Cloth for High-Efficient Electrocatalytic Urea Oxidation
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1 Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2018 Supporting Information In-situ Growth of Single-Layered α-ni(oh) 2 Nanosheets on Carbon Cloth for High-Efficient Electrocatalytic Urea Oxidation Chong Lin 1,2, Zhengfei Gao 1,2, Feng Zhang 1, Jianhui Yang 2, Bin Liu 2, Jian Jin 1* 1 i-lab, CAS Key Laboratory of Nano-Bio Interface, and CAS Center for Excellence in Nanoscience, Suzhou Institute of Nano-Tech and Nano-Bionics, Chinese Academy of Sciences, Suzhou, , P. R. China. 2 Key Laboratory of Synthetic and Natural Functional Molecule Chemistry of Ministry of Education, College of Chemistry & Materials Science, Northwest University, Xi an, , P. R. China. Supplementary Figures: Figure S1. Wetting properties of water on SL Ni(OH) 2 NS/CC. A water droplet (4 μl) touches the SL Ni(OH) 2 NS modified CC, and it spreads out quickly within 31.2 ms.
2 Figure S2. SEM images of (a) and (b) ML Ni(OH) 2 NS and (c) and (d) SL Ni(OH) 2 NS, respectively. Figure S3. Calculated structures of α-ni(oh) 2 (a) and β-ni(oh) 2 (b). The corresponding interlayer distances are labeled. H atoms are intentionally removed.
3 Figure S4. XRD plots of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solutions with volume ratios (v/v) of 2/1, 1/1 and 1/2, respectively. Figure S5. (a-c) SEM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 2/1. (d-f) SEM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 1/1. (g-i) SEM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratios (v/v) of 1/2.
4 Figure S6. (a and b) TEM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 2/1. (c and d) TEM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 1/1. (e and f) TEM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 1/2. Figure S7. (a and b) AFM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 2/1. (c) corresponding height profile.
5 Figure S8. (a and b) AFM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 1/1. (c) corresponding height profile. Figure S9. (a and b) AFM images of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 1/2. (c) corresponding height profile. Figure S10. BET of Ni(OH) 2 NS prepared from CH 3 OH and H 2 O mixed solution with volume ratios (v/v) of 2/1, 1/1 and 1/2, respectively.
6 Figure S11. (a and b) SEM images of Ni(OH) 2 NS/CC prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 2/1. (c and d) SEM images of Ni(OH) 2 NS/CC prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 1/1. (e and f) SEM images of Ni(OH) 2 NS/CC prepared from CH 3 OH and H 2 O mixed solution with volume ratio (v/v) of 1/2.
7 Figure S12. TEM images of Ni(OH) 2 NS prepared from ethanol (a) and propanol (b). (c) corresponding XRD plots. Figure S13. Schematic diagram of the growth mechanism of Ni(OH) 2. Figure S14. CV plots of (a) CC, (b) ML Ni(OH) 2 /CC, and (c) SL Ni(OH) 2 NS/CC under 1M KOH and 0.33 M urea at different scan rates.
8 Figure S15. LSV plots of ML Ni(OH) 2 NS/CC prepared from CH 3 OH and H 2 O mixed solution with volume ratios (v/v) of 2/1, 1/1 and 1/2 in 1 M KOH & 0.33 M urea, respectively. Figure S16. CV plots of ML Ni(OH) 2 NS/CC prepared from CH 3 OH and H 2 O mixed solution with volume ratios (v/v) of (a) 2/1, (b) 1/1 and (c) 1/2 in 1 M KOH & 0.33 M urea at different scan rates, respectively. (d) corresponding calculated differential current vs scan rates at 0.05 V vs. Ag/AgCl, respectively.
9 Figure S17. EIS plots of ML Ni(OH) 2 NS/CC prepared from CH 3 OH and H 2 O mixed solution with volume ratios (v/v) of 2/1, 1/1 and 1/2 in 1 M KOH & 0.33 M urea, respectively. Figure S18. SEM images of ML Ni(OH) 2 /CC prepared from water after CA tests for 20,000 s.
10 Figure S19. (a) CV plots of ML Ni(OH) 2 NS/CC after CA tests for 36,000 s at different scan rates. (b) calculated differential current vs. scan rates at 0.05 V vs. Ag/AgCl. Figure S20. SEM images of CNT paper (a), Ni(OH) 2 NS/CNT paper (b and c), RGO (d), and Ni(OH) 2 NS/RGO (e and f), respectively.
11 Figure S21. TEM images of (a) and (b) reduced graphene oxide (RGO), (c) and (d) Ni(OH) 2 NS/RGO. Table S1. A summary of the performance of Ni-based catalysts for urea electrooxidation. Ni-based catalysts Electrolytes Potential/current ( V vs ma/cm 2 ) CA (ma/cm 2 vs s) References Rh-Ni foil 1 M KOH& 0.33 M urea 1.524/60 30/1 800 s at 1.4 V S1 Ni(OH) 2 tube/ni foam 1 M KOH& 0.33 M urea 1.708/ /300 s at 1568 V S2 Ni/RGO 1 M KOH& 0.33 M urea 1.5/10 9/3 600 s at 1.5 V S3 NiO NS/Ni foam 1 M KOH& 0.33 M urea 1.588/56 54/3 600 s at V S4 Ni-WC/C 1 M KOH& 0.33 M urea 1.424/42 8.5/3 600 s at V S5 Ni-WC/MWNT 1 M KOH& 0.33 M urea 1.424/48 S6 Ni 1.5Mn 1.5O 4 1 M KOH& 0.33 M urea 1.37/6.9 18/1 000 s at V S7 Metallic Ni(OH) 2 1 M KOH& 0.33 M urea 1.496/ / s at V S8 Ni-P 1 M KOH& 0.33 M urea 1.52/70 41/1 000 s at 1.52 V S9 CE-NiFe/NF 1 M KOH& 0.33 M urea 1.568/70 40/1 000 s at 1.52V S10 SL Ni(OH) 2 NS/CC 1 M KOH& 0.33 M urea 1.512/ / s at V This work References S1. Rebecca L. King, Gerardine G. Bott. Investigation of multi-metal catalysts for stable hydrogen production via urea electrolysis. J. Power Sources 2011, 196,
12 S2. Ren-Yu Ji, Der-Sheng Chan, Jiin-Jiang Jow, Mao-Sung Wu. Formation of open-ended nickel hydroxide nanotubes on three-dimensional nickel framework for enhanced urea electrolysis. Electrochem. Commun. 2013, 29, S3. Dan Wang, Wei Yan, Santosh H. Vijapur, Gerardine G. Botte. Electrochemically reduced graphene oxide nickel nanocomposites for urea electrolysis. Electrochim Acta 2013, 89, S4. Mao-Sung Wu, Guan-Wei Lin, Run-Song Yang. Hydrothermal growth of vertically-aligned ordered mesoporous nickel oxide nanosheets on three-dimensional nickel framework for electrocatalytic oxidation of urea in alkaline medium. J. Power Sources 2014, 27, S5. Lu Wang, Mingtao Li, Zhiyu Huang, Yingming Li, Suitao Qi, Chunhai Yi, Bolun Yang. Ni-WC/C nanocluster catalysts for urea electrooxidation. J. Power Sources 2014, 264, S6. Lu Wang, Tingting Du, Jin Cheng, Xing Xie, Bolun Yang, Mingtao Li. Enhanced activity of urea electrooxidation on nickel catalysts supported on tungsten carbides/carbon nanotubes. J. Power Sources 2015, 280, S7. Sivakumar Periyasamy, Palaniappan Subramanian, Elena Levi, Doron Aurbach, Aharon Gedanken, and Alex Schechter. Exceptionally Active and Stable Spinel Nickel Manganese Oxide Electrocatalysts for Urea Oxidation Reaction. ACS Appl. Mater. Interfaces 2016, 8, S8. Xiaojiao Zhu, Xinyu Dou, Jun Dai, Xingda An, Yuqiao Guo, Lidong Zhang, Shi Tao, Jiyin Zhao, Wangsheng Chu, Xiao Cheng Zeng, Changzheng Wu, and Yi Xie. Metallic Nickel Hydroxide Nanosheets Give Superior Electrocatalytic Oxidation of Urea for Fuel Cells. Angew. Chem. Int. Ed. 2016, 55, S9. Rui Ding, Xudong Li, Wei Shi, Qilei Xu, Luo Wang, Haixia Jiang, Zeng Yang, Enhui Liu. Mesoporous Ni-P nanocatalysts for alkaline urea electrooxidation. Electrochim. Acta 2016, 222, S10. Mao-Sung Wu, Chi-Yu Jao, Farn-Yih Chuang, Fang-Yi Chen. Carbon-encapsulated nickel-iron nanoparticles supported on nickel foam as a catalyst electrode for urea electrolysis. Electrochim. Acta 2017, 227,
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