Institute for Electron Microscopy and Nanoanalysis Graz Centre for Electron Microscopy

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Institute for Electron Microscopy and Nanoanalysis Graz Centre for Electron Microscopy Micromechanics Ass.Prof. Priv.-Doz. DI Dr. Harald Plank a,b a Institute of Electron Microscopy and Nanoanalysis, Graz University of Technology, 8010 Graz, AUSTRIA b Graz Centre for Electron Microscopy, 8010 Graz, AUSTRIA 16 May 2017

2 Outline In this part so called Micro Electro Mechanical Systems (MEMS) are in the main focus We start with the definition what MEMS actually are Then we briefly discuss the main fabrication routes We then discuss a series of different MEMS applications by means of their operation principle Finally, we have a look on micromechanics itself to see possibilities and limitations

3 WHAT IS A MEMS?

2013 Edition 4 MEMS Definition Although the definition slightly varies, a system is called Micro-Electro-Mechanical-System if 1. the relevant part have at least one dimension D in the range 100 µm D 0.1 µm Atomic Scale Nano Scale Micro Scale Meso Scale

2013 Edition 5 MEMS Definition Although the definition varies a little, a system is called Micro-Electro-Mechanical-System if 1. the relevant part have at least one dimension D in the range 1000 µm D 0.1 µm 2. they contains actuators something IS moved by an electrical signal piezoelectric movement electrostatically driven movement

2013 Edition 6 MEMS Definition Although the definition varies a little, a system is called Micro-Electro-Mechanical-System if 1. the relevant part have at least one dimension D in the range 1000 µm D 0.1 µm 2. they contains actuators something IS moved by an electrical signal 3. they contains mechanical sensors something MOVES which is then detected electrically Thermal Mechanical sensors C Chemical Magnetic Optical Electrical

2013 Edition 7 MEMS Definition Typically, a MEMS device can not operate on its own but is mostly packaged together with an integrated circuit (IC) The IC provides an electronic interface to the sensor or actuator, signal processing / compensation, and analog and or digital output The MEMS can be integrated in two different ways 1. Monolithic integration full integration in the relevant IC chip 2. Co-integrated MEMS system is on a separate chip and packaged together with the IC sensor and relevant electronics are fully integrated sensor and relevant electronics are separated

8 NICE BUT IS THAT RELEVANT?

9 Relevance This area is very matured as it started about 55 years ago 1961 first silicon pressure sensor (Kurz et-al) 1967 resonant gate transistor (Nathanson, et-al) Beside the highly important application as nano-probe for Atomic Force Microscopy (AFM), MEMS can be found in many commercial everyday products: pressure sensors gas sensors microphones accelerometers gyroscopes digital light projectors ink jet printer cartridges micro-motor systems communication devices... and many more

10 An Intensive Example - Automotive

11 MEMS Market

12 HOW TO FABRICATE MEMS?

13 Fabrication Approaches MEMS processing iteratively uses three main processes 1. Patterning usually resist based to define the selected area fabrication of subsequent layers

14 Fabrication Approaches MEMS processing iteratively uses three main processes 1. Patterning usually resist based to define the selected area fabrication of subsequent layers 2. Deposition creation of a material film from Å up to about 100 µm Chemical gas stream reacts (condenses) on the surface Physical direct material condensation (reaction) on the surface Thin Film Deposition Physical Deposition Chemical Deposition Evaporation Sputtering Chemical Vapour Deposition Atomic Layer Deposition

15 Fabrication Approaches MEMS processing iteratively uses three main processes 1. Patterning usually resist based to define the selected area fabrication of subsequent layers 2. Deposition creation of a material film from Å up to about 100 µm Chemical gas stream reacts (condenses) on the surface Physical direct material condensation (reaction) on the surface 3. Etching removing materials on selected (patterning) or non-selected areas Wet etching solution based with high chemical selectivity Dry etching sputtering (material implantation) and / or plasma / gas approaches liquids Gaseous Directed particles

16 Fabrication Methods In MEMS microfabrication there are typical two different basic approaches 1. Bulk machining for the straightforward material removal Selective or non-selective material removal (patterning dependent) Both, physical and chemical material removing is used The latter, however, is more often used as it allows two different types Isotropic spatially homogeneous independent on the materials crystallographic structure Anisotropic different etch rates in different crystallographic orientations 2. Surface machining This process is different as it allows the fabrication of free-standing surface layers Lets have a closer look on that Gaseous Directed particles Liquids

17 Surface Micromachining for Freestanding Structures The key to fabricate free-standing regions is the introduction of a sacrificial layer, smart patterning design and a multistep fabrication procedure It starts with the introduction of the sacrificial layer This is followed by the resist layer and its patterning And is finalized by the removal of the sacrificial layer

18 Advanced Freestanding Structures Challenge: how to free only SOME parts why the others should be fixed with the substrate? While the first two steps remain the same, the buried oxide layer (lower red region) can then be removed in a second step to vertically release large structures (again the accelerometer) DC

19 Multi Level Processing A Close Look micro rotation device fixed fixed fixed movable movable

20 Multi Level Processing A Close Look micro rotation device fixed fixed fixed movable movable

21 Multi Level Processing With this approach even highly complex MEMS concept can be realized (~ 10k per 5x5 mm chip)

22 APPLICATIONS PART I

23 Atomic Force Microscopy Bulk Machining Atomic Force Microscopy (AFM) has been evolved into a standard surface analyses tool to access 3D morphology and material properties on the nanoscale The essential element, however, is the cantilever with a nanoscale tip How to fabricate that?

24 AFM - Adding Further Functionalities A smart combination of these multi-step application procedures allows integration of additional functionalities in AFM cantilever For instance, so called hollow cantilever / tips have been demonstrated for dynamic nanofluidic applications

25 AFM - Adding Further Functionalities A smart combination of these multi-step application procedures allows integration of additional functionalities in AFM cantilever For instance, so called hollow cantilever / tips have been demonstrated for dynamic nanofluidic applications

26 AFM - Adding MEMS Elements However, such systems only become MEMS if actuating and / or sensing elements are added As example, adding a thin, piezo-resistive layer enables the monolithic integration of a detection element self-sensing elements give information about the cantilever movement

27 AFM - Adding MEMS Elements In this special case, this eliminates the space consuming optical detection system Advantages are the Much more simple handling Integratability in highly space confined systems

28 Accelerometers As the name says, this type measures acceleration for application in Phones Game controllers Airbag sensors Machine vibrations Seismic activity Pedometers Inertial navigation systems RC flight components

29 Accelerometers Capacitive Basic Principle It bases on the an accelerated mass which is changes the capacity relative to neighbored electrodes easy electric detection

30 Accelerometers Capacitive Basic Principle The sensor responses 1) on the displacement x and 2) on the entailed change in the capacity C These quantities, in turn, depend on x = -m.a/k m mass; k spring constant; a acceleration C = e.a/d e dielectric constanct; A capacitance area; d separation distance (f (x) ) From that it is obvious that the design can be adapted to maximize the sensitivity via Increasing the mass m (larger proof mass body) Reducing the spring constant m (reducing the spring cross sections) Increasing the capacitance area (many, high electrodes)

C 1 C 2 31 Multi-Axis Accelerometers If the movement is now perpendicular to the before discussed direction the capacity is homogenously in- / decreasing for both C1 and C2 This can be used to enable a two axis accelerometer! C 1 = C 2 C 1 C 2

32 Multi-Axis Accelerometers If the movement is now perpendicular to the before discussed direction the capacity is homogenously in- / decreasing for both C1 and C2 This can be used to enable a two axis accelerometer! By adding a third electrode in vertical direction, a 3-axes device can be realized Real devices use large comb structures in X and Y to clearly differentiate between the X and Y

33 Accelerometers Piezoresistive Basic Principle Instead of a capacitive detection the sensing mechanism can also use the piezoelectric effect This effect bases on low concentration dopants (mostly conductive species) If the material is stressed or strained it changes its conductivity When such materials or doping zones are fabricated the right way it gives high flexibility

34 Accelerometers Piezoresistive Basic Principle Basic setup is simpler in geometry but more complex by its layer sequence

35 Accelerometers Piezoresistive Basic Principle Electric operation requires complex models

36 Accelerometers Piezoresistive Basic Principle Advantages: The overall structure is usually much simpler and smaller than for capacitive sensors The sensors usually allow high frequency sensing As the design can be done more rigid higher accelerations can be measured (up to 6000 g) Low hysteresis (compared to piezoelectric MEMS see later) Disadvantages Much more complex operation w.r.t. electric readout Environmental sensitive (T, humidity, ) Not long time stable piezoresistive capacitive

37 Accelerometers Piezoelectric Basic Principle In contrast to piezoresistivity, the piezoelectric effect is more dedicated to the crystal structures When attaching an electrode on top and on bottom, the mechanical deformation induces a voltage which can be measured (materials could be quartz, Zinc-Oxide (ZnO), Lead-Titanate (PbTiO 3 ) or Lead-free Bariumtitanate (BaTiO 3 ). The essential part, however, is that this effect can be TURNED AROUND, meaning that applying a voltage leads to mechanical deformation with sub-nanometer accuracy (very important later on)

38 Accelerometers Piezoelectric Basic Principle These sensors consist of a multi-layer structure with top and bottom electrodes and the piezoelectric material in the center

39 Accelerometers Piezoelectric Basic Principle These sensors consist of a multi-layer structure with top and bottom electrodes and the piezoelectric material in the center Once the proof mass bends the beam the piezoelectric effect causes the desired voltage However, the spatial position of the sensor is absolutely essential!

40 Accelerometers Piezoelectric Basic Principle Advantages: The design is simple and robust which minimizes fabrication efforts The sensors usually allow high frequency sensing As the design can be done more rigid higher accelerations can be measured (up to 6000 g) Disadvantages Much more complex operation w.r.t. electric readout No static measurements! Environmental sensitive (T, humidity, ) Not long time stable Hysteresis effects

41 Accelerometers Principle Comparison