NCU/Nicolaus Copernicus University
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1 Complete denomination: Biomaterials and Cosmetics Department Location (city, country): Torun, Poland Head of Department: Alina Sionkowska Contact person in NEWGEN: Alina Sionkowska Working Group involvment: WP1 and WP2 Staff: 8 staff (1 Prof., 3 researchers) GENERAL PRESENTATION Research topics:modification of polymer properties, miscibility and physico chemical properties of polymer blends containing biopolymers i.e. collagen, chitosan, silk, elastin, keratin, cellulose, physico chemical properties of polymer composites, biopolymeric films and sponges for biomedical applications, polymeric biomaterials. Researchers expertises:preparation and characterization of materials containing biopolymers: polymer blends, composites, biomaterials Physico chemical properties: thermal properties, viscosity, rheological properties,photodegradation of materials, mechanical properties. Nicolaus Copernicus University Faculty of Chemistry Gagarin Torun - POLAND
2 Raw materials synthesis Extraction of collagen from several sources, The natural source of collagen: -Tendons -Skin (fish and mammals) -Fish scales -Other marine sources
3 Mixing of collagen solution with hydroxyapatite and homogenizaton Raw materials synthesis Scaffolds a. Collagen Processing Dissolving tail tendons of rats Freeze drying + H2O Rat tails 0.1 M CH3COOH Freeze- dried collagen 1 or 2% (w/w) collagen suspension b. Collagen/hydroxyapatite scaffold fabrication + HAp Freeze drying Porous collagen/hydroxyapatite matrix Collagen/hydroxyapatite solution in polystyrene mold Physical method Cross-linking Chemical method Add EDC/NHS Dehydrothermal treatment (DHT) 110 C, 24 h Porous Collagen/hydroxyapatite matrix in polystyrene mold Collagen/hydroxyapatite hydrogel Freeze drying Cross-linked porous collagen/hydroxyapatite matrix Cross-linked porous collagen/hydroxyapatite matrix
![Compressive modulus [kpa] NCU/Nicolaus Copernicus University Raw materials synthesis polymer blends -](/docs-images/87/97071907/images/4-4.jpg "biopolymer/synthetic polymer blends - blends of two biopolymers composites - polymer/biopolymer with")
4 Compressive modulus [kpa] NCU/Nicolaus Copernicus University Raw materials synthesis polymer blends - biopolymer/synthetic polymer blends - blends of two biopolymers composites - polymer/biopolymer with hydroxyapatite - biopolymer with montmorillonite SEM of sponge made of chitiosan, silk fibroin and nanoohydroxyapatyte 0 SF 80:20 50:50 20:80 CTS Compressive modulus of silk fibroin/chitosan blends
5 Photodegradation of materials The effects of artificial solar radiation from an Accelerated Weathering Chamber (Weatherometer) and/or UV-irradiation on the properties of biopolymeric materials. 0 UV 2h UV 8h UV AFM image of the surface of the film made of silk fibroin before and after 2 and 8 hours of irradiation
6 Acronym/name partner FACILITIES Specialized techniques available in our lab : a tensile tests Zwick&Roell 0.5, the quartz Ubbelohde capillary viscometer and Ubbelohde capillary viscometers, a mercury lamp Philips TUV 300 which emits light mainly 254 nm, the Accelerated Weathering Chamber s (Weatherometer) Suntest which produces artificial sunlight (Xenon lamp, nm) Genesis II FTIR spectrophotometer Mattson (USA) equipped in ATR device (MIRacleTM PIKE Technologies) with zinc selenide (ZnSe) crystal, the DSA10 goniometer of Krüss GmbH (Germany), equipped with software for the drop shape analysis, a rotary viscometer Bohlin Visco 88 with concentric cylinder at different temperatures (25-40 C) and shear rates ( s -1 ), differential scanning calorimeter Netzsch 204 F1 Phoenix a Shimadzu spectrophotometer (Model UV-1601PC)
7 Acronym/name partner FACILITIES Wetting: contact angles, surface free energy ( s ) and its polar ( sd ) and dispersive ( sp ) components Mechanical properties Zwick&Roell testing machine DSC 204 F1 Phoenix - Netzsch DSA10 goniometer Thermal properties: Temperature range: -180 C to 700 C Wide range of heating rates: K/min to 200 K/min Fast cooling: max. 200 K/min Very short time constant with T-sensor Extremely high sensitivity with µ-sensor Intracooler for the extended range: -85 C to 600 C Automatically controlled liquid nitrogen cooling: -180 C to 700 C TM-DSC: programming and evaluation of temperature modulated DSC tests with unique FRC correction
Katarzyna Lewandowska
RHEOLOGICAL PROPERTIES OF CHITOSAN BLENDS WITH PARTIALLY HYDROLYZED POLYACRYLAMIDE IN DIFFERENT SOLVENTS Katarzyna Lewandowska Faculty of Chemistry, Chair of Chemistry and Photochemistry of Polymers, Nicolaus
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