Department of Chemical Engineering

Size: px
Start display at page:

Download "Department of Chemical Engineering"

Transcription

1 Department of Chemical Engineering Laboratory Analysis Dr. Mahar Diana Hamid Ms. Norhaya Abdul Rahim Differential Scanning Calorimeter(DCS mettler) (RM150 Thermoanalytical technique in which the difference in the amount of heat required to increase the temperature of a sample and reference is measured as a function of temperature Gas Chromatography (Agilent) (RM150 Is a common type of chromatography used in analytical chemistry for separating and analyzing compounds that can be vaporized without decomposition. TGAms (RM300 To measures the amount and rate of change in the weight of a material as a functionof temperature and time. UV Spectrophotometer To absorption spectroscopy or reflectance spectroscopy in the ultraviolet visible spectral region. Bioprocesses Loboratory Research Dr. Adeline Chua Seak May Mrs. Azira Idris Centrifuge Centrifuges work by the sedimentation principle, where the centripetal acceleration is used to separate substances of differrent densities.

2 Freezer Drayer To separate and recover volatile substances, and to purify materials Gas Chomatography Separating the different components of a mixture (the relative amounts of such components can also be determined) Image Analyser & Microscope C/W PC to see objects that are too small Ion Chromatography To analyze cations, anions and organic acids present in the water sample Total Organic Carbon Analyzer (TOC-VCSN) Determine organic carbon content in solution fluid research lab Prof. Ir. Dr. Mohd. Ali Hashim Prof. Ir. Dr. Mohd Azlan Hussain Mr. Rizman B. A. Lateff Evaporator, Rotary to control the sample temperature at desired spesification Glove Box to maintain an atmosphere less than 1 ppm O2 and 1 ppm H2O Level And Flow Process Control (teaching) to study the P.I.D controller parameters for level and flow process Table-top low speed centrifuge to mix the sample Temperature Control Pilot Plan (teaching) to study the P.I.D controller parameters for temperature and flow process Vacuum oven model VO 500 (memmert)

3 high-precision temperature control and turbo-drying Instumentation Dr. Nur Awanis Binti Hashim Ms. Norhaya Abdul Rahim BET (surface Area)micromeritic (RM250 Pore size, adsorption and desorption CHNS Analyzer (RM200 To know the component of carbon, hydrogen,nitrogen and sulfur Gas Chromatography (HP agilent) (RM150 Gas chromatography (GC), is a common type of chromatography used in analytical chemistry for separating and analyzing compounds that can be vaporized without decomposition Gas chromatography ms (Agilent) (RM250 Is a method that combines the features of gas-liquid chromatography and mass spectrometry to identify different substances within a test sample High performance Liquid Chromatography (RM150 Is a chromatographic technique used to separate a mixture of compounds in analytical chemistry and biochemistry with the purpose of identifying, quantifying and purifying the individual components of the mixture. Particle sizer (RM100 To measure sample a notion introduced for comparings dimensions of solid particles (flecks), liquid particles (droplets)

4 Pycnometer(micromeritic) (RM100 Measure Density (solid foam) Temperature Programmed Desorption (TPD) (RM150 For the method of observing desorbed molecules from a surface when the surface temperature is increased. Zeta potientiol (malvern) (RM100 Is widely used for quantification of the magnitude of the electrical charge at the double layer Lab Termodinamik Reseach Lab Prof. Dr. Mohamed Kheireddine Bin Taieb Aroua Ms. Fazizah Abdullah HPLC (High Performance Liquid Chromatrgrapy) To Identify quantity or concentration of the compound component (price : rm150 per sample) ICP (Inductivety Couple Plasma) To know Heavy metal Concentration (price : RM200 per sample) Planetary Ball Mill To destroy the sample into the most subtle particle (nano) Makmal Termodinamik ICP (Inductivety Couple Plasma) To Know Concentration for heavy metal Prof. Dr. Mohamed Kheireddine Bin Taieb Aroua Ms. Fazizah Abdullah Planetary Ball Mill To destroy the sample into the most subtle particle (Nano) mass transfer reseach lab solvent extractor to extraction the sample

5 Pasca Siswazah Lab Dr. Brahim Si Ali Mr. Muhammad Kamalrul Ariffin Bin Mohd Shariffuddin SASTEC Peristaltic Pump BT100-2J Peristaltic pumps use a custom ordering system that enables part types and sizes to be selected according to the desired application UV Spectrophotometer UviLine 9400 Measurement of absorbance and transmission Concentration measurements up to 8 standards Multi-wavelength Spektra scan with online graphic Kinetics Polymer Processing Lab For produce sample of polymer. Assoc. Prof. Dr. Rozita Yusoff High Speed Mixer For mixing resin of polymer in high speed. Tensile Kut For shaping polymer sample Two Roll Mill For mixing polymer resin in high temperature. For polymer testing & oil and gas. Dr. Badrul Hisham Bin Mohamad Jan Atmospheric Consistometer of cement. Atmospheric Consistometer of cement Creep Tester for tensile test in high temperature.

6 EP/Lubricity Tester for measuring lubricity of drilling fluid. Melt Flow Index (Teaching) for measure flow rate of polymer. of cement Atmospheric Consistometer - of cement. Dr. Badrul Hisham Bin Mohamad Jan EP/Lubricity Tester -for measuring lubricity of drilling fluid. Dr. Badrul Hisham Bin Mohamad Jan Melt Flow Index -for measure flow rate of polymer. Assoc. Prof. Dr. Rozita Yusoff Melt Flow Index -for measure flow rate of polymer. Assoc. Prof. Dr. Rozita Yusoff

7 unit operation reseach lab Prof. Ir. Dr. Abdul Aziz Bin Abdul Raman Prof. Dr. Mohamed Kheireddine Bin Taieb Aroua mixing RIG to mix the sample Mrs. Siti Fatimah Haslina Ismail Workshop fabrication,maintenance and servising for Department Of Chemical Engineering. Prof. Ir. Dr. Abdul Aziz Bin Abdul Raman Mr. Jalaluddin Hj. Ahmad Zainuddin Mr. Kamaruddin Hassan Band Saw for cutting soft metarial likes wood,plastic and polimer. boiler supply steam for teaching equipment in the pilot lab. Drilling machine for cutting and drilling work peace Lathe machine to cutting,sanding,knurling,drilli ng to the work piece Metal Arc Welding (Teaching) for welding metal Zarah Prof. Dr. Nik Meriam Binti Nik Sulaiman - For membrance setup Ms. Norhaya Abdul Rahim

Chromatography & instrumentation in Organic Chemistry

Chromatography & instrumentation in Organic Chemistry Chromatography & instrumentation in Organic Chemistry What is Chromatography? Chromatography is a technique for separating mixtures into their components in order to analyze, identify, purify, and/or quantify

More information

CHROMATOGRAPHY AND MASS SPECTROMETER

CHROMATOGRAPHY AND MASS SPECTROMETER 22 CHROMATOGRAPHY AND MASS SPECTROMETER 22.1 INTRODUCTION We know that the biochemistry or biological chemistry deals with the study of molecules present in organisms. These molecules are called as biomolecules

More information

Introduction to Pharmaceutical Chemical Analysis

Introduction to Pharmaceutical Chemical Analysis Introduction to Pharmaceutical Chemical Analysis Hansen, Steen ISBN-13: 9780470661222 Table of Contents Preface xv 1 Introduction to Pharmaceutical Analysis 1 1.1 Applications and Definitions 1 1.2 The

More information

Liquid storage: Holds the solvent which is going to act as the mobile phase. Pump: Pushes the solvent through to the column at high pressure.

Liquid storage: Holds the solvent which is going to act as the mobile phase. Pump: Pushes the solvent through to the column at high pressure. High performance liquid chromatography (HPLC) is a much more sensitive and useful technique than paper and thin layer chromatography. The instrument used for HPLC is called a high performance liquid chromatograph.

More information

SEPARATION BY BARRIER

SEPARATION BY BARRIER SEPARATION BY BARRIER SEPARATION BY BARRIER Phase 1 Feed Barrier Phase 2 Separation by barrier uses a barrier which restricts and/or enhances the movement of certain chemical species with respect to other

More information

PROPOSAL ON RATE OF CHARGES FOR USING EQUIPMENT IN CENTRALIZE LAB

PROPOSAL ON RATE OF CHARGES FOR USING EQUIPMENT IN CENTRALIZE LAB PROPOSAL ON RATE OF CHARGES FOR USING EQUIPMENT IN CENTRALIZE LAB A. Rate of s for using equipment in Lab 243 Liquid Chromatography (LC) laboratory (Reference Lecturer: Dr. Cheng Lai Hoong) Equipment 1.

More information

Glove Box / BRAUN MB 150B-G

Glove Box / BRAUN MB 150B-G Glove Box / BRAUN MB 150B-G Glove box: This box is always filled with N 2 or Ar gas without moisture, which can be perform for the measurement and/or synthetic experiments of air- and/or moisturesensitive

More information

Ionization Techniques Part IV

Ionization Techniques Part IV Ionization Techniques Part IV CU- Boulder CHEM 5181 Mass Spectrometry & Chromatography Presented by Prof. Jose L. Jimenez High Vacuum MS Interpretation Lectures Sample Inlet Ion Source Mass Analyzer Detector

More information

VALLIAMMAI ENGINEERING COLLEGE SRM Nagar, Kattankulathur

VALLIAMMAI ENGINEERING COLLEGE SRM Nagar, Kattankulathur VALLIAMMAI ENGINEERING COLLEGE SRM Nagar, Kattankulathur 603 203 DEPARTMENT OF ELECTRONICS AND INSTRUMENTATION ENGINEERING QUESTION BANK V SEMESTER EI6501 Analytical Instruments Regulation 2013 Academic

More information

HYPHENATED TECHNOLOGY GUIDE

HYPHENATED TECHNOLOGY GUIDE HYPHENATED TECHNOLOGY GUIDE TABLE OF CONTENTS TG-IR...3 Hiden Analytical MS Systems for TG-MS...4 TG-MS...5 TG-GC/MS...6 TG-IR-GC/MS...8 HYPHENATED TECHNOLOGY GUIDE Coupling, or hyphenating, two instruments

More information

Chromatographic Methods of Analysis Section 2: Planar Chromatography. Prof. Tarek A. Fayed

Chromatographic Methods of Analysis Section 2: Planar Chromatography. Prof. Tarek A. Fayed Chromatographic Methods of Analysis Section 2: Planar Chromatography Prof. Tarek A. Fayed Planar chromatography includes two types: 1- Thin Layer Chromatography (TLC). 2- Paper Chromatography (PC). Thin

More information

Supporting Information. Synthesis of Mg/ Al Layered Double Hydroxides for Adsorptive Removal of. Fluoride from Water: A Mechanistic and Kinetic Study

Supporting Information. Synthesis of Mg/ Al Layered Double Hydroxides for Adsorptive Removal of. Fluoride from Water: A Mechanistic and Kinetic Study Supporting Information Synthesis of Mg/ Al Layered Double Hydroxides for Adsorptive Removal of Fluoride from Water: A Mechanistic and Kinetic Study Gautam Kumar Sarma and Md. Harunar Rashid* Department

More information

Material Analysis Technology R&D Efforts

Material Analysis Technology R&D Efforts TECHNICAL REPORT Material Analysis Technology R&D Efforts H. KUWABARA Material analysis technology has become a core technology indispensable not only for R&D and product development but also for securing

More information

Open Column Chromatography, GC, TLC, and HPLC

Open Column Chromatography, GC, TLC, and HPLC Open Column Chromatography, GC, TLC, and HPLC Murphy, B. (2017). Introduction to Chromatography: Lecture 1. Lecture presented at PHAR 423 Lecture in UIC College of Pharmacy, Chicago. USES OF CHROMATOGRAPHY

More information

Chromatography Lab # 4

Chromatography Lab # 4 Chromatography Lab # 4 Chromatography is a method for separating mixtures based on differences in the speed at which they migrate over or through a stationary phase which means that a complex mixture will

More information

What type of samples are common? Time spent on different operations during LC analyses. Number of samples? Aims. Sources of error. Sample preparation

What type of samples are common? Time spent on different operations during LC analyses. Number of samples? Aims. Sources of error. Sample preparation What type of samples are common? Sample preparation 1 2 Number of samples? Time spent on different operations during LC analyses 3 4 Sources of error Aims Sample has to be representative Sample has to

More information

Atmospheric Analysis Gases. Sampling and analysis of gaseous compounds

Atmospheric Analysis Gases. Sampling and analysis of gaseous compounds Atmospheric Analysis Gases Sampling and analysis of gaseous compounds Introduction - External environment (ambient air) ; global warming, acid rain, introduction of pollutants, etc - Internal environment

More information

النسيف والتخثر / Bleeding and clotting الطب. علن االدوية / Pharmacology. اآلحيبء الذقيقة والونبعة Microbiology and / Immunology

النسيف والتخثر / Bleeding and clotting الطب. علن االدوية / Pharmacology. اآلحيبء الذقيقة والونبعة Microbiology and / Immunology GC-MS system Ultraviolet Fluorescence Analysis Cabinet UV-VIS Fluorescence detector LC/MS/MS system Ultrasonic Cleaner Analyzer platelet hematology analyzer Electrophoresis system (4 Units) Elisa Microplate

More information

Matter & Changes in Matter

Matter & Changes in Matter Matter & Changes in Matter Changing States- MELTING Melting- solid liquid Melting point of H20 is 32 F or 0 C Thermal energy is ABSORBED! Example: Ice cubes absorb thermal energy and melt. Changing States-

More information

Fragrances Sampling and Analysis

Fragrances Sampling and Analysis Fragrances Sampling and Analysis Picture: Roman Kaiser at field work Picture source: Givaudan Marco Stöckli, Eva Gleißner 17.11.2015 1 http://www.wysinfo.com/perfume/picts/0_wysinfo-smell%20drawing2_550_1.jpg,

More information

HYPHENATED TECHNOLOGY GUIDE

HYPHENATED TECHNOLOGY GUIDE HYPHENATED TECHNOLOGY GUIDE TABLE OF CONTENTS TG-IR...3 Hiden Analytical MS Systems for TG-MS...4 TG-MS...5 TG-GC/MS...6 TG-IR-GC/MS...8 HYPHENATED TECHNOLOGY GUIDE Coupling, or hyphenating, two instruments

More information

Medicinal Chemistry. Lab Name Location Person in Charge Programs Served Courses Served. College of Pharmacy

Medicinal Chemistry. Lab Name Location Person in Charge Programs Served Courses Served. College of Pharmacy Medicinal Chemistry Laboratories Medicinal Chemistry Lab Name Location Person in Charge Programs Served Courses Served Medicinal Chemistry M12-128 Chefa a Alhourani Nabeel Baniodeh College of Pharmacy

More information

Polymer engineering syllabus (BSc)

Polymer engineering syllabus (BSc) Polymer engineering syllabus (BSc) First semester Math 1 Physics 1 Physics 1 lab General chemistry General chemistry lab workshop Second semester Math 2 Physics 2 Organic chemistry 1 Organic chemistry

More information

ADVANCED ANALYTICAL LABORATORY

ADVANCED ANALYTICAL LABORATORY An Information Brochure on ADVANCED ANALYTICAL LABORATORY ANDHRA UNIVERSITY Visakhapatnam - 530 003 Andhra Pradesh, India Sponsored by DEPARTMENT OF SCIENCE & TECHNOLOGY Government of India New Delhi 110016

More information

X-Ray & Thermal Analysis Unit. Unit Pengurusan Makmal Universiti Blok T03 Bangunan UIRL Universiti Teknologi Malaysia Skudai Johor

X-Ray & Thermal Analysis Unit. Unit Pengurusan Makmal Universiti Blok T03 Bangunan UIRL Universiti Teknologi Malaysia Skudai Johor X-Ray & Thermal Analysis Unit Unit Pengurusan Makmal Universiti Blok T03 Bangunan UIRL Universiti Teknologi Malaysia 81310 Skudai Johor Contents Introduction Team Members Laboratory Instrument XPS XRD

More information

Introduction to Electromagnetic Radiation and Radiative Transfer

Introduction to Electromagnetic Radiation and Radiative Transfer Introduction to Electromagnetic Radiation and Radiative Transfer Temperature Dice Results Visible light, infrared (IR), ultraviolet (UV), X-rays, γ-rays, microwaves, and radio are all forms of electromagnetic

More information

x Contents 3 The Stationary Phase in Thin-Layer Chromatography Activating and Deactivating Stationary Phases Snyder s Adsorption M

x Contents 3 The Stationary Phase in Thin-Layer Chromatography Activating and Deactivating Stationary Phases Snyder s Adsorption M Contents 1 History of Planar Chromatography... 1 1.1 History of Paper Chromatography (PC)... 1 1.2 History of Thin-Layer Chromatography... 7 1.3 The History of Quantitative Planar Chromatography... 8 References.....

More information

Course goals: Course goals: Lecture 1 A brief introduction to chromatography. AM Quality parameters and optimization in Chromatography

Course goals: Course goals: Lecture 1 A brief introduction to chromatography. AM Quality parameters and optimization in Chromatography Emqal module: M0925 - Quality parameters and optimization in is a separation technique used for quantification of mixtures of analytes Svein.mjos@kj.uib.no Exercises and lectures can be found at www.chrombox.org/emq

More information

MICROSTRUCTURE-BASED PROCESS ENGINEERING AND CATALYSIS

MICROSTRUCTURE-BASED PROCESS ENGINEERING AND CATALYSIS MICROSTRUCTURE-BASED PROCESS ENGINEERING AND CATALYSIS 1 2 APPLICATION PORTFOLIO Fine chemistry We design chemical processes from lab to pilot scale in a safe, efficient and flexible way: using micro-

More information

Research Equipment in the UCA Chemistry Department

Research Equipment in the UCA Chemistry Department Research Equipment in the UCA Chemistry Department Varian 220 Atomic Absorption Spectrometer Atomic Absorption spectroscopy is used to measure the amount of a metal ion present in a solution. It is particularly

More information

The University of Jordan Accreditation & Quality Assurance Center Course Syllabus Course Name:

The University of Jordan Accreditation & Quality Assurance Center Course Syllabus Course Name: The University of Jordan Accreditation & Quality Assurance Center Course Syllabus Course Name: 1 Course title INSTRUMENTAL ANALYSIS LABORATORY 2 Course number 0303316 Credit hours (theory, practical) 1

More information

Central laboratory Instruments

Central laboratory Instruments Central laboratory Instruments (A) Chemistry and Physics Unit 1- Atomic Force Microscope (AFM) Application: Study the surface morphology of Polymer 2- Gel Permeation Chromatography (GPC) Application: Molecular

More information

Thermal Methods of Analysis Theory, General Techniques and Applications. Prof. Tarek A. Fayed

Thermal Methods of Analysis Theory, General Techniques and Applications. Prof. Tarek A. Fayed Thermal Methods of Analysis Theory, General Techniques and Applications Prof. Tarek A. Fayed 1- General introduction and theory: Thermal analysis (TA) is a group of physical techniques in which the chemical

More information

Tips & Tricks GPC/SEC: Quantify and Get More Than Molar Mass Averages

Tips & Tricks GPC/SEC: Quantify and Get More Than Molar Mass Averages Tips & Tricks GPC/SEC: Quantify and Get More Than Molar Mass Averages Daniela Held, PSS Polymer Standards Service GmbH, Mainz, Germany Gel permeation chromatography/size-exclusion chromatography (GPC/SEC)

More information

Designed polymers for purification of flavor oils

Designed polymers for purification of flavor oils Designed polymers for purification of flavor oils IFEAT Conference 2014 Rome, September 23, 2014 Ecevit Yilmaz, PhD Global Product Manager Industrial Resins MIP Technologies AB a subsidiary of Biotage

More information

Chromatography. Gas Chromatography

Chromatography. Gas Chromatography Chromatography Chromatography is essentially the separation of a mixture into its component parts for qualitative and quantitative analysis. The basis of separation is the partitioning of the analyte mixture

More information

Petroleum Thermodynamic Research Group

Petroleum Thermodynamic Research Group Petroleum Thermodynamic Research Group Labs 6-128 & 6-133 Chemical and Materials Engineering (CME) Bldg. The Petroleum Thermodynamic Research Group investigates the properties of hydrocarbon resources

More information

Photochemistry of Nitro-Polycyclic Aromatic Hydrocarbons. August 9, 2011

Photochemistry of Nitro-Polycyclic Aromatic Hydrocarbons. August 9, 2011 Photochemistry of Nitro-Polycyclic Aromatic Hydrocarbons August 9, 2011 Photochemistry focuses on the absorption of light by atoms and molecules leading to chemical reactions. With the absorption of light,

More information

Chromatography. writing in color

Chromatography. writing in color Chromatography writing in color Outlines of Lecture Chromatographic analysis» Principles and theory.» Definition.» Mechanism.» Types of chromatography.» Uses of Chromatography. In 1906 Mikhail Tswett used

More information

Lecture 15: Introduction to mass spectrometry-i

Lecture 15: Introduction to mass spectrometry-i Lecture 15: Introduction to mass spectrometry-i Mass spectrometry (MS) is an analytical technique that measures the mass/charge ratio of charged particles in vacuum. Mass spectrometry can determine masse/charge

More information

General Separation Techniques

General Separation Techniques ecture 2. Basic Separation Concepts (1) [Ch. 1] General Separation Techniques - Separation by phase creation - Separation by phase addition - Separation by barrier - Separation by solid agent - Separation

More information

CHAPTER 4 - STATES OF MATTER. Mr. Polard Physical Science Ingomar Middle School

CHAPTER 4 - STATES OF MATTER. Mr. Polard Physical Science Ingomar Middle School CHAPTER 4 - STATES OF MATTER Mr. Polard Physical Science Ingomar Middle School SECTION 1 MATTER VOCABULARY SECTION 1 Matter : anything that takes up space and has mass (pg 72, 102) Solid : Matter with

More information

Principles of Gas- Chromatography (GC)

Principles of Gas- Chromatography (GC) Principles of Gas- Chromatography (GC) Mohammed N. Sabir January 2017 10-Jan-17 1 GC is a chromatographic technique utilizes gas as the mobile phase which is usually an inert gas (Hydrogen, Helium, Nitrogen

More information

Synthesis of nano-sized anatase TiO 2 with reactive {001} facets using lamellar protonated titanate as precursor

Synthesis of nano-sized anatase TiO 2 with reactive {001} facets using lamellar protonated titanate as precursor Supporting Information Synthesis of nano-sized anatase TiO 2 with reactive {001} facets using lamellar protonated titanate as precursor Liuan Gu, Jingyu Wang *, Hao Cheng, Yunchen Du and Xijiang Han* Department

More information

METHODS FOR THE ANALYSIS OF ORGANIC CHEMISTRY ON TITAN. Thesis by. Robert Hodyss. In Partial Fulfillment of the Requirements.

METHODS FOR THE ANALYSIS OF ORGANIC CHEMISTRY ON TITAN. Thesis by. Robert Hodyss. In Partial Fulfillment of the Requirements. METHODS FOR THE ANALYSIS OF ORGANIC CHEMISTRY ON TITAN Thesis by Robert Hodyss In Partial Fulfillment of the Requirements for the Degree of Doctor of Philosophy CALIFORNIA INSTITUTE OF TECHNOLOGY Pasadena,

More information

Chapter 23 Introduction to Analytical Separations

Chapter 23 Introduction to Analytical Separations Chapter 23 Introduction to Analytical Separations Homework Due Monday April 24 Problems 23-1, 23-2, 23-7, 23-15, 23-27, 23-29, 23-32 Analytical Separations: Universal approach to analyzing complex mixtures

More information

TANDEM MASS SPECTROSCOPY

TANDEM MASS SPECTROSCOPY TANDEM MASS SPECTROSCOPY 1 MASS SPECTROMETER TYPES OF MASS SPECTROMETER PRINCIPLE TANDEM MASS SPECTROMETER INSTRUMENTATION QUADRAPOLE MASS ANALYZER TRIPLE QUADRAPOLE MASS ANALYZER TIME OF FLIGHT MASS ANALYSER

More information

Analytical Instruments

Analytical Instruments Analytical Instruments ToronTech.com About Torontech The Torontech group is proud to be a Canadian corporation headquartered in Toronto; the commercial, technical, and economic hub of Canada. With offices

More information

CHALLENGES IN MICROPLASTICS IDENTIFICATION IS ONE DETECTION METHOD ENOUGH?

CHALLENGES IN MICROPLASTICS IDENTIFICATION IS ONE DETECTION METHOD ENOUGH? CHALLENGES IN MICROPLASTICS IDENTIFICATION IS ONE DETECTION METHOD ENOUGH? ANNA ELERT, ROLAND BECKER, ERIK DÜMICHEN, PAUL EISENTRAUT, JANA FALKENHAGEN, HEINZ STURM, ULRIKE BRAUN Federal Institute for Material

More information

RESEARCH ON BENZENE VAPOR DETECTION USING POROUS SILICON

RESEARCH ON BENZENE VAPOR DETECTION USING POROUS SILICON Section Micro and Nano Technologies RESEARCH ON BENZENE VAPOR DETECTION USING POROUS SILICON Assoc. Prof. Ersin Kayahan 1,2,3 1 Kocaeli University, Electro-optic and Sys. Eng. Umuttepe, 41380, Kocaeli-Turkey

More information

Orderly Arranged Fluorescence Dyes as a Highly Efficient Chemiluminescence Resonance Energy Transfer Probe for Peroxynitrite

Orderly Arranged Fluorescence Dyes as a Highly Efficient Chemiluminescence Resonance Energy Transfer Probe for Peroxynitrite Supporting Information: Orderly Arranged Fluorescence Dyes as a Highly Efficient Chemiluminescence Resonance Energy Transfer Probe for Peroxynitrite Zhihua Wang, Xu Teng and Chao Lu* State Key Laboratory

More information

Applications of Laser Spectroscopy to Highly Sensitive Analyses

Applications of Laser Spectroscopy to Highly Sensitive Analyses G u e s t F o r u m Guest Forum Series of Lectures by Screening Committees of the Second Masao Horiba Awards Applications of Laser Spectroscopy to Highly Sensitive Analyses Cavity Ring-Down Spectroscopy

More information

Amphiphilic diselenide-containing supramolecular polymers

Amphiphilic diselenide-containing supramolecular polymers Electronic Supplementary Material (ESI) for Polymer Chemistry. This journal is The Royal Society of Chemistry 2014 Amphiphilic diselenide-containing supramolecular polymers Xinxin Tan, Liulin Yang, Zehuan

More information

-:Vijay Singh(09CEB023)

-:Vijay Singh(09CEB023) Heterogeneous Semiconductor Photocatalyst -:Vijay Singh(09CEB023) Guided by Azrina Abd Aziz Under Dr. Saravanan Pichiah Preparation of TiO 2 Nanoparticle TiO 2 was prepared by hydrolysis and poly-condensation

More information

Indium Triflate-Assisted Nucleophilic Aromatic Substitution Reactions of. Nitrosobezene-Derived Cycloadducts with Alcohols

Indium Triflate-Assisted Nucleophilic Aromatic Substitution Reactions of. Nitrosobezene-Derived Cycloadducts with Alcohols Supporting Information Indium Triflate-Assisted ucleophilic Aromatic Substitution Reactions of itrosobezene-derived Cycloadducts with Alcohols Baiyuan Yang and Marvin J. Miller* Department of Chemistry

More information

高等食品分析 (Advanced Food Analysis) I. SPECTROSCOPIC METHODS *Instrumental methods: 1. Spectroscopic methods (spectroscopy): a) Electromagnetic radiation

高等食品分析 (Advanced Food Analysis) I. SPECTROSCOPIC METHODS *Instrumental methods: 1. Spectroscopic methods (spectroscopy): a) Electromagnetic radiation *Instrumental methods: 1. Spectroscopic methods (spectroscopy): a) Electromagnetic radiation (EMR): γ-ray emission X-Ray absorption, emission, fluorescence and diffraction Vacuum ultraviolet (UV) absorption

More information

Mass Spectrometry in MCAL

Mass Spectrometry in MCAL Mass Spectrometry in MCAL Two systems: GC-MS, LC-MS GC seperates small, volatile, non-polar material MS is detection devise (Agilent 320-MS TQ Mass Spectrometer) Full scan monitoring SIM single ion monitoring

More information

TAAQI - Advanced Instrumental Techniques of Chemical Analysis

TAAQI - Advanced Instrumental Techniques of Chemical Analysis Coordinating unit: Teaching unit: Academic year: Degree: ECTS credits: 2018 205 - ESEIAAT - Terrassa School of Industrial, Aerospace and Audiovisual Engineering 714 - ETP - Department of Textile and Paper

More information

Chemistry Instrumental Analysis Lecture 37. Chem 4631

Chemistry Instrumental Analysis Lecture 37. Chem 4631 Chemistry 4631 Instrumental Analysis Lecture 37 Most analytes separated by HPLC are thermally stable and non-volatile (liquids) (unlike in GC) so not ionized easily by EI or CI techniques. MS must be at

More information

DETERMINATION OF λ max OF ANTIBIOTIC F-40 PRODUCED BY Streptomyces sulfonensis sp.nov.,

DETERMINATION OF λ max OF ANTIBIOTIC F-40 PRODUCED BY Streptomyces sulfonensis sp.nov., WORLD JOURNAL OF PHARMACY AND PHARMACEUTICAL SCIENCES Venkateswara et al. SJIF Impact Factor 6.041 Volume 5, Issue 11, 1643-1647 Research Article ISSN 2278 4357 DETERMINATION OF λ max OF ANTIBIOTIC F-40

More information

Supporting Information

Supporting Information Supporting Information Phenyl-Modified Carbon Nitride Quantum Dots with Distinct Photoluminescence Behavior Qianling Cui, Jingsan Xu,* Xiaoyu Wang, Lidong Li,* Markus Antonietti, and Menny Shalom anie_201511217_sm_miscellaneous_information.pdf

More information

COURSE DELIVERY PLAN - THEORY Page 1 of 6

COURSE DELIVERY PLAN - THEORY Page 1 of 6 COURSE DELIVERY PLAN - THEORY Page 1 of 6 Department of Applied Chemistry B.Tech: Chemical Engineering Regulation: 2013 Sub. Code / Sub. Name : CH6501 / Instrumental Methods of Analysis Unit: I LP: Sub

More information

Rational design of light-directed dynamic spheres

Rational design of light-directed dynamic spheres Electronic Supplementary Information (ESI) Rational design of light-directed dynamic spheres Yumi Okui a and Mina Han* a,b a Department of Chemistry and Department of Electronic Chemistry Tokyo Institute

More information

Far UV Absorbance Detector

Far UV Absorbance Detector Far UV Absorbance Detector Theory Most organic and inorganic species absorb strongly in the far UV. Notable exceptions are the inert gases, helium and nitrogen which absorb very weakly in this region.

More information

Figure 1. Pore size distribution

Figure 1. Pore size distribution Product Information '2:(;Ã237,325(Ã/ÃDQGÃ9 Polymeric Adsorbents Dow has developed a new polymeric adsorbent type for the concentration of organics from air and water. Key features of these adsorbents are:

More information

Questions on Instrumental Methods of Analysis

Questions on Instrumental Methods of Analysis Questions on Instrumental Methods of Analysis 1. Which one of the following techniques can be used for the detection in a liquid chromatograph? a. Ultraviolet absorbance or refractive index measurement.

More information

applied as UV protective films

applied as UV protective films Nanocomposite gels via in-situ photoinitiation and disassembly of TiO 2 -Clay composites with polymers applied as UV protective films Chuanan Liao, Qing Wu, Teng Su, Da Zhang, Qingsheng Wu and Qigang Wang*

More information

Sulfur-bubble template-mediated synthesis of uniform porous g-c 3 N 4 with superior photocatalytic performance

Sulfur-bubble template-mediated synthesis of uniform porous g-c 3 N 4 with superior photocatalytic performance Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 Electronic Supplementary Information Sulfur-bubble template-mediated synthesis of uniform porous

More information

Exercises Evaporation (page 451) 23.2 Condensation (pages )

Exercises Evaporation (page 451) 23.2 Condensation (pages ) Exercises 23.1 Evaporation (page 451) 1. The four forms in which matter exists solid, liquid, gas, and plasma are called. 2. Water that is left out in an open container will eventually. 3. Is the following

More information

4. How can fragmentation be useful in identifying compounds? Permits identification of branching not observed in soft ionization.

4. How can fragmentation be useful in identifying compounds? Permits identification of branching not observed in soft ionization. Homework 9: Chapters 20-21 Assigned 12 April; Due 17 April 2006; Quiz on 19 April 2006 Chap. 20 (Molecular Mass Spectroscopy) Chap. 21 (Surface Analysis) 1. What are the types of ion sources in molecular

More information

INTRODUCTION TO ISA SYMBOLOGY

INTRODUCTION TO ISA SYMBOLOGY ERT 213/3 Process instrumentations INTRODUCTION TO ISA SYMBOLOGY DR. RAHIMAH BINTI OTHMAN (Email: rahimah@unimap.edu.my) COURSE OUTCOMES COs 3. Able to design process instruments in bioprocess engineering

More information

Supporting Information for: Emulsion-assisted synthesis of monodisperse binary metal nanoparticles

Supporting Information for: Emulsion-assisted synthesis of monodisperse binary metal nanoparticles Supporting Information for: Emulsion-assisted synthesis of monodisperse binary metal nanoparticles Zhen Yin, Ding Ma* and Xinhe Bao* Synthesis of the PdCu nanoparticles: All synthesis was carried out under

More information

Boiling Point ( C) Boiling Point ( F)

Boiling Point ( C) Boiling Point ( F) Technical Data of Cannabinoids Solvents Chemical Formula FW (g/mol) Boiling Point ( C) Boiling Point ( F) Melting Point ( C) Density (g/ml) Solubility in Water (g/100 g) Flash Point ( C) Isopropyl alcohol

More information

Analytical techniques: Environmental samples. Lecture 2 Universidade do Algarve

Analytical techniques: Environmental samples. Lecture 2 Universidade do Algarve Analytical techniques: Environmental samples Lecture 2 Universidade do Algarve Terms, definitions & applications Difference between technique and method: Analytical technique: Fundamental scientific application

More information

Chemical Laboratory Techniques

Chemical Laboratory Techniques Unit 23: Chemical Laboratory Techniques Unit code: H/601/0355 QCF level: 4 Credit value: 15 Aim This unit gives learners the opportunity to practise and become proficient in a range of practical skills

More information

Experiment UPHPLC: Separation and Quantification of Components in Diet Soft Drinks

Experiment UPHPLC: Separation and Quantification of Components in Diet Soft Drinks Experiment UPHPLC: Separation and Quantification of Components in Diet Soft Drinks bjective: The purpose of this experiment is to quantify the caffeine content of a diet soda sample using Ultra-High Performance

More information

Physical Separations and Chromatography

Physical Separations and Chromatography Lab #5A & B: Physical Separations and Chromatography Individual Objectives: At the end of these experiments you should be able to: Ø Distinguish between Rf and tr; chromatograph and chromatogram; adsorption

More information

CHROMATOGRAPHY. The term "chromatography" is derived from the original use of this method for separating yellow and green plant pigments.

CHROMATOGRAPHY. The term chromatography is derived from the original use of this method for separating yellow and green plant pigments. CHROMATOGRAPHY The term "chromatography" is derived from the original use of this method for separating yellow and green plant pigments. THEORY OF CHROMATOGRAPHY: Separation of two sample components in

More information

Spectroscopy and Chromatography

Spectroscopy and Chromatography Spectroscopy and Chromatography Introduction Visible light is one very small part of the electromagnetic spectrum. The different properties of the various types of radiation depend upon their wavelength.

More information

HPLC Background Chem 250 F 2008 Page 1 of 24

HPLC Background Chem 250 F 2008 Page 1 of 24 HPLC Background Chem 250 F 2008 Page 1 of 24 Outline: General and descriptive aspects of chromatographic retention and separation: phenomenological k, efficiency, selectivity. Quantitative description

More information

Qualitative observation descriptive observation has no numerical measurement

Qualitative observation descriptive observation has no numerical measurement 1 Chem 047: Physical and chemical properties Chemistry 047 Properties of substances, and Physical and Chemical Changes A. Some definitions B. Properties of substances C. The Classification of Matter D.

More information

PRINCIPLE OF ICP- AES

PRINCIPLE OF ICP- AES INTRODUCTION Non- flame atomic emission techniques, which use electrothermal means to atomize and excite the analyte, include inductively coupled plasma and arc spark. It has been 30 years since Inductively

More information

Supporting Information. Size-tunable Ni nanoparticles supported on surface-modified, cage-type mesoporous

Supporting Information. Size-tunable Ni nanoparticles supported on surface-modified, cage-type mesoporous Supporting Information Size-tunable Ni nanoparticles supported on surface-modified, cage-type mesoporous silica as highly active catalysts for CO 2 hydrogenation Ching-Shiun Chen, a,b* Canggih Setya Budi,

More information

Paper: 12, Organic Spectroscopy Module: 5, Applications of UV spectroscopy

Paper: 12, Organic Spectroscopy Module: 5, Applications of UV spectroscopy Subject Chemistry Paper No and Title Module No and Title Module Tag Paper 12: Organic Spectroscopy Applications of UV-visible Spectroscopy CHE_P12_M5 TABLE OF CONTENTS 1. Learning Outcomes 2. Introduction

More information

Pharmaceutics and Pharmaceutical Technology

Pharmaceutics and Pharmaceutical Technology Pharmaceutics and Pharmaceutical Technology Pharmaceutics and Pharmaceutical Technology Laboratories Lab Name Location Person in Charge Programs Served Courses Served Pharmaceutics A M12-127 Pharmaceutics

More information

CHAPTER THREE: MATTER, PROPERTY, AND CHANGE

CHAPTER THREE: MATTER, PROPERTY, AND CHANGE CHAPTER THREE: MATTER, PROPERTY, AND CHANGE CLASSIFICATION OF MATTER! A sample of matter can be a gas, a liquid, or a solid. These three forms of matter are called the states of matter. STATES OF MATTER!

More information

Fourier Transform Infrared Spectrometry Prelab Last modified: June 17, 2014

Fourier Transform Infrared Spectrometry Prelab Last modified: June 17, 2014 Fourier Transform Infrared Spectrometry Prelab Recommended reading: AirUCI Lab Manual: Environmental Chemistry Text: FTIR Lab Pages: 6, 7, 13 16 on Light Absorption Pages: 175 177, 184, 185 on Molecular

More information

HPLC Workshop 16 June 2009 What does this do? Chromatography Theory Review Several chromatographic techniques Even though each method utilizes different techniques to separate compounds, the principles

More information

Chapter 1 and Sections

Chapter 1 and Sections Chapter 1 and Sections 3.1-3.3 Major Goals of Chapter 1: 1. Define the term chemistry. 2. Identify substances (matter) as chemicals. 3. Describe some physical and chemical properties of matter. 4. Describe

More information

Red Color CPL Emission of Chiral 1,2-DACH-based Polymers via. Chiral Transfer of the Conjugated Chain Backbone Structure

Red Color CPL Emission of Chiral 1,2-DACH-based Polymers via. Chiral Transfer of the Conjugated Chain Backbone Structure Electronic Supplementary Material (ESI) for Polymer Chemistry. This journal is The Royal Society of Chemistry 2015 Red Color CPL Emission of Chiral 1,2-DACH-based Polymers via Chiral Transfer of the Conjugated

More information

This method describes the identification of the following prohibited colorants in cosmetic products:

This method describes the identification of the following prohibited colorants in cosmetic products: A. IDENTIFICATION BY TLC 1. SCOPE AND FIELD OF APPLICATION This method describes the identification of the following prohibited colorants in cosmetic products: Names C I number Pigment Orange 5 12075 Metanil

More information

CHAPTER A2 LASER DESORPTION IONIZATION AND MALDI

CHAPTER A2 LASER DESORPTION IONIZATION AND MALDI Back to Basics Section A: Ionization Processes CHAPTER A2 LASER DESORPTION IONIZATION AND MALDI TABLE OF CONTENTS Quick Guide...27 Summary...29 The Ionization Process...31 Other Considerations on Laser

More information

Photocatalytic degradation of dyes over graphene-gold nanocomposites under visible light irradiation

Photocatalytic degradation of dyes over graphene-gold nanocomposites under visible light irradiation Photocatalytic degradation of dyes over graphene-gold nanocomposites under visible light irradiation Zhigang Xiong, Li Li Zhang, Jizhen Ma, X. S. Zhao* Department of Chemical and Biomolecular Engineering,

More information

AlCl3(aq) + 3 NaOH(aq) Al(OH)3(s) + 3 NaCl(aq)

AlCl3(aq) + 3 NaOH(aq) Al(OH)3(s) + 3 NaCl(aq) 1. Under which conditions does a real gas behave most like an ideal gas? A) at low temperatures and high pressures B) at low temperatures and low pressures C) at high temperatures and high pressures D)

More information

Introduction to Mass Spectrometry (MS)

Introduction to Mass Spectrometry (MS) Introduction to Mass Spectrometry (MS) MS Mass Spectrometry (MS) This is a very powerful analytical tool that can provide information on both molecular mass and molecular structure. Molecules come in all

More information

Methods of Separation. Vacuum Filtration. Distillation. The Physical Separation of Matter Chemistry 11 2/17/2014

Methods of Separation. Vacuum Filtration. Distillation. The Physical Separation of Matter Chemistry 11 2/17/2014 The Physical Separation of Matter Chemistry 11 Methods of Separation n Depending upon the physical properties of the substances involved, various methods of separation can be used. n Hand separation: A

More information

SCAL, Inc. Services & Capabilities

SCAL, Inc. Services & Capabilities SCAL, Inc. Services & Capabilities About Us 30 years of service 2019 marks the 30th year in operation for Midlandbased Special Core Analysis Laboratories, Inc. (SCAL, Inc.). We're proud to celebrate this

More information

Yujuan Zhou, Kecheng Jie and Feihe Huang*

Yujuan Zhou, Kecheng Jie and Feihe Huang* Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2017 A redox-responsive selenium-containing pillar[5]arene-based macrocyclic amphiphile: synthesis,

More information

INDUSTRIAL RESOURCES, INC. Power Plant Fundamentals Training

INDUSTRIAL RESOURCES, INC. Power Plant Fundamentals Training INDUSTRIAL RESOURCES, INC Power Plant Fundamentals Training Module 2 Power Plant Theory Power Plant Fundamentals Training This program is designed to provide you with a fundamental understanding of power

More information

Formation Damage Caused by Drilling Muds: A Comprehensive Study Using SEM/EDS, GC/MS and Related Instruments

Formation Damage Caused by Drilling Muds: A Comprehensive Study Using SEM/EDS, GC/MS and Related Instruments AADE-10-DF-HO-17 Formation Damage Caused by Drilling Muds: A Comprehensive Study Using SEM/EDS, GC/MS and Related Instruments S. Vincent Yang, Halliburton Copyright 2010, AADE This paper was prepared for

More information