ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: TE5 Product #: 395xxxxxxx Series Issue Date: June 15, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/E, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Specialist> (1) Parts, sub-materials and unit parts This document covers the TE5 RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Remarks: Please see appropriate pages as identifed in Table 1 1 Form 585-047 Rev. A 2/21/06
Table 1: List of Raw Materials covered by this report Total Parts Raw Material Part Number Raw Material Description Page(s) 1 DRKOxxx Element 3-7 2 DRCUxxx Element 8-15 3 DRAGxxx Element 16-20 4 LOZZ194 (692213) Wire-Solder 21-26 5 910-017 Cap 27-35 6 867-002 Socket with pin 36-46 7 009116 Ceramic Paper 47-53 2
Test Report Number : TWNC00294416 Applicant: Littelfuse Philippines Inc. Date : Jan 17, 2013 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Copper Nickel Alloy wires Part Number : DRKO Date Sample Received : Jan 11, 2013 Date Test Started : Jan 11, 2013 : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0294416* Page 1 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00294416 (Ⅰ) Test Result Summary: Result Test Item Unit Test Method Submitted RL samples Heavy Metal Cadmium (Cd) content ppm With reference to IEC 62321: 2008, by microwave digestion and 2 determined by ICP-OES. Lead (Pb) content ppm With reference to IEC 62321: 2008, by microwave digestion and 2 determined by ICP-OES. Mercury (Hg) content ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. 2 With reference to IEC mg/kg 62321: 2008, by boiling Chromium VI (Cr 6+ ) content with water extraction and Negative 0.02 50 cm 2 determined by UV-Vis Spectrophotometer. Remarks: ppm = parts per million based on weight of tested sample = mg/kg = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm 2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result. Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 11, 2013 Test Period : Jan 11, 2013 To Jan 15, 2013 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0294416* Page 2 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00294416 (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / Electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Negative *2 Get 50cm 2 sample Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0294416* Page 3 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00294416 Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0294416* Page 4 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00294416 Photo *THJ0294416* Page 5 of 5 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00296620 Applicant: Elschukom Elektroschutzkomponentenbau Date : Jan 30, 2013 GmbH Gewerbestrasse 87, D-98669 Veilsdorf, Germany Sample Description: One (1) group of submitted samples said to be : Sample Description :Tin plated Wires Style / Item No. :Please see page two to three. Country of Origin :Germany Date Sample Received :Jan 23, 2013 Date Test Started :Jan 23, 2013 : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0296620* Page 1 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00296620 Sample Description: Style / Item No. : (A-1)101--271.0--- tin plated copper wire Cu, Sn--% (A-2)101--283.0--- tin plated, copper plated copper nickel alloy wire Elcon30, Sn--% (A-3)101--272.0--- tin plated, copper plated steel wire ElconF, Sn--% (A-4)101--281.0--- tin plated, copper plated iron nickel alloy wire ElconD, Sn--% (A-5)101--221.0--- tin plated copper nickel alloy wire - CuNi44, Sn--% (A-6)101--24-.0--- tin plated, silver plated copper wire Cu, Ag--%, Sn--% (A-7)101--257.0--- tin plated brass wire Cu80Zn20, Sn--% Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0296620* Page 2 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00296620 Sample Description: Style / Item No. : (A-9)101--234.0--- - tin plated silver copper alloy wire AgCu90, Sn--% (ElCu90, Sn--%) (A-10)101--255.---- tin plated copper zinc alloy wire Cu70Zn30, Sn--% (A-11)101--229.---- tin plated copper nickel alloy wire CuNi12, Sn--% (A-12)101--235.---- tin plated silver copper alloy wire Ag72Cu28, Sn--% (A-13)101--231.---- tin plated silver wire Ag1000, Sn--% (A-14)101--236.---- tin plated silver copper alloy wire Ag45Cu55, Sn--%(AgCu55, Sn) (A-15)101--266.---- tin plated silver copper alloy wire AgCu70, Sn--%(ElCu70, Sn) (A-16)101--238.---- tin plated silver copper alloy wire AgCu80, Sn--%(Elcu80, Sn) (A-17)101--228.0--- tin plated tungsten wire W, Sn Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0296620* Page 3 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00296620 (Ⅰ) Test Result Summary: Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Test Item Unit Test Method Chromium VI (Cr 6+ ) content ppm ppm ppm mg/kg with 50 cm 2 With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer. Result Mixed all kinds of metal wire RL 2 37 2 2 Negative (#) 0.02 Remarks: ppm = parts per million based on weight of tested sample = mg/kg = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm 2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result. # = Due to the insufficient sample area, reduced total sample surface of 10 cm 2 was used and the dilution factor was adjusted accordingly. Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 23, 2013 Test Period : Jan 23, 2013 To Jan 29, 2013 *THJ0296620* Page 4 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00296620 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0296620* Page 5 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00296620 (Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Metal Cr 6+ Polymers / Electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Negative *2 Get 50cm 2 sample Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0296620* Page 6 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00296620 Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3,HCl,HF,H 2 O 2,H 3 BO 3 Metals HNO 3,HCl,HF Electronics HNO 3,HCl,H 2 O 2,HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0296620* Page 7 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00296620 Photo *THJ0296620* Page 8 of 8 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00282894 Applicant: Littelfuse Philippines Inc. Date : Nov 01, 2012 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Solder wire Part Number : 692213 Date Sample Received : Oct 24, 2012 Date Test Started : Oct 25, 2012 : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0282894* Page 1 of 6 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282894 (Ⅰ) Test Result Summary : Heavy Metal Test Item Result (ppm) Silvery Metal Wire Cadmium (Cd) content Lead (Pb) content 84 Mercury (Hg) content Chromium VI (Cr 6+ ) content (mg/kg with 50cm 2 ) Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected < = Less than mg/kg with 50cm 2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received : Oct 24, 2012 Test Period : Oct 25, 2012 To Nov 01, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0282894* Page 2 of 6 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282894 (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Remark: Reporting limit = Quantitation limit of analyte in sample 2 ppm 0.02 mg/kg with 50cm 2 *THJ0282894* Page 3 of 6 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282894 (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Make up with deionized water By boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0282894* Page 4 of 6 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282894 Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0282894* Page 5 of 6 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282894 Photo *THJ0282894* Page 6 of 6 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00282891 Applicant: Littelfuse Philippines Inc. Date : Oct 31, 2012 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : TRTE cap Part Number : 910-017 Date Sample Received : Oct 24, 2012 Date Test Started : Oct 25, 2012 : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0282891* Page 1 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Number : TWNC00282891 Result (ppm) Brown Plastic *THJ0282891* Page 2 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅰ) Test Result Summary : Test Item Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) Number : TWNC00282891 Result (ppm) Brown Plastic Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Oct 24, 2012 Test Period : Oct 25, 2012 To Oct 30, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0282891* Page 3 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282891 (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested 2 ppm samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested 2 ppm samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples 2 ppm are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr 6+ ) 1.0:2008 in annex C, by alkaline content digestion and determined by UV-Vis 1 ppm spectrophotometer. Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Phthalates Hexabromocyclododecane (HBCDD) With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD. Remark: Reporting limit = Quantitation limit of analyte in sample 5 ppm 5 ppm 50 ppm 50 ppm 10 ppm *THJ0282891* Page 4 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282891 (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0282891* Page 5 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅳ) Measurement Flowchart: Number : TWNC00282891 Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0282891* Page 6 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅳ) Measurement Flowchart: Number : TWNC00282891 Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0282891* Page 7 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅳ) Measurement Flowchart: Number : TWNC00282891 Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0282891* Page 8 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282891 Photo *THJ0282891* Page 9 of 9 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00316621 Applicant: Littelfuse Philippines Inc. Date : Jun 13, 2013 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Socket with pin Part Number : 867-002 Date Sample Received : Jun 05, 2013 Date Test Started : Jun 06, 2013 : As requested by the applicant, for details please refer to attached pages. Tested Components (1) Black plastic body (2) Coppery metal substrate of pin (3) Silvery plating layer of pin Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0316621* Page 1 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00316621 Test Result Summary: Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Antimony (Sb) Content Test Item Unit Test Method Chromium VI (Cr 6+ ) content Chromium VI (Cr 6+ ) content ppm ppm ppm ppm ppm mg/kg with 50 cm 2 With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to USEPA 3052, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer. With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer. Result (1) (2) (3) RL 2 2 2 -- -- 2 -- -- 1 -- Negative Negative 0.02 *THJ0316621* Page 2 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00316621 Test Item Unit Test Method Result (1) (2) (3) RL Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ppm -- -- 5 Dibrominated Biphenyls (DiBB) ppm -- -- 5 Tribrominated Biphenyls (TriBB) ppm -- -- 5 Tetrabrominated Biphenyls ppm -- -- 5 (TetraBB) With reference to IEC 62321: Pentabrominated Biphenyls ppm 2008, by solvent extraction -- -- 5 (PentaBB) and determined by GC-MS and Hexabrominated Biphenyls ppm further HPLC-DAD confirmation -- -- 5 (HexaBB) when necessary. Heptabrominated Biphenyls ppm -- -- 5 (HeptaBB) Octabrominated Biphenyls (OctaBB) ppm -- -- 5 Nonabrominated Biphenyls (NonaBB) ppm -- -- 5 Decabrominated Biphenyl (DecaBB) ppm -- -- 5 *THJ0316621* Page 3 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00316621 Test Item Unit Test Method Result (1) (2) (3) RL Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ppm -- -- 5 Dibrominated Diphenyl Ethers (DiBDE) ppm -- -- 5 Tribrominated Diphenyl Ethers (TriBDE) ppm -- -- 5 Tetrabrominated Diphenyl Ethers ppm -- -- 5 (TetraBDE) With reference to IEC 62321: Pentabrominated Diphenyl Ethers ppm 2008, by solvent extraction -- -- 5 (PentaBDE) and determined by GC-MS and Hexabrominated Diphenyl Ethers ppm further HPLC-DAD confirmation -- -- 5 (HexaBDE) when necessary. Heptabrominated Diphenyl Ethers ppm -- -- 5 (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) ppm -- -- 5 Nonabrominated Diphenyl Ethers (NonaBDE) ppm -- -- 5 Decabrominated Diphenyl Ether (DecaBDE) ppm -- -- 5 Halogen Content Fluorine (F) ppm With reference to EN -- -- 50 Chlorine (Cl) ppm 14582:2007 by calorimetric -- -- 50 bomb with oxygen and Bromine (Br) ppm -- -- 50 determined by Ion Iodine (I) ppm Chromatograph. -- -- 50 Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ppm -- -- 50 With reference to EN 14372: Dibutyl Phthalate (DBP) ppm -- -- 50 2004, by solvent extraction Benzyl Butyl Phthalate (BBP) ppm -- -- 50 and determined by GC-MS. Diisobutyl phthalate (DIBP) ppm -- -- 50 Others With reference to USEPA Hexabromocyclododecane ppm 3540C, by solvent extraction (HBCDD) and determined by GC-MS. -- -- 10 *THJ0316621* Page 4 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00316621 Remarks: ppm = parts per million based on weight of tested sample = mg/kg = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm 2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of test. Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Jun 05, 2013 Test Period : Jun 06, 2013 to Jun 13, 2013 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr 6+ ) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0316621* Page 5 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008 Number : TWNC00316621 For non-metal part Sample preparation For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Cr 6+ Cd/Pb/Hg Substrate Plating Weigh sample and add organic solvent Weigh sample and add alkaline solution For different material, digest the sample with appropriate acid *1 Cr 6+ By Soxhlet extraction or Solvent extraction Definite temp. extraction Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Concentrate the extract and make up with organic solvent Cool and filter the extract Make up with deionized water By boiling water extraction Analyzed by GC-MS Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3,HCl,HF,H2O 2,H3BO 3 Metals HNO 3,HCl,HF Electronics HNO 3,HCl,H 2 O 2,HBF 4 Analyzed by UV-VIS *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0316621* Page 6 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Measurement Flowchart: Number : TWNC00316621 Test for Heavy Metal (Sb ) Contents Reference Method:USEPA 3052 Sampling Weigh sample and digest in microwave digestion oven with suitable acid Confirm the tested samples are totally dissolved Transfer the digested solution and make up with deionized water Analyzed by ICP-OES *THJ0316621* Page 7 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Measurement Flowchart: Number : TWNC00316621 Test for Halogen Content Reference Method:EN 14582 Sampling Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0316621* Page 8 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Measurement Flowchart: Number : TWNC00316621 Test for Phthalates Contents Reference Method: EN 14372: 2004 Sampling Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MS *THJ0316621* Page 9 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Measurement Flowchart: Number : TWNC00316621 Test for Hexabromocyclododecane (HBCDD) Reference Method:USEPA 3540C Sampling Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MS *THJ0316621* Page 10 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00316621 (1) (2) (1) (2)(3) End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0316621* Page 11 of 13 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 11492 台北市內湖區瑞光路 423 號 8 樓
Test Report Number : TWNC00282889 Applicant: Littelfuse Philippines Inc. Date : Oct 31, 2012 LIMA Technology Center, Lipa City, Malvar, Batangas Sample Description: One (1) group of submitted samples said to be : Part Description : Ceramic paper Part Number : 009116 Date Sample Received : Oct 24, 2012 Date Test Started : Oct 25, 2012 : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0282889* Page 1 of 7 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Number : TWNC00282889 Result (ppm) White Ceramic Paper Remarks: ppm = Parts per million based on weight of tested sample = mg/kg = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received : Oct 24, 2012 Test Period : Oct 25, 2012 To Oct 30, 2012 *THJ0282889* Page 2 of 7 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr 6+ ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Number : TWNC00282889 Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and 2 ppm determined by ICP-OES. Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and 2 ppm Mercury (Hg) content Chromium VI (Cr 6+ ) content determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 2 ppm 1 ppm *THJ0282889* Page 3 of 7 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282889 (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS Biphenyls (PBBs) and further HPLC-DAD confirmation 5 ppm when necessary. Polybrominated Diphenyl Ethers (PBDEs) Halogen Content With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Remark: Reporting limit = Quantitation limit of analyte in sample 5 ppm 50 ppm *THJ0282889* Page 4 of 7 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282889 (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 For metal part Sample preparation For non-metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 Confirm the tested samples are totally dissolved By spot test Get 50cm 2 sample Negative *2 Weigh sample and add alkaline solution Definite temp. extraction Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3, HCl,HF,H 2 O 2, H 3 BO 3 Metals HNO 3, HCl,HF Electronics HNO 3, HCl,H 2 O 2, HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0282889* Page 5 of 7 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
(Ⅳ) Measurement Flowchart: Number : TWNC00282889 Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0282889* Page 6 of 7 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓
Number : TWNC00282889 Photo *THJ0282889* Page 7 of 7 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 114 台北市內湖區瑞光路 423 號 8 樓