Electrodes - Connect/Replace. Reagents - Install/Replace. Select method ph electrode calibration. Reagent calibration.

Transcription

1 Short-For t-form Reminders Electrodes - Connect/Replace Reagents - Install/Replace Select method ph electrode calibration Reagent calibration Running methods Running sequences Direct measurements Maintenance recommendations Storage recommendations Spare parts & accessories Electrodes Calibration standards & solutions D2T066 Printed by Radiometer Analytical SAS B Short-Form Reminders

2 Short-Form Reminders 2

3 Only one key press to check the electrodes in use! Electrodes - Connect/Replace Form no. and 2 Select method Electrodes to be connected Install electrode system GND Temp Pt-Pt Ref E Socket Electrode REF Single reference electrode TEMP Temperature sensor GND Single metal electrode Pt-Pt Double metal electrode E/E2 Other electrode types Example: phc240-a to address TIM/E (socket E on rear panel).

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5 To replace reagents, use the reagent installation procedure Reagents - Install/Replace Form no. 2 and 2 Select method Install reagent system. Enter Reagent window 3. If required, rinse burette 2. 2 then 4. Install reagent bottle and press to flush then if another reagent is already installed

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7 Straightforward method selection Select method Form no. 3 Select method. Enter main 2. 2 Select method menu from list Confirm Check icons You can run the method You can run the method. However a calibration must be performed soon Check the reagents for installation or calibration purposes. Check the electrodes and reagents for calibration purposes Programming error due to missing parameters

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9 Calibrate your electrode ph electrode calibration Form no. 4 Run calibration. Enter Electrode 2. window 3. To run the calibration 4. Enter User ID and temperature, if required, and confirm 5. Rinse electrode(s) and dip in beaker 6. The measurement starts Confirm Calibration can be performed on up to 5 buffers.

10 Automatic result display Press to save results Results: zero ph and sensitivity View statistics 2 then 2 More cycles/end of analysis Emergency stop Stop Resume analysis

11 Calibrate your reagent Reagent calibration Form no. 5 Select reagent. Enter Reagent window 2. then to select reagent from list 3. Confirm Run calibration. To run the calibration 2. Enter User ID and temperature, if required, and confirm

12 3. Enter standard amount then confirm 4. Rinse electrode(s) and dip in beaker 5. Confirm 6. The measurement starts Automatic result display Press to save result View statistics 2 then 2 Stop More tests/end of analysis Resume analysis Emergency stop

13 Run your analyses Running methods Form no. 6 Run. To run your selected method 2(*). Enter User ID and temperature, if required, and confirm 3(*). Enter Sample ID, sample amount and confirm 4(*). Rinse electrode(s) and dip electrode(s) in beaker then confirm 5. The measurement starts (*) In Run sample start = Shortcut mode, steps 2, 3 and 4 and are chained automatically:. Rinse and dip electrodes in beaker. 2. To start measurements.

14 Automatic result display (*) Press to save results (*) In Run sample end = Shortcut mode, this window does not appear and the results are displayed. View statistics (*) 2 then 2 (*) In Run sample end = Shortcut mode, this window does not appear. More tests/end of analysis (*) Running new tests/samples in Run Sample start = Shortcut mode: Rinse and dip electrodes in beaker then or 2 (*) In Run sample end = Shortcut mode, this window only appears if several sample replicates have been edited for the method. Stop Del Emergency stop Resume analysis. To resume analysis. Calculations are not performed To end an analysis before the maximum titration time or the maximum volume have been reached. Calculations are performed, if result found

15 Use your Sample stack for daily analyses Running sequences Form no. 7 Preparing the sample stack. 3 XYZ + 5. Place beaker no. onto the sample changer turntable Enter a new sample ID and confirm Repeat steps 2 to 5 for each beaker in the sequence 7. Esc then Esc 3. Check the sample test quantity or enter the sample test quantity to place in beaker no Confirm

16 Run SAC sequence. 2(*). Enter User ID and temperature, if required, confirm (*) In Run sample start = Shortcut mode, step 2 is skipped. Emergency stop Stop Resume analysis. To repeat measurements in the same beaker. Stop 2 Next analysis. To start measurements in the next beaker. Stop Del 2 End of analysis. To stop the sequence. To end an analysis before the maximum titration time or the maximum volume have been reached. Calculations are performed, if result found.

17 A? in the Electrode tab? Check your programming Direct measurements Form no. 8 Live measurements. Select method and 2 2. Connect the electrode(s). See form no. 3. Dip electrode(s) in beaker 4. Enter Electrode menu and 2 5. To select an electrode and display measurements 6. Esc To stop measurements

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19 For burette air bubble removal, run the Flush procedure Maintenance recommendations Form no. 9 Daily Check and maintain electrodes according to manufacturer recommendations. Check that there is no crystallisation at piston level, if so rinse the burette using appropriate solvent to remove crystals. If not sufficient, dismount burette to remove crystals. Check that there is no crystallisation at addition tip end that may block the reagent to pour freely, if so use appropriate solvent to remove crystals. Check the level of reagent in the reagent bottle Empty waste bottle if installed. Remove air bubbles from the burette and tubing by running a Flush procedure from the burette menu. Weekly Reagent glass cylinder piston Reagent Flush the burette with appropriate solvent to ensure complete cleaning of burette and stopcock. Change burette stand Check the piston for leakages. The burette stand must be changed when liquid can be seen between the two sealing lips. Refer to diagram.

20 Annualy Replace burette stand,, 5, 0, 25, 50 ml and the anti-diffusion tip, part. no Frequent use or use with aggressive or concentrated reagents occurring crystallisation risks may severely reduce the burette and anti-diffusion tip lifetime and may consequently require to replace them more frequently. Replace burette stand set of 3 tubing, (stands 5, 0, 25, 50 ml, part number X3T5 and stand ml, part number X3T6). Replace damaged burette accessories: bottle stopper, desiccant tubing. Contact your Radiometer Analytical representative for instrument revision and cleaning. Recommendations of use After installing new burette and/or tubing, before use, check that all tubing fittings are sufficiently tightened to prevent leakage, and that no tubings are crimped (do not over tight fittings) The reagent should be at room temperature before use in the burette. Do not leave burette installed with concentrated base, acid or salt solutions. Always rinse after use, at least daily, to increase stopcock and burette lifetime. Organic solvents: the organic solvents given as reacting with and/or destroying the VITON (Fluorinated polymer) should not be used with our burette stands (example: TetraHydroFurane). The solvents given as simply making inflate the VITON are allowed. Please contact us if you wish to work with solvents destroying the VITON.

21 Keep your system in tiptop condition! Storage recommendations Form no. 0 Daily Rinse electrodes and delivery tip throughly with distilled water after use. Store the electrode(s) following the instructions given in the respective operating instructions. Overnight and up to week In case of spillages, clean the exterior surface of the instrument with a soft cloth and tepid water. Avoid the accumulation of excess water around the keyboard area. Long-term week or more Run the Remove burette procedure from the Burette menu to remove reagent and rinse burette and tubings. If the system is to be left in the same location, store electrode(s) following the long-term storage instructions given in the respective operating instructions. If the system is to be transported, dismount the burette stand, metal rod, and cell accessories before packing. For transportation, always use the packaging supplied by the manufacturer.

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23 Ordering information at a glance Spare parts & accessories Form no. Part no. Type Description X5T025 X5T026 X5T07 X5T027 X5T028 Burette stands B50 Burette Stand, ml, UV protected with connection tubing B505 Burette Stand, 5 ml, UV protected with connection tubing B50 Burette Stand, 0 ml, UV protected with connection tubing B525 Burette Stand, 25 ml, UV protected with connection tubing B550 Burette Stand, 50 ml, UV protected with connection tubing X3T069 X3T070 X3T0 Replacement parts Delivery tubing with anti-diffusion tip Titrant bottle stopper GL45 assembly with desiccant & suction tubing Titrant bottle stopper GL45 assembly with desiccant & suction tubing for B Fuse, slow blow,.0a, (5 x 20 mm) D402, Stirring Magnet, L = 20 mm S72T004 Molecular Sieve, 250 g X3T5 Maintenance Kit of 3 tubes for B5xx (excl, B50) X3T6 Maintenance Kit of 3 tubes for B50 only Polypropylene titration vessels Titration Vessel, PP, ml (pack of 50 pcs) Titration Vessel, PP, ml (pack of 50 pcs) Titration Vessel, PP, 8-25 ml (pack of 50 pcs) Titration Vessel, PP, -9 ml (pack of 50 pcs)

24 Part no. Type Description Notebook keyboard X3T08 X6T005 X6T006 X6T007 X6T008 X6T009 X6T00 X6T0 Notebook Keyboard Mask Notebook Keyboard 83-keys, PS/2 port, US version Notebook Keyboard 83-keys, PS/2 port, French Notebook Keyboard 83-keys, PS/2 port, German Notebook Keyboard 83-keys, PS/2 port, Danish Notebook Keyboard 83-keys, PS/2 port, Spanish Notebook Keyboard 83-keys, PS/2 port, Italian Numeric Keypad, PS/2 port Balance connecting cables A95Z20 C20Z 9pf/m/25pm (Mettler PE + option 06; Mettler AE + option 02 or 0) A95Z205 C205Z 9pf/2m/25pm (Mettler PE + option 06; Mettler AE + option 02 or 0) A95Z206 C206Z m serial cable for Mettler AM, PM, SM, AT, MT, UMT, PJ, AJ A95Z202 C202Z 9bf/m/25bm (Sartorius MasterPro, QC, MP8-4) A95Z204 C204Z 9bf/2m/25bm (Sartorius MasterPro, QC, MP8-4) A95Z207 C207Z 9pf/.20m/25pm (Precisa, old models) A95Z208 C208Z 9pf/m/RJ45 (Precisa, XB series) For other balances, please consult.

25 Ordering information at a glance Electrodes Form no. 2 Part no. Type Description Combined ph/reference electrodes Acid/Base titrations E6M33 phc200-8 Combined ph electrode, Red Rod, porous pin junction E6M400 phc240-8 Combined ph electrode, Red Rod, annular junction E6M500 phc Combined ph electrode, Red Rod, epoxy body protection E6M50 phc Combined ph electrode, Red Rod, with temperature probe E6M300 phc300-8 Combined ph electrode, Ag/AgCl, porous pin junction E6M302 phc Combined ph electrode, Ag/AgCl, epoxy body protection E6M305 phc308-8 Combined ph electrode, Ag/AgCl, with temperature probe Single ph electrodes EM006 phg20-8 Glass ph electrode, ø = 7.5 mm, general purpose EM003 phg2-8 Glass ph electrode, ø = 7.5 mm, alkaline samples Combined Metal/Reference electrodes RedOx & Precipitation titrations E3M003 MC305Pt-9 Combined Platinum electrode, Ag/AgCl Ref., Screw cap * E34M004 MC609Ag-9 Combined Silver electrode, Hg/Hg 2 SO 4 Ref., Screw cap * * For use with connection cable, type CL4, part no. A94L4 Single Metal electrodes E34M003 M295Ag Silver Rod, ø = 7.5 mm, PTFE body, banana plug ** E3M00 M24Pt Platinum Plate, ø = 7.5 mm, glass body, banana plug ** ** For use with adapter, type BNC-m/Banana-f, part no. A94P807 Temperature Sensor E5M00 T20 Temperature Sensor, glass

26 Part no. Type Description Pt-Pt Metal electrodes E32M00 M23Pt2 Double platinum wire, 2 banana plugs *** E32M002 M24Pt2-8 Double platinum staples, short cable *** For use with adapter, type BNC-f/2 Banana, part no. A94P80 ISE electrodes Complexometric & Precipitation titrations E4M002 ISE25Ca Ion Selective Electrode, Calcium, Screw cap * E4M003 ISE25Cl Ion Selective Electrode, Chloride, Screw cap * E4M006 ISE25Cu Ion Selective Electrode, Copper, Screw cap * E4M007 ISE25F Ion Selective Electrode, Fluoride, Screw cap * E4M07 ISEC30F Combined Ion Selective Electrode, Fluoride, Ag/AgCl ref., Screw cap * * For use with connection cable, type CL4, part no. A94L4 Single Reference electrodes E2M009 REF20 Reference Electrode, Red Rod, ø = 7.5 mm, banana plug ** E2M0 REF40 Reference Electrode, Calomel, ø = 7.5 mm, banana plug ** E2M02 REF60 Reference Electrode, Mercurous Sulphate, ø = 7.5 mm, banana plug ** E2M00 REF25 Reference Electrode, Red Rod, double junction, banana plug ** ** For use with adapter, type BNC-m/Banana-f, part no. A94P807

27 Ordering information at a glance Calibration standards & solutions Form no. 3 Part no. Type Description IUPAC Series ph Standards SM00 ph.679 ph.679 ±0.00 at 25 C, 500 ml SM002 ph ph ±0.00 at 25 C, 500 ml SM003 ph ph ±0.00 at 25 C, 500 ml SM004 ph ph ±0.00 at 25 C, 500 ml SM005 ph 7.43 ph 7.43 ±0.00 at 25 C, 500 ml SM006 ph 9.80 ph 9.80 ±0.00 at 25 C, 500 ml SM007 ph 0.02 ph 0.02 ±0.00 at 25 C, 500 ml SM008 ph 2.45 ph 2.45 ±0.05 at 25 C, 500 ml Series SM02 ph 4 ph 4.00 at 25 C, 500 ml SM03 ph 7 ph 7.00 at 25 C, 500 ml SM04 ph 0 ph 0.00 at 25 C, 500 ml Electrode Maintenance Solutions S6M00 RENOVO N Normal Cleaning Solution, 250 ml S6M002 RENOVO X Xtra Strong Cleaning Solution, 250 ml C20C370 KS400 Pepsin in HCl Cleaning Solution, 250 ml C20C380 KS40 Thiourea Solution, 250 ml, for junction cleaning C20C300 KS00 KCl Solution, saturated, 500 ml, for Red Rod & Calomel reference C20C500 KS60 K 2 SO 4 Solution, saturated, 500 ml, for Hg/Hg 2 SO 4 reference C20C30 KS20 KCl Solution, saturated with AgCl, 500 ml, for Ag/AgCl reference S2M00 KCl C KCl Crystals, 5 g S9M00 GK ANNEX Electrode Maintenance Kit for ph & reference electrodes

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