A Research on Effect of Finishing Applications on Fabric Stiffness and Prediction of Fabric Stiffness

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Journal of Materials Science and Engineering A 8 (9-10) (2018) 190-197 doi: 10.17265/2161-6213/2018.9-10.003 D DAVID PUBLISHING A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric Alev Erenler 1 and R. Tuğrul Oğulata 2 1. Sinop University, Gerze Vocational School, Sinop 57600, Turkey 2. Çukurova University, Textile Engineering Department, Adana 01330, Turkey Abstract: In this study fabric stiffness/softness is examined which is an important element of applications on finishing processes of fabric. It is also studied the prediction of the fabric stiffness/softness with help of different parameters. Specific to this aim three different weft densitoes (30 tel/cm), 3 different yarn numbers (20/1, 24/1, 30/1 Nm) and 3 different weaving patterns were used and 27 different fabrics were weaved. During the weaving process warp yarn is 100% polyester and weft yarn is 67-33% cotton/polyester. Three different finishing processes are applied to the 27 different fabrics (softness finishing treatment, crosslinking finishing and antipilling finishing) in 3 different concentrations and at the end there are 243 sample fabrics gathered. test was applied to the samples according to the ASTM (American Society for Testing and Materials) D 4032-94 the Circular Bending Method. Test results were evaluated statistically. It was seen that the established model was related with p < 0.0001 also, Artificial Neural Network (ANN) model was formed in order to predict the fabric softness using the test results. MATLAB packet model was used in forming the model. ANN was formed with 5 inputs (fabric plait, weft yarn no, weft density, weft type, finishing concentration) and 1 output (stiffness). ANN model was established using feed forward-back propagation network. There were many trials in forming the ANN and the best results were gathered at the values established with 0.97317 regression value, 2 hidden layers and 10 neurons. Key words :Softness, stiffness, bending rigidity, artificial neural network. 1. Introduction At the result of the developing life standards and technology which affected the whole parts of the life, from now on instead of the standards of the supplies, the expectations of the demands direct not only the product but also the production process in textile sector as well as the other sectors. The recent studies show that the modern consumers meet their clothing needs to the direction in their new life style which is more dynamic and comfortable [1]. Indirectly the results of the developing life standards, consumers expect from the clothing not only covering, protecting and looking good but also feeling comfortable in the cloth at every time of the day. In this context, the descriptive factor in the consumer demand and quality Corresponding author: Alev Erenler, Ph.D., assistant Prof. Dr., research fields: textile finishing, comfort, artificial neural networks. sense was the performance features such as strength, specificity etc. beforehand but today the comfort features are important as well as performance features. Among the comfort features the most prominent features are yarn, weaving and fiber in terms of fabric handle. The resistance of the fabric against the bending is a symbol of stiffness of the fabric product [2]. In general, fabric behavior can be assessed by subjective and objective methods [3]. The stiffness value is needed to be defined in order to decide whether the fabric is being able to formed, sewed and able to evaluate the objective visualtiy of the fabric [4]. In this study, the effects of the finishing applications on the fabric stiffness/softness which are important comfort elements are examined and aimed to predict the fabric stiffness/softness via different parameters. The softness of the fabric was interpreted depending on the values of the fabric bending resistance.

A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric 191 2. Material and Method One type warp yarn was used on the fabrics produced to use in the study. In this way, the variations resulted from the warp yarn were eliminated. Warp yarn is 70/72 100% Polyester IMG yarn, weft yarn is 63-33% cotton/polyester. The weaving patterns which were used in the fabric production are 2/2 Z Twill weave, 3/1 Z Twill weave and 4/2 Z Twill weave. And the weft densities, which were used in the fabric production, are 30-32-34 yarn/cm. So, 27 kinds of fabrics were produced. In order to make the study easier the samples were numbered. The sample fabrics numerations used in the study and their features were given in Table 1. The pre-finishing applications and dying application were made under the factory standards and the finishing applications were made under the laboratory circumstances. Softness finishing process, crosslinking finishing process and antipilling finishing processes which are thought to be effective on the comfort specialties were applied at three different concentrations and at the end 243 different sample fabrics were gathered. The finishing concentrations and the inscriptions applied to the sample cloth were given in Table 2. ASTMs (American Society for Testing and Materials) were applied to the 270 total sample fabrics (in numbers as; 243 different finishing processes applied and 27 fabrics on which finishing process did not applied), grounding D 4032-94 the Circular Bending Test Method using the Circular Bending Measurement Device Digital Pneumatic Tester Device Table 1 Fabric specialties and numbers. Fabric Weaving pattern Weft yarn number Weft density Fabric number number Weaving pattern Weft yarn number Weft density 1 2/2 Z Twill 20/1 OE 30 15 3/1 Z Twill 24/1 OE 34 2 2/2 Z Twill 20/1 OE 32 16 3/1 Z Twill 30/1 OE 30 3 2/2 Z Twill 20/1 OE 34 17 3/1 Z Twill 30/1 OE 32 4 2/2 Z Twill 24/1 OE 30 18 3/1 Z Twill 30/1 OE 34 5 2/2 Z Twill 24/1 OE 32 19 4/2 Z Twill 20/1 OE 30 6 2/2 Z Twill 24/1 OE 34 20 4/2 Z Twill 20/1 OE 32 7 2/2 Z Twill 30/1 OE 30 21 4/2 Z Twill 20/1 OE 34 8 2/2 Z Twill 30/1 OE 32 22 4/2 Z Twill 24/1 OE 30 9 2/2 Z Twill 30/1 OE 34 23 4/2 Z Twill 24/1 OE 32 10 3/1 Z Twill 20/1 OE 30 24 4/2 Z Twill 24/1 OE 34 11 3/1 Z Twill 20/1 OE 32 25 4/2 Z Twill 30/1 OE 30 12 3/1 Z Twill 20/1 OE 34 26 4/2 Z Twill 30/1 OE 32 13 3/1 Z Twill 24/1 OE 30 27 4/2 Z Twill 30/1 OE 34 14 3/1 Z Twill 24/1 OE 32 Table 2 The codes of the finishing applications and the inscriptions. Finishing treatments Finishing code Softness Crosslinking Antipilling Y B A Concentration Chemicals Low (gr/lt) (W) Middle (gr/lt) (X) High (gr/lt) (Z) Arristan 91 10 20 30 ph ph 5-5.5 ph 5-5.5 ph 5-5.5 Reaknitt ZFR 50 60 70 CHT Catalyst 21 21 21 Polyavin Pen 10 10 10 ph ph 4-4.5 ph 4-4.5 ph 4-4.5 Arristan epd 30 40 50 ph ph 4.5-5 ph 4.5-5 ph 4.5-5

192 A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric [1]. Statistical analysis was made on the results data of themeasurement and ANN model were established in order to be able to make predictions on stiffness value. 3. Results and Conclusions 3.1 Statistical Analyzed Results Finishing applications were made and stiffness test was applied on the fabrics 270 total, the results were studied through variance analysis. The analysis was formed using Design Expert 6.0.8 packet program at α = 0.05 reliable level. Full Factorial analysis was preferred in establishing the statistical model. In this examination, the meaning of the items on the results was increased while the F and p values were decreasing. Besides in order to define a factor effective on a result the p values should be under the point 0.05. % contribution defines the percentage of the total variance examined in the factor. The effect of the factor on the results increases as this value increases. On the established statistical model the p value was found as p < 0.0001, this value shows that the model is meaningful. The variance results of the established model are given in Table 3. When Table 3 is examined, the most effective parameter on the softness of the fabric is seen as weft yarn number. The second most effective parameter is defined as type of the finishing process. In addition to these the matching of the items is also effective on the fabric. 3.1.1 The Diagnosis of the Established Model After the data collected from the experiment design were interpreted with the help of the variance analysis, the appropriateness of the established model should be checked. To achieve this % distribution and remnant value-experiment number graphics, the % distribution graphic is given in Fig. 1 and the remnant value-experiment number graphic is given in Fig. 2. 3.1.2 Analyzed Results When Fig. 3 is examined it is seen that finishing processes have a meaningful effect on fabric softness. Antipilling finishing applications at low level softened the 2/2 Z Twill weave, and stiffed at middle and high concentration. Besides at the end of the analysis, all fabric types became stiffed after the crosslinking finishing applications as expected at. This situation is thought because of the chemical which has resin essence. When Fig. 4 is examined, it is seen that the effect of the Antipilling applications on fabric softness depends on not only finishing concentration but also fabric pattern. Low concentrated antipilling application increases the softness of the fabric at 2/2 Z Twill weaved Table 3 Variance results of the established model. Factor F-value p-value Contribution % Model 120.43 < 0.0001 - A Weaving Pattern 160.13 < 0.0001 5.87 B Weft Yarn Number 951.51 < 0.0001 34.86 C Weft Density 170.15 < 0.0001 6.23 D Finishing Treatment 606.04 < 0.0001 33.31 E Concentration 3.81 0.0233 0.14 AB 39.57 < 0.0001 2.90 AD 17.45 < 0.0001 1.92 BC 30.69 < 0.0001 2.25 BD 42.66 < 0.0001 4.69 CD 9.71 < 0.0001 1.07 DE 14.88 < 0.0001 1.64 R 2 value 0.9487 Standard devaluation 9.085E-003 CV % 9.22

A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric 193 DESIGN-EXPERT Plot Normal Plot of Residuals 99 Normal % Probability 95 90 80 70 50 30 20 10 5 1-2.99-1.58-0.17 1.24 2.65 Studentized Residuals Fig. 1 Normal % distribution curve. DESIGN-EXPERT Plot 3.00 Residuals vs. Run Studentized Residuals 1.50 0.00-1.50-3.00 1 47 93 139 185 231 277 323 Run Number Fig. 2 Remnant value-experiment number graphic.

194 A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric DESIGN-EXPERT Plot X = D: Apre Y = E: Konsantrasyon 0.23167 Interaction Graph E: Konsantrasy on E1 W E2 X E3 Z Actual Factors A: desen = 2/2 Dimi B: Atki Iplik No = 20/1 OE C: Atki SIklIgI = 30 0.185003 0.138335 3 0.0916675 0.045 Apresiz A B Y D: Apre Fig. 3 Effect of finishing type and concentration fabric on fabric softness. DESIGN-EXPERT Plot 0.23167 Interaction Graph D: Apre X = A: desen Y = D: Apre D1 Apresiz D2 A D3 B D4 Y Actual Factors B: Atki Iplik No = 20/1 OE C: Atki SIklIgI = 30 E: Konsantrasyon = W 0.185003 0.138335 0.0916675 0.045 2/2 Dimi 3/1 Dimi 4/2 Dimi A: desen Fig. 4 Effect of finishing type and pattern on fabric softness.

A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric 195 fabric, causes no change at 3/1 Z Twill weaved fabric and stiffed the fabric of 4/2 Z Twill weaved fabric. 3.2 Model of Artificial Neural Network MATLAB packet model was used in forming the ANN model [6]. While the ANN was establishing 80% (216 pieces) of the total 270 samples were selected for education and 20% (54 pieces) were selected for test. During the education of the 216 pieces samples 70% were used for education and 15% were used for cross validation. Established model were tested with the 54 samples which it had not seen beforehand. ANN model was established using feed forward-back propagation network [7, 8]. At interception stage MSE (mean square error) was used. Ten different ANN models were established using different network parameters in order to get optimum prediction modeling. The topologies of the established models were given in Table 4. The best results were gained at the first network among the established network models. The network model of the established network was given in Fig. 5 and the regression results of the network were given in Fig. 6. When Fig. 6 is examined it can be seen the values of the established model as; for training R = 0.97112, for interception R = 0.9764, for test R = 0.9808 and the general regression value is R = 0.97317. These values show that the learning and the prediction ability of the established network model is pretty good. In Table 5, the stiffness test measurement results and specialties of some samples are selected in random method from the 216 pieces education pieces. In Table 6, the stiffness test measurement results (measured stiffness value) and specialties of some samples selected in random method from the 54 pieces training pieces selected from the firstly met samples. It was also given the prediction value formed by artificial Table 4 Network number Topologies of established YSA models. Network structure Training function Transfer function Hidden layer Neuron number 1 Trainlm Tansig 2 10 2 Trainlm Tansig 2 20 3 Trainlm Tansig 2 30 4 Trainlm Tansig 2 40 5 Trainlm Tansig 1 10 6 Trainlm Tansig 1 20 7 Trainlm Tansig 1 30 8 Trainlm Tansig 1 40 9 Trainlm Logsig 2 10 10 Trainlm Logsig 2 20 Fig. 5 The model of the established network.

196 A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric Fig. 6 Regression results. Table 5 Specialties of some fabric samples from the training group and stiffness values. Inputs Targets Fabric number Weaving pattern Weft yarn number Weft density Finishing treatments Concentrations value 16 3/1 Z Twill 30/1 OE 30 0 0 0.0600 17 3/1 Z Twill 30/1 OE 32 0 0 0.0767 19 4/2 Z Twill 20/1 OE 30 0 0 0.0920 21 4/2 Z Twill 20/1 OE 34 0 0 0.1270 22 4/2 Z Twill 24/1 OE 30 0 0 0.0653 85 2/2 Z Twill 24/1 OE 30 A z 0.1040 86 2/2 Z Twill 24/1 OE 32 A z 0.1130 88 2/2 Z Twill 30/1 OE 30 A z 0.1083 89 2/2 Z Twill 30/1 OE 32 A z 0.1003 115 2/2 Z Twill 30/1 OE 30 B w 0.0920 117 2/2 Z Twill 30/1 OE 34 B w 0.1220 118 3/1 Z Twill 20/1 OE 30 B w 0.1450 228 3/1 Z Twill 20/1 OE 34 Y x 0.0980 229 3/1 Z Twill 24/1 OE 30 Y x 0.0660 230 3/1 Z Twill 24/1 OE 32 Y x 0.0727 231 3/1 Z Twill 24/1 OE 34 Y x 0.0520

A Research on Effect of Finishing Applications on Fabric and Prediction of Fabric 197 Table 6 Specialties of the some fabric samples from the test group and predict of stiffness value. Inputs Measured Prediction Fabric number Weaving Weft yarn Finishing Weft density pattern number treatment Concentration değeri değeri 27 4/2Z Twill 30/1 OE 34 0 0 0.0677 0.067763 28 2/2 Z Twill 20/1 OE 30 A w 0.1287 0.1222 29 2/2 Z Twill 20/1 OE 32 A w 0.1483 0.15297 30 2/2 Z Twill 20/1 OE 34 A w 0.1630 0.17818 60 2/2 Z Twill 24/1 OE 34 A x 0.1193 0.11376 61 2/2 Z Twill 30/1 OE 30 A x 0.0730 0.077431 90 2/2 Z Twill 30/1 OE 34 A z 0.1140 0.11895 91 3/1 Z Twill 20/1 OE 30 A z 0.1483 0.14139 92 3/1 Z Twill 20/1 OE 32 A z 0.1537 0.14139 133 4/2Z Twill 30/1 OE 30 B w 0.0913 0.099119 134 4/2Z Twill 30/1 OE 32 B w 0.0863 0.070434 242 4/2Z Twill 30/1 OE 32 Y x 0.0607 0.065407 267 4/2Z Twill 24/1 OE 34 Y z 0.0623 0.06049 neural network model. When Table 6 is examined, real values of the test samples are closely similar to established ANN model s prediction values. This situation proves the correctness of the artificial neural network model. It is seen that it is possible to predict the fabric softness successfully with the established Artificial Neural Network Model using the fabric production parameters as inputs. Referances [1] Okur, A., Ku c u k, A. S., and Kaplan, S. 2008. Giysi Termal Konforunun Belirlenmesine Yo nelik Bir Yo ntem Gelisţirilmesi. Tu bitak Project with Project No 107M200. [2] Özdemi r, H., and Ogŭlata, R. T. 2010. Farklı Egĭrme Sistemleri I le U retilmis I pliklerin O rme Kumasļarın Egĭlme Dayanımı (Sertlik) Degĕrlerine Etkisi. Tekstil ve Konfeksiyon 4: 313-9. [3] Özgu ney, A. T., Tasķin, C., Gu rkan U nal, P., O zcȩli k, G., and O zerdem, A. 2009. Handle Properties of the Woven Fabrics Made of Compact Yarns. Tekstil ve Konfeksiyon 2: 108-13. [4] Okur, A. 1995. Pamuklu Dokuma Kumasļarın Egĭlme Direncļeri ve Do ku mlu lu k O zellikleri U zerine Bir Arasţırma. Tekstil ve Mu hendis 9: 47-8. [5] Astm, D. 2001. Standard Test Method for of Fabric by the Circular Bend Procedure. American Society for Testing and Materials, Pennsylvania, 4032-94. [6] http://www.mathworks.com/products/neural-network/ 01.04.2013. [7] Balci, O., and Ogŭlata, R. T. 2007. Prediction of the CIELab Values of the Stripped Cotton Fabrics Using Artificial Neural Network-Levenberg Marquardt Technique. In Proceedings of 6th International Conference-TEXSCI 2007, Republic of Czech-Liberec, 269-71. [8] Bhattacharjee, D., and Kothari, V. 2007. A Neural Network System for Prediction of Thermal Resistance of Textile Fabrics. Textile Research Journal 77 (1): 4-12.