauvolfia Yunnanensis Tsiang GENG Chang-an and LIU Xi-kui * (3) 303 Schiff-base Amino Alcohol-zinc Complex for Enantioselective Addition of Phenylacetylene to Aromatic Ketones CHEN Chao, HONG Liang, WANG Quan, ZHANG Bang-zhi and WANG Rui * (3) 306 Mutation Analysis of AVPR2 and AQP2 Gene in Chinese Patients with Congenital Nephrogenic Diabetes Insipidus WANG Ying, LI Hong-jun *, YU Zhen-xiang, BAO Yong-li, WU Yin, YU Chun-lei *, MENG Xiang-ying and LI Yu-xin (3) 312 Expression and Characterization of HIV-1 Envelope Glycoprotein in Pichia Pastoris ZHAO Li-hui, YU Xiang-hui, JIANG Chun-lai, WU Yong-ge, SHEN Jia-cong * and KONG Wei * (3) 316

4 CHEM. RES. CHINESE UNIVERSITIES Vol.24 Comparison Between the Effects of 2-Selenium Bridged β-cyclodextrin and Ebselen on Treating SHRsp Stroke JIA Zhi-dan, LIN Feng, LIU Lei, MU Ying, YAN Gang-lin * and LUO Gui-min * (3) 322 In vivo Anti-tumor Effect of sirna Against STAT3 on Transplanted Lewis Lung Cancer in Mice WANG Chun-guang, WANG Rong-you, SUN Mei, LI Jin-dong, GAO Nan, ZHANG Xing-yi *, SHI Dong-lei and JIN Cheng-yan (3) 330 Peptide Inhibitors of HIV-1 Virus Infection Based on Cullin-5 ZHU Ke-tong, ZHANG Xi-zhen, LOU Chao-ping, GUO Bo, DU Juan, WANG Xiao-dan,WU Yong-ge, KONG Wei * and YU Xiang-hui * (3) 338 Cloning and Expression of Intracellular Part of Receptor Protein Tyrosine Phosphatase RPTPα and Preparation of Its Polyclonal Antibodies CHEN Yang, YANG Su-juan, FU Yao, WANG Jia-peng, ZHAO Zhi-zhuang and FU Xue-qi * (3) 344 Purification and Characterization of a Proteolytic Enzyme from Fig Latex HUANG Lu, QU He-zhi, ZHANG Lei, DU Shan-shan, YANG Shuo, HAO Dong-yun and WANG Xiao-ping * (3) 348 Decomposition Reaction of Zn-MPA(3-Mercaptopropionic Acid) Complex Under Microwave Irradiation JIAN Wen-ping, LIU Sheng, LI Jun * and YANG Wen-sheng (3) 353 Preparation, Characterization and Catalytic Performance of La-SO 2 4 /SBA-15 in Esterification of Acetic Acid with n-butanol TIAN Zhi-ming, DENG Qi-gang *, SUN Hui and ZHAO De-feng * (3) 357 Controllable Synthesis of Titania Nanocrystals with Different Morphologies and Application to the Degradation of Phenol CHEN Da-wei, SHI Jin-e, YAN Ji-chang *, WANG Yue-hong, YAN Fu-cheng, SHANG Shu-xia and XUE Jing (3) 362 Ultra-large Scale Molecular Dynamics Simulation for Nano-engineering ZHAO Jian-wei *, YIN Xing, LIANG Shuai, LIU Yun-hong, WANG Dong-xu, DENG Sheng-yuan and HOU Jie (3) 367 Theoretical Studies on N 2 H+O Reaction LÜ Ying-wen, LÜ Wen-cai * and SU Zhong-min (3) 371 Preparation and Characterization of Titania-grafted Poly(styrene-divinybenzene) Nanocomposite Microspheres LI Sen, CHENG Jiang, WANG Kuan and YANG Zhuo-ru * (3) 378 Synthesis and Characterization of a One-dimensional Coordination Polymer Generated from Unsymmetrical Bridging Organosulfur Ligand WANG Lei, ZHANG Hui, DONG Wen-jun, SHI Zhan and FENG Shou-hua * (4) 389 Two New Iron Coordination Polymers Based on Fe-pyta Chains Incorporating Pyridine-2,4,6-tricarboxylate CHEN Zi-yun and PENG Meng-xia * (4) 392 Synthesis and Crystal Structure of a Complex of Melamine with Benzoic Acid ZHANG Xiu-lian * (4) 396 Synthesis, Characterization, and DNA Binding Properties of Dinuclear Copper(II) Complex [Cu 2 (TATP) 2 (L-Leu) 2 (ClO 4 ) 2 ] 2 2H 2 O GU Qin, LIN Qing-bin, LIU Ying-ju, LE Xue-yi * and FENG Xiao-long (4) 401 Preparation of Copper Phthalocyanine Crystals Using Solvothermal Synthesis XIA Dao-cheng, LI Wan-cheng, WANG Xu, YU Shu-kun, FAN Cui-xiang, MA Chun-yu, CHENG Chuan-hui, FAN Zhao-qi, DU Guo-tong *, CONG Fang-di and DU Xi-guang (4) 407 Biological Fingerprinting Analysis of Interaction Between Taxoids in Taxus and Microtubule Protein by Microdialysis Coupled with High-performance Liquid Chromatography/Mass Spectrometry for Screening Antimicrotubule Agents LEI Xiao-yuan, KONG Liang, SU Xing-ye, GUO Ming and ZOU Han-fa * (4) 411 Simultaneous LC-MS/MS Determination of Danshensu and Paeoniflorin for Permeability Studies in Caco-2 Intestinal Absorption Model LIU Li, ZHAO Xiao-ping, ZHU Di-feng, CHENG Yi-yu and QU Hai-bin * (4) 420 Cytotoxic Diarylheptanoids from Pericarps of Juglans Cathayensis Dode LI Yi-xiu, RUAN Han-li *, ZHOU Xue-feng, ZHANG Yong-hui, PI Hui-fang and WU Ji-zhou (4) 427 Detecting and Identifying in vivo Metabolites of Brodimoprim via LC/ESI-MS with Data-dependent Scanning LIN Yan-ping, SI Duan-yun and LIU Chang-xiao * (4) 430 Efficient Synthesis of 3,5,6,7-Tetrahydro-4H-cyclopenta [4,5]thieno[2,3-d] Pyrimidin-4-ones LIU Ming-guo, ZHONG Ying and DING Ming-wu * (4) 437 Chiral Separation of Spiro-compounds and Determination Configuration LIANG Ya, GUO Jing-jing, LIU Xiu-ming and WEI Rong-bao * (4) 441 Synthesis of 3-Benzyloxy-6-methyl-7-methoxyphenanthrene-9-carboxaldehyde with Utilize Intramolecular Heck Reaction as the Key Step SONG Yan-ling, ZHAI Xin, SUN Zhi-feng, KIM Sang-hee and GONG Ping * (4) 445 Intercalation, Cytotoxicity, and Molecular Modeling of Acenaphtho[1,2-b]pyrrole Chromophores as a New Family of Antitumor Agents ZHANG Zhi-chao *, ZHANG Jing, YUAN Chun-li, WU Gui-ye and QIAN Xu-hong * (4) 449

No.6 Volume Contents of Chemical Research in Chinese Universities to Vol.24(2008) 5 Synthesis, Characterization and Antibacterial Activity of New 5-Aryl Pyrazole Oxime Ester Derivatives LIU Xin-hua *, ZHI Li-ping, SONG Bao-an and XU Hong-li (4) 454 Transferring CdTe Nanoparticles from Liquid Phase to Polyvinylpyrrolidone Nanofibers by Electrospinning and Detecting Its Photoluminescence Property WANG Shu-gang, YANG Qing-biao, BAI Jie, SONG Yan, ZHANG Chao-qun and LI Yao-xian * (4) 459 Biomimetic Decarboxylation of Carboxylic Acids with PhI(OAc) 2 Catalyzed by Manganese Porphyrin [Mn(TPP)OAc] GHOLAM REZA Karimipour * and ROXANA Ahmadpour (4) 464 First Total Synthesis of Hyacinthacine A 6 from the Protected Derivative of Polyhydroxylated Pyrrolidine ZHANG Tao-xiang, ZHOU Ling and CAO Xiao-ping * (4) 469 Synthesis of 4 -Spironucleoside via Radical Translocation Cyclization Reaction DANG Shao-feng, SUN Jing-bo, XU Xian-xiu, WANG Pei and WU Jin-chang * (4) 473 Design, Synthesis and Biological Activity of Ethyl 2-(N-Substituted-arylsulfonamido)-2-oxoacetate WANG Bao-lei, WU Jing, HE Feng-qi, LI Yong-hong and LI Zheng-ming * (4) 477 Inhibition of Growth of Human Ileocecal Adenocarcinoma Cells HCT-8 and Inducing Apoptosis by Different RGDcontaining Peptides WANG Hua, YANG Shao-juan, GAO Shuo-hui, HUANG Yi-bing, LI Jing, CAI Ming-jun, XU Li * and ZHANG Xue-zhong * (4) 481 Synthesis of Codon-optimized Human Interleukin-18 Gene by Combination of Chemical and Enzymatic Method GAO Chao-hui, SHI Xiao-yue, HOU Xin-tong, MENG Qing-fan, Zhang Ying-jiu and TENG Li-rong * (4) 487 Inhibition of Ampicillin-resistance in Bacteria by Modified DNAzymes CHEN Fei, LI Zhe, YANG Shuo, WANG Rui-jian, LIU Bin, SONG Yu-ming, SUN Yan-hong, HAO Dong-yun and WANG Xiao-ping * (4) 491 Synthesis and Evaluation of Nicotinoylamino Acid Compounds as Radiosensitizer QIN Zhi-zhong, ZHANG Feng-bao, JIANG Tie-nan, LI Mei-jia, WANG Rong-xian * and LI Yi-liang (4) 496 Effect of β Radiation on Bcl-2 and Bax Expressions in Benign Prostate Hyperplasia Tissues MA Qing-jie, GAO Shi, ZHAO Jie, GU Xin-quan, CAI Shan-yu and ZHAO Guo-qing * (4) 501 Establishment of a Tumor-bearing Mouse Model Stably Expressing EGFP Labeled Human MUC1 VNTRs ZHANG Shu-zi, ZHANG Hai-hong, ZHANG Wa, SHI He-liang, YU Xiang-hui, KONG Wei * and LI Wei (4) 505 Impedance Studies of Spinel LiMn 2 O 4 Electrode/electrolyte Interfaces ZHUANG Quan-chao, FAN Xiao-yong, XU Jin-mei, WEI Guo-zhen, DONG Quan-feng and SUN Shi-gang * (4) 511 Relative Responses of Noble Gases Using a Pulsed Discharge Helium Photoionization Detector: Theoretical Calculation and Experimental Determination ZHANG Hai-tao, WU Di * and ZHANG Li-xing (4) 516 Theoretical Studies on the Iodine-catalyzed Nucleophilic Addition of Acetone with Five-membered Heterocycles WANG Yan-hua *, LI Li and CHEN Xue-song (4) 520 Comparison of the Sol-gel Method with the Coprecipitation Technique for Preparation of Hexagonal Barium Ferrite WANG Jing-ping *, LIU Ying, ZHANG Mi-lin, QIAO Ying-jie and XIA Tian (5) 525 Hydrothermal Synthesis, Crystal Structure and Spectroscopic Investigations of [Y(C 6 NO 2 H 5 ) 3 (H 2 O) 2 ] n (1.5nZnCl 4 ) nh 2 O with Unprecedented Polycationic Chains FANG Xiao-niu *, CHEN Wen-tong and LIU Dong-sheng (5) 529 Synthesis and Soft Magnetic Properties of Mg-doped Ni Nanoparticles YANG Jing-hai *, FENG Bo, LIU Yang, ZHANG Yong-jun, YANG Li-li, WANG Ya-xin, LANG Ji-hui and WANG Dan-dan (5) 534 Gold Nanoparticle-based Colorimetric Sensor for ph Sensing ZHU Lin, XUE Dong-hua and WANG Zhen-xin * (5) 537 QSAR Studies on PCDD/Fs by Kernel PLS TANG Kai-lin, LI Tong-hua * and CHEN Kai (5) 541 Iodine Determination by Microwave Plasma Torch Atomic Emission Spectrometer Coupled with Online Preconcentration Vapor Generation echnique FEI Yan-qun, LUO Gui-min, FENG Guo-dong, CHEN Huan-wen, FEI Qiang, HUAN Yan-fu * and JIN Qin-han * (5) 546 Subunit Characteristics of Pig Pancreas Ferritin Revealed by MALDI-TOF MS and RP-HPLC HUANG Lin, LIN Zhi-cao, LIN Qing, LUO Lian-zhong and HUANG He-qing * (5) 550 Selective Reduction of 7-Demethylsinomenine LI Yu-feng, BU Qing-min, QIAN Yi, PAN Yi *, LI Jian-xin, HUANG Le-qun and ZHU Hong-jun (5) 557 Syntheses and Structures of Binaphthyl-bridged Schiff Bases WANG Bin, LI Min-xiong, XU Shan-sheng, SONG Hai-bin and WANG Bai-quan * (5) 561

6 CHEM. RES. CHINESE UNIVERSITIES Vol.24 Isolation of Trichoderma reesei pyrg Negative Mutant by UV Mutagenesis and Its Application in Transformation LONG Hao, WANG Tian-hong * and ZHANG Ying-kuan (5) 565 Synthesis and Luminescent Property of Polycarbazole/Polyhedral Oligomeric Silsesquioxane Nanocomposites ZHU Yu-fang, ZHAO Jun-feng, WANG Xi and LI Qi-fang * (5) 570 Synthesis, Characterization and Biological Activities of Novel Acrylamide Compounds XU Liang-zhong *, XU Zhong-jie, ZHANG Gong-sheng, ZHOU Kai and ZHAI Zhi-we (5) 575 Construction of HIV-1 Virus-like Particle Vaccine ZHAO Dong-hai, ZHANG Xi-zhen, YU Xiang-hui * and KONG Wei * (5) 579 Isolation and Purification of Polysaccharides from Cordyceps minlitaris and Its Inhibition on the Proliferation of Rat Glomerular Mesangial Cells HOU A-li, MENG Qing-fan, AN Jin-shuang, ZHU Kai, FENG Yun and TENG Li-rong * (5) 584 Preparation and Characterization of Biodegradable Polylactide(PLA) Microspheres Encapsulating Ginsenoside Rg3 LIU Cheng-bai, ZHANG Di, LI De-guan, JIANG Dan and CHEN Xia * (5) 588 Purification and Characterization of the Catalytic Domain of Protein Tyrosine Phosphatase SHP-1 and the Preparation of Anti-ΔSHP-1 Antibodies LI Wan-nan, ZHUANG Yan, LI He, SUN Ying, FU Yao, WU Xiao-xia, ZHAO Zhi-zhuang and FU Xue-qi * (5) 592 Etoposide Induces Mitochondria-Associated Apoptotic Cell Death in Human Gastric Carcinoma Cells LI Jing-hua, CHEN Yue, WANG Jia-si, KONG Wei and JIN Ying-hua * (5) 597 Low Temperature Heat Capacities and Thermodynamic Properties of Zinc L-Threonate Zn(C 4 H 7 O 5 ) 2 (s) by Adiabatic Calorimetry CHEN Jing-tao, DI You-ying *, TAN Zhi-cheng, CHEN San-ping and GAO Sheng-li (5) 603 Thermal Behavior, Nonisothermal Decomposition Reaction Kinetics of Mixed Ester Double-base Gun Propellants YI Jian-hua, ZHAO Feng-qi *, XU Si-yu, GAO Hong-xu and HU Rong-zu (5) 608 TiO 2 -Supported Binary Metal Oxide Catalysts for Low-temperature Selective Catalytic Reduction of NO x with NH 3 WU Bi-jun *, LIU Xiao-qin, XIAO Ping and WANG Shu-gang (5) 615 Catalytic Oxidation of NO over La 0.8 Sr 0.2 MnO 3 Perovskite ZHAO Ying-xian *, WEI Feng and YU Ying (5) 620 Thermal Degradation Kinetics of N,N'-Di(diethoxythiophosphoryl)-1,4-phenylenediamine REN Yuan-lin *, CHENG Bo-wen, ZHANG Jin-shu, JIANG Ai-bing and FU Wen-li (5) 628 Effects of Lanthanide Ions on Electrooxidation of Methanol WANG Hai-tao *, YIN Yu-chun and GAO Shu-juan (5) 632 Electroless Nickel Plating and Electroplating on FBG Temperature Sensor SHEN Ren-sheng, TENG Rui, LI Xiang-ping, ZHANG Jin, XIA Dao-cheng, FAN Zhao-qi, YU Yong-sen, ZHANG Yu-shu and DU Guo-tong * (5) 635 Blends of Polypropylene and Syndiotactic 1,2-Polybutadiene: Morphology, Crystallization Behaviors and Mechanical Properties ZHANG Cheng-wu, HUANG Yu-dong *, WANG Sheng-chao, ZHANG Chun-yu and ZHANG Xue-quan (5) 640 Influence of Glycerol Content on Properties of Wheat Gluten/Hydroxyethyl Cellulose Biocomposites SONG Yi-hu *, ZHENG Qiang and LIU Cheng (5) 644 PTC/NTC Behavior of PVDF Composites Filled with GF and CF WANG Xin-lei, ZHANG Guo *, LI Ji-xin, LI Zhuo-shi, LIU Zhan-fang and LIU Xiu-qi (5) 648 Effect of Ultrasonication on Optical Properties and Electronic States of Conjugated Polymer MEH-PPV WU Meng, YANG Gui-zhong, WANG Meng, WANG Wei-zhi, WANG Min and LIU Tian-xi * (5) 653 Cis- and Trans-Coordination Assembly of Nitrogen Heterocycle with Copper(II) and Silver(I) TAN Di, TAN Gui-ping, HUANG Xiao-chun, TONG Shan-ling *, YANG Ke-er and YAN Yan * (6) 661 Synthesis, Characterization, and Properties of Supported Tungstozincate Bridged by Co(II) Complex Fragment LIU Kun, LI Jia, LIU Hong-bo and CHEN Ya-guang * (6) 668 Preparation and Magnetic Property of La 0.7 Sr 0.3 MnO 3 Nanorod by Combination Sol-Gel with Molten Salt QI Shu-yan, FENG Jing *, XU Xiao-dong, WANG Jing-ping, HOU Xiang-yu and ZHANG Mi-lin (6) 672 Synthesis and Structural Characterization of Manganese Carbonyl Incorporated Polyoxomolybdate (n-bu 4 N) 2 [Mo 6 O 16 (OCH 3 ) 2 {HOCH 2 C(CH 2 O) 3 } 2 {Mn(CO) 3 } 2 ] WANG Jing-ping, LI Ji-li and NIU Jing-yang * (6) 675 Vacuum Ultraviolet Excited Photoluminescence Properties of Y 2 O 2 S:Eu 3+,Bi 3+ Phosphor WANG Zhi-long, WANG Yu-hua * and ZHANG Jia-chi (6) 679 Preparation, Crystal Structure, and Thermal Analysis of Carbohydrazide Trinitrophloroglucinolate LIU Zhen-hua, ZHANG Tong-lai *, HU Xiao-chun, ZHANG Jian-guo, YANG Li, and QIAO Xiao-jing (6) 683

No.6 Volume Contents of Chemical Research in Chinese Universities to Vol.24(2008) 7 Effects of Magnesium and Ferric Ions on Crystallization of Calcium Sulfate Dihydrate Under the Simulated Conditions of Wet Flue-gas Desulfurization GAO Xiang *, HUO Wang, ZHONG Yi, LUO Zhong-yang, CEN Ke-fa, NI Ming-jiang and CHEN Le-ming (6) 688 Determination of Acetonitrile Volume Fraction in Mobile Phase by HPLC WU Yi, WANG Zhi-wu, GU Jing-kai and WANG Ying-wu * (6) 694 Characterization of Hapten-Protein Conjugates for Immunoassay of Polycyclic Aromatic Hydrocarbons(PAHs) ZHANG Yan-feng *, GAO Zhi-xian, SUN Hong-wen and DAI Shu-gui (6) 697 Electrochemical Study on the Interaction of Protein with Bromothymol Blue and Its Analytical Application WANG Xue-liang, YANG Jie and JIAO Kui * (6) 701 Determination of Seven Major Ginsenosides in Different Parts of Panax quinquefolius L.(American Ginseng) with Different Ages ZHANG Kun, WANG Xiao, DING Lan, LI Juan, QU Chen-ling, CHEN Li-gang, JIN Hai-yan * and ZHANG Han-qi (6) 707 Fluorescent Switch Behavior of 1, 2-Bis(4-pyridyl) Ethylene Controlled by ph in Aqueous Solution ZOU Wen-sheng, SHEN Qian-jin, WANG Yu * and JIN Wei-jun * (6) 712 Quantitative Analysis of Berberine in Processed Coptis by Near-Infrared Diffuse Reflectance Spectroscopy ZHANG Yong, XIE Yun-fei, SONG Feng-rui, LIU Zhi-qiang, CONG Qian * and ZHAO Bing * (6) 717 Fabrication of Poly(4-vinylpyridine) Nanofiber and Fluorescent Poly(4-vinylpyridine)/Porphyrin Nanofiber by Electrospinning SONG Yan, ZHAN Nai-qian, YU Miao, YANG Qing-biao, ZHANG Chao-qun, WANG Heng-guo and LI Yao-xian * (6) 722 Preparation of Highly Active Pt-K/γ-Al 2 O 3 Catalyst for o-phenylphenol Synthesis from o-cyclohexenylcyclohexanone Dehydrogenation DING Jie-lian *, LIN Ling, XU Jian-dong and ZENG Chong-yu (6) 726 Synthesis of an Anti-AIDs Drug Delavirdine Derivate, Resdelasu GUAN Qing-xiang, HE Li-peng, WANG Xi, ZHANG Wen-yan, WANG En-si * and YU Xiang-hui * (6) 731 Regioselective Deprotection of 1,3-Dibenzyl-5-(N,N-dimethylamino)-6-phenylethyluracil LI A-min, WANG Xiao-wei, ZHANG Zhi-li, CHENG Zhi-jian and LIU Jun-yi * (6) 735 Synthesis of Heterocycle Compounds Containing Two Pyridazinone Units XIN Bing-wei * (6) 739 Preparation of Nicotinic Acid from Oxidation of 3-Picoline with Oxygen Under Catalysis of T(o-Cl)PPMn BAI Jin-quan *, WANG Qi-chang, HU Yun and GUO Feng-yan (6) 743 Asymmetric Synthesis of (R)- and (S)-Moprolol WANG Zhao-yang, WANG Yan, SUN Li-wen and ZHU Jin-tao * (6) 747 Cloning, Expression and Purification of Wheat Acetyl-CoA Carboxylases CT Domain in E. coil WANG Rui-jian, YANG Xue-ying, ZHENG Liang-yu *, YANG Ye, GAO Gui and CAO Shu-gui * (6) 752 Functional Mechanism of Resveratrol in Inhabiting Growth of Cells ls174t and Its Mechanism in Subcutaneously Transplanted Tumor of Nude Mice CHEN Jie, DONG Xin-shu * and GUO Xing-gang (6) 756 Lethal Effect of Benzene Nitrogen Mustard Glucoside Derivate on K562 Cells LIU Tie-mei, ZHU Guang-ze, ZHOU Jin-song, SUN Zhi and XIE Feng * (6) 762 Construction and Expression of Human Survivin and Preparation of Its Polyclonal Antibody ZHANG Hai-hong, ZHANG Xi-zhen, ZHAO Dong-hai, SHI He-liang, YU Yong-hui, WU Yong-ge, YU Xiang-hui * and KONG Wei * (6) 767 Effects of Temperature and Energy on Stability of Oligomeric Enzyme Probed on Electrospray Ionization Mass Spectrometry LI Zhi-li * (6) 771 Inhibition Mechanism of Cholinesterases by Carbamate: A Theoretical Study YAO Yuan and LI Ze-sheng * (6) 778 Electrochemical Oxidation of Ammonia on Ir Anode in Potential Fixed Electrochemical Sensor HAN Yi-ping, LUO Peng, CAI Chen-xin, XIE Lei and LU Tian-hong * (6) 782 Thermal Decomposition of Ammonium 3-Nitro-1,2,4-triazol-5-onate Monohydrate LI Ji-zhen *, FAN Xue-zhong, ZHANG Jiao-qiang, ZHANG Guo-fang and WANG Bo-zhou (6) 786 DFT Study on Intermolecular Cleavage Reaction of N-(2-Hydroxyphenyl)-phthalamic Acid ZHAO Chu-feng, TANG Ming-sheng *, WANG Hong-ming *, WEI Dong-hui, ZHAO Jing, ZHANG Shou-ren and CAO Shu-xia (6) 790 Effective VTeO/SBA-15 Catalyst Prepared by Precursor Method for the Selective Oxidation of Propane to Acrolein FENG Mao-ying, HUANG Chuan-jing, WENG Wei-zheng, WAN Hui-lin *, XU Qin and ZHOU Zhao-hui (6) 793

8 CHEM. RES. CHINESE UNIVERSITIES Vol.24 Synthesis, Crystal Structure, Physical Properties, and Application of a Series of Functional Dibenzo[d,f][1,3] dioxepine Derivatives ZHANG Hai-quan *, ZHANG Cheng-bo, ZHENG Yan, YANG Bing and MA Yu-guang * (6) 798 Preparation of 5-Fluorouracil Loaded Polylactide-co-glycolide-co-methoxy Poly(ethylene glycol)(plga- mpeg) Nanoparticles via High Speed Shearing LIN Hang, REN Hui, WANG Xi-shan *, TANG Qing-chao, TANG Jun * and WANG Ce (6) 805 Letters One-step Synthesis of ε-caprolactam by the Liquid Phase Nitrosation of Cyclohexane over the Catalysts Containing CH 3 COO or COOH MAO Li-qiu *, CHEN Lei, WU Bo-hua, YIN Du-lin, YOU Kui-yi, LIU Ping-le and LUO He-an (2) 246 Preparation and Electrode Performance of Ferrihydrites for Rechargeable Lithium Batteries WANG Hong, LAI Xiao-yong, XIA Wei, YU Ran-bo, MAO Dan, XING Chao-jian, YAO Jian-xi, WANG Dan * and LI Xiao-tian * (3) 383 Research Notes Zinc Borohydride-Ionic Liquid: a Stable and Efficient System for Reductive Reaction of Aldehydes with Primary Amines to Corresponding Secondary Amines NIAN Bao-yi *, XU Gang, WU Jiang-ping and YANG Li-rong (1) 120 Fabrication and Optical Property of Cu 7 S 4 Hollow Nanoparticles Formed Through Kirkendall Effect WANG Chen-guang, XU Zhu-de * and LIU Run (2) 249 An Efficient and Simple Reaction: Solvent-Free Preparation of Rosolic Acid Under Microwave Irradiation LI Min, ZHANG Qi-jun, YANG Jun-wei, TONG Shan-ling, YANG Ke-er, XIAO Feng-shou, K. P. Ng. Dennis * and YAN Yan * (3) 385 Reduction of Aldehydes by Fe-H 2 O-CO 2 System in Supercritical Carbon Dioxide HUANG Xi-zhe and JIANG Huan-feng * (5) 658