SVENSK STANDARD SS-EN ISO 376. Metalliska material Kalibrering av kraftmätdon avsedda för kontroll av maskiner för enaxlig provning (ISO 376:1999)

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SVENSK STANDARD SS-EN ISO 376 Fastställd 2002-02-01 Utgåva 1 Metalliska material Kalibrering av kraftmätdon avsedda för kontroll av maskiner för enaxlig provning (ISO 376:1999) Metallic materials Calibration of force-proving instruments used for the verification of uniaxial testing machines (ISO 376:1999) ICS 77.040.10 Språk: engelska Tryckt i mars 2002 Copyright SIS. Reproduction in any form without permission is prohibited.

Europastandarden gäller som svensk standard. Detta dokument innehåller den officiella engelska versionen av. Standarden ersätter SS-EN 10002-3, utgåva 1. The European Standard has the status of a Swedish Standard. This document contains the official English version of. This standard supersedes the Swedish Standard SS-EN 10002-3, edition 1. Dokumentet består av 25 sidor. Upplysningar om sakinnehållet i standarden lämnas av SIS, Swedish Standards Institute, tel 08-555 520 00. Standarder kan beställas hos SIS Förlag AB som även lämnar allmänna upplysningar om svensk och utländsk standard. Postadress: SIS Förlag AB, 118 80 STOCKHOLM Telefon: 08-555 523 10. Telefax: 08-555 523 11 E-post: sis.sales@sis.se. Internet: www.sisforlag.se

EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM EN ISO 376 January 2002 ICS 77.040.10 Supersedes EN 10002-3:1994 English version Metallic materials - Calibration of force-proving instruments used for the verification of uniaxial testing machines (ISO 376:1999) Matériaux métalliques - Etalonnage des instruments de mesure de force utilisés pour la vérification des machines d'essais uniaxiaux (ISO 376:1999) This European Standard was approved by CEN on 26 December 2001. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2002 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. E

Page 2 Provläsningsexemplar / Preview Contents Page Foreword... 3 1 Scope...4 2 Normative reference...4 3 Principle...4 4 Characteristics of force-proving instruments...5 5 Symbols, units and designations...6 6 Calibration of the force-proving instrument...6 7 Classification of the force-proving instrument...10 8 Use of calibrated force-proving instruments...12 Annex A (informative) Example of dimensions of force transducers and corresponding loading fittings...13 Annex B (informative) Additional information...20 Bibliography...23

Page 3 Foreword The text of the International Standard from Technical Committee ISO/TC 164 "Mechanical testing of metals" of the International Organization for Standardization (ISO) has been taken over as an European Standard by Technical Committee ECISS/TC 1 "Steel - Mechanical testing", the secretariat of which is held by AFNOR. This European Standard replaces EN 10002-3:1994. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by July 2002, and conflicting national standards shall be withdrawn at the latest by July 2002. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of the International Standard ISO 376:1999 has been approved by CEN as a European Standard without any modifications.

Page 4 Provläsningsexemplar / Preview Metallic materials Calibration of force-proving instruments used for the verification of uniaxial testing machines 1 Scope This International Standard covers the calibration of force-proving instruments used for the static verification of uniaxial testing machines (e.g. tension/compression testing machines) and describes a procedure for classifying these instruments. A force-proving instrument is defined as being the whole assembly from the force transducer through to and including the indicator. This International Standard generally applies to force-proving instruments in which the force is determined by measuring the elastic deformation of a loaded member or a quantity which is proportional to it. 2 Normative reference The following normative document contains provisions which, through reference in this text, constitute provisions of this International Standard. For dated references, subsequent amendments to, or revisions of, any of these publications do not apply. However, parties to agreements based on this International Standard are encouraged to investigate the possibility of applying the most recent edition of the normative document indicated below. For undated references, the latest edition of the normative document referred to applies. Members of ISO and IEC maintain registers of currently valid International Standards. ISO 7500-1, Metallic materials Verification of static uniaxial testing machines Part 1: Tension/compression testing machines Verification and calibration of the force-measuring system. 3 Principle Calibration consists of applying precisely-known forces to the loaded member and recording the data from the deflection measuring system, which is considered an integral part of the force-proving instrument. When an electrical measurement is made, the indicator may be replaced by another indicator and the force-proving instrument need not be recalibrated provided the following conditions are fulfilled. a) The original and replacement indicators have calibration certificates traceable to national standards which give the results of calibration in terms of electrical base units (volt, ampere). The replacement indicator shall be calibrated over a range equal to or greater than the range for which it is used with the force-proving instrument and the resolution of the indicator shall be at least equal to the resolution of the indicator when it is used with the force-proving instrument. b) The units and excitation source of the replacement indicator should be respectively of the same quantity (e.g. 5 V, 10 V) and type (e.g. AC or DC carrier frequency). c) The uncertainty of each indicator (both the original and the replacement indicators) shall not influence the uncertainty of the whole assembly of the force-proving instrument. It is recommended that the uncertainty of the replacement indicator should be no greater than 1/3 of the uncertainty of the entire system.

Page 5 4 Characteristics of force-proving instruments 4.1 Identification of the force-proving instrument All the elements of the force-proving instrument (including the cables for electrical connection) shall be individually and uniquely identified, e.g. by the name of the manufacturer, the model and the serial number. For the force transducer, the maximum working force shall be indicated. 4.2 Application of force The force transducer and its loading fittings shall be designed so as to ensure axial application of force, whether in tension or compression. Examples of loading fittings are given in annex A. 4.3 Measurement of deflection Measurement of the deflection of the loaded member of the force transducer may be carried out by mechanical, electrical, optical or other means with adequate accuracy and stability. The type and the quality of the deflection measuring system determine whether the force-proving instrument is classified only for specific calibration forces or for interpolation (see clause 7). Generally, the use of force-proving instruments with dial gauges as a means of measuring the deflection is limited to the forces for which the instruments have been calibrated. The dial gauge, if used over a long travel, may contain large localised periodic errors which produce an uncertainty too great to permit interpolation between calibration forces. The dial gauge may be used for interpolation if its periodic error has a negligible influence on the interpolation error of the force-proving instrument.

Page 6 Provläsningsexemplar / Preview 5 Symbols, units and designations For the purpose of this International Standard, the symbols, units and designations given in Table 1 shall apply. Table 1 Symbols, units and designations Symbol Unit Designation a F N N Maximum capacity of the measuring range F f N Maximum capacity of the transducer i o Reading a on the indicator before application of force i f Reading a on the indicator after removal of force X Deflection with increasing test force X' Deflection with decreasing test force X r Average value of the deflections with rotation X wr Average value of deflections without rotation X max Maximum deflection X min Minimum deflection X a Computed value of deflection X N Deflection corresponding to the maximum capacity b % Relative reproducibility error with rotation b' % Relative repeatability without rotation f o % Relative zero error f c % Relative interpolation error r Resolution of the indicator v % Relative reversibility error of the force-proving instrument Reading value corresponding to the deflection. 6 Calibration of the force-proving instrument 6.1 General Before undertaking the calibration of the force-proving instrument, ensure that this instrument is able to be calibrated. This can be done by means of preliminary tests such as those defined below and given as examples. 6.1.1 Overloading test This optional test is described in clause B.1. 6.1.2 Verification relating to application of forces Ensure that the attachment system of the force-proving instrument allows axial application of the force when the instrument is used for tensile testing; that there is no interaction between the force transducer and its support on the calibration machine when the instrument is used for compression testing. Clause B.2 gives an example of a method which can be used. NOTE surface. Other methods can be used, e.g. a method using a flat-based transducer with a spherical button or upper bearing

Page 7 6.1.3 Variable voltage test This test is left to the discretion of the calibration service. For force-proving instruments requiring an electrical supply, verify that a variation of ± 10 % of the line voltage has no significant effect. This verification can be carried out by means of a force transducer simulator or by another appropriate method. 6.2 Resolution of the indicator 6.2.1 Analogue scale The thickness of the graduation marks on the scale shall be uniform and the width of the pointer shall be approximately equal to the width of a graduation mark. The resolution (r) of the indicator shall be obtained from the ratio between the width of the pointer and the centre-tocentre distance between two adjacent scale graduation marks (scale interval), the recommended ratios being 1/2, 1/5 or 1/10, a spacing of 1,25 mm or greater being required for the estimation of a tenth of the division on the scale. A vernier scale of dimensions appropriate to the analogue scale may be used to allow direct fractional reading of the instrument scale division. 6.2.2 Digital scale The resolution is considered to be one increment of the last active number on the numerical indicator, provided that the indication does not fluctuate by more than one increment with no force applied to the instrument. 6.2.3 Variation of readings If the readings fluctuate by more than the value previously calculated for the resolution (with no force applied to the instrument), the resolution shall be deemed to be equal to half the range of fluctuation. 6.2.4 Units The resolution (r) shall be converted to units of force. 6.3 Minimum force Taking into consideration the accuracy with which the deflection of the instrument may be read during calibration or during its subsequent use for verifying machines, the minimum force applied to a force-proving instrument shall comply with the two following conditions: a) the minimum force shall be greater than or equal to: 4 000 r for class 00 2 000 r for class 0,5 1 000 r for class 1 500 r for class 2 b) the minimum force shall be greater than or equal to 0,02 F f. 6.4 Calibration procedure 6.4.1 Preloading Before the calibration forces are applied, in a given mode (tension or compression), the maximum force shall be applied to the instrument three times. The duration of the application of each preload shall be between 1 min and 1,5 min.

Page 8 Provläsningsexemplar / Preview 6.4.2 Procedure The calibration shall be carried out by applying two series of calibration forces to the force-proving instrument with increasing values only, without disturbing the device. Then apply at least two further series of increasing and decreasing values. Between each of the further series of forces, the force-proving instrument shall be rotated symmetrically on its axis to positions uniformly distributed over 360 (i.e. 0, 120, 240 ). If this is not possible, it is permissible to adopt the following positions: 0, 180 and 360 (see Figure 1). For the determination of the interpolation curve, the number of forces shall be not less than eight, and these forces shall be distributed as uniformly as possible over the calibration range. NOTE 1 If a periodic error is suspected, it is recommended that intervals between the forces which correspond to the periodicity of this error should be avoided. NOTE 2 This procedure determines only the maximum hysteresis of the device. Accurate determination of the hysteresis can only be performed on dead-weight machines. The force-proving instrument shall be pre-loaded three times to the maximum force in the direction in which the subsequent forces are to be applied. When the direction of loading is changed, the maximum force shall be applied three times in the new direction. The readings corresponding to no force shall be noted after waiting at least 30 s after the force has been totally removed. NOTE 3 There should be a wait of at least 3 min between subsequent measurement series. Instruments with detachable parts shall be dismantled, as for packaging and transport, at least once during calibration. In general, this dismantling shall be carried out between the second and third series of calibration forces. The maximum force shall be applied to the force-proving instrument at least three times before the next series of forces is applied. Before starting the calibration of an electrical force-proving instrument, the zero signal may be noted (see clause B.3). 6.4.3 Loading conditions The time interval between two successive loadings shall be as uniform as possible, and no reading shall be taken at least 30 s after the start of the force change. The calibration shall be performed at a temperature stable to 1 C, this temperature shall be within the range 18 C to 28 C and shall be recorded. Sufficient time shall be allowed for the force-proving instrument to attain a stable temperature. NOTE When it is known that the force-proving instrument is not temperature compensated, care should be taken to ensure that temperature variations do not affect the calibration. Strain gauge transducers shall be energized for at least 30 min before calibration. 6.4.4 Determination of deflection A deflection is defined as the difference between a reading under force and a reading without force. NOTE This definition of deflection applies to output readings in electrical units as well as to output readings in length units.

Page 9 Figure 1 Positions of the force-proving instrument 6.5 Assessment of the force-proving instrument 6.5.1 Relative reproducibility and repeatability errors, b and b' These errors are calculated for each calibration force and in the two cases: with rotation of the proving instrument (b) and without rotation (b' ), using the following equations: where b = Xmax Xmin X r 100 X r = X1 + X3 + X5 3 where b = X2 X1 X wr 100 X wr = X1 + X2 2 6.5.2 Relative interpolation error, f c This error is determined using a first-, second-, or third-degree equation giving the deflection as a function of the calibration force. NOTE For other methods of determining this error, see the Bibliography.