Post-Healing of Defects: Alternative Way for Passivation of Carbon-Based Mesoscopic Perovskite Solar Cells via Hydrophobic Ligand Coordination
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1 Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2018 Supporting Information for Post-Healing of Defects: Alternative Way for Passivation of Carbon-Based Mesoscopic Perovskite Solar Cells via Hydrophobic Ligand Coordination Guangguang Huang, a Chunlei Wang, a Hao Zhang, b Shuhong Xu, a Qingyu Xu,*,b Yiping Cui *,a a. Advanced Photonics Center, Southeast University, Nanjing, , P. R. China b. School of Physics, Southeast University, Nanjing, , P. R. China * wangchl@seu.edu.cn, xuqingyu@seu.edu.cn, and cyp@seu.edu.cn Fig. S1 Adsorption position of ligands in different device structures. Perovskite film solar cells HTL ligand Quantum dot sensitized solar cells ligand selective modification absorber Type-Ⅰ ETL Type-Ⅱ Type-Ⅲ Fig. S2 Digital images of the triple-layer scaffold at different stages. Perovskite TOPO Front Back 1
2 Fig. S3 The PCE changes of fully printable carbon-based MPSCs with varying TOPO precursor concentration. The average PCE is collected from 10 different test points. The mm represents 10-3 mmol/ml PCE (%) TOPO concentration (mm) Fig. S4 XPS of pristine and TOPO post-treated MAPbI 3 film. 6.0x10 5 I3d 3.0x10 5 Pb4f C1s N1s O1s
3 Fig. S5 XPS results of C 1s (a), N 1s (b), I 3d (c), Pb 4f (d), O 1s (e) and P 2p (f) for pristine and TOPO post-treated MAPbI 3 film. (a) (b) (c) 2.5x x x10 4 C from TOPO Adventitious Carbon C from perovskite C1s pristine Film N1s 3x10 5 2x10 5 1x10 5 I3d (d) (e) (f) 8.0x x10 4 Pb4f 2.4x x10 4 O1s P2p 1.6x Fig. S6 Nyquist plots of devices with/without TOPO post-treatment and the equivalent circuit employed to fit the EIS spectra. The fitting results are showed in Table S Pristine TOPO Fitting for Pristine Fitting for TOPO Z'' (ohm) Z' (ohm) 3
4 Fig. S7 V oc of devices with/without TOPO post-treatment plotted against light intensity on a logarithmic scale. Normalized Voc (%) Pristine SCs +TOPO SCs Light intensity (mw/cm 2 ) Fig. S8 X-Ray Diffraction (XRD) of pristine and post-treated TOPO perovskite film. Pristine film +TOPO ligand Intensity (a.u.) * FTO + TiO2 * theta (degree) 4
5 Fig. S9 Time-resolved photoluminescence (TRPL) of pristine and TOPO post-treated MAPbI 3 film deposited on TiO 2. PL intensity (a.u.) pristine film +TOPO ligand ExpDec2 of pristine film ExpDec2 of +TOPO ligand Time (ns) Fig. S10 Atomic force microscope (AFM) images of pristine and TOPO post-treated perovskite film. (a) (b) Pristine film +TOPO ligand RMS= RMS=
6 Fig. S11 The solubility of chlorobenzene to perovskite film at different TOPO amount. The TOPO concentration used for the MPSCs is 0.001mmol/ml. The area of perovskite film in bottle is equal to the MPSCs (0.64 cm 2 ). TOPO concentration (mmol/ml) Time (h) Table. S1 The fitting results of EIS in Fig S6. Rs (Ω) Rtr (Ω) CPEtr-T CPEtr-P Rrec(Ω) CPErec-T CPErec-P Pristine E E TOPO E E Table. S2 The fitting results of TRPL in Fig S9. Function: y=a1*exp(-x/t1) + a2*exp(-x/t2) t1(ns) a1 t2(ns) a2 tavg(ns) Pristine TOPO
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