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Albaha University Faculty of Engineering Mechanical Engineering g Department MEASURING INSTRUMENTS AND CALIBRATION Lecture (7) Temperature measurement By: Ossama Abouelatta o_abouelatta@yahoo.com Mechanical Engineering Department Faculty of Engineering Albaha University 2013 Measuring Instruments and Calibration Dr. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University AIMS This lecture e aims: to identify the principles of temperature measurement. to define thermoelectric effect sensors (thermocouples) and to differentiate between its types. to define varying resistance devices. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (2)

OUTLINE Principles of temperature measurement Thermoelectric effect sensors (thermocouples) Thermocouple types Thermocouple protection The thermopile Digital thermometer Varying resistance devices Resistance thermometers (resistance temperature devices) Thermistors Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (3) INTRODUCTION Temperature measurement is very important in all spheres of life and especially so in the process industries. However, it poses particular problems, since temperature measurement cannot be related to a fundamental standard of temperature in the same way that the measurement of other quantities can be related to the primary standards of mass, length and time. If two bodies of lengths l 1 and l 2 are connected together end to end, the result is a body of length l 1 + l 2. A similar ila relationship exists between een separate ate masses and separate times. However, if two bodies at the same temperature are connected together, the joined body has the same temperature as each of the original bodies. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (4)

INTRODUCTION When you measure the temperature of a body, you are measuring the intensity of heat rather than the amount of heat. The amount of heat possessed by a body at a given temperature depends on its weight and its specific heat. The specific heat of a given material is the amount of heat necessary to raise the temperature of a specific number of grams of that material 1. Specific heat can be expressed in: Calories per Pound per Degree Cli Celsius or in British Thermal Unit (BTU's) per Pound per Degree Fahrenheit. The relationship between the quantity of heat (in BTU's) and specific heat is illustrated by the following example: Example: How many BTU's are necessary to heat 5 pounds of iron from 80 to 100 F? Solution: The specific heat of iron is 0.11 BTU/1 F. Therefore, Q = m.c. T = 5 x 0.11 x (100-80) = 11 BTU s Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (5) INTRODUCTION Temperature is referred to the Hotness and the Coldness of a body. Units of temperature: Celsius degree ( C), Kelvin (K), and Fahrenheit ( F). Relationships: Fahrenheit Celsius Celsius to Kelvin: K = C + 273.15 Celsius to Fahrenheit: F = 9/5 C + 32 Fahrenheit to Celsius: C = 5/9 (F 32) Celsius Kelvin Fahrenheit Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (6)

INTRODUCTION Instruments to measure temperature can be divided into separate classes according to the physical principle on which they operate. The main principles used are: The thermoelectric effect Resistance change Sensitivity of semiconductor device Radiative heat emission Thermography Thermal expansion Resonant frequency change Sensitivity of fibre optic devices Acoustic thermometryt Color change Change of state of material. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (7) (1) THERMOELECTRIC EFFECT SENSORS (THERMOCOUPLES) Thermoelectric effect sensors rely on the physical principle that, when any two different metals are connected together, an e.m.f., mf which is a function of the temperature, is generated at the junction between the metals. The general form of this relationship is: where e is the e.m.f. generated and T is the absolute temperature. This is clearly non-linear, which is inconvenient for measurement applications. Fortunately, for certain pairs of materials, the terms involving squared and higher powers of T (a 2 T 2, a 3 T 3 etc.) are approximately zero and the e.m.f. mf temperature relationship is approximately linear according to: Wires of such pairs of materials are connected together th at one end, and in this form are known as thermocouples. Thermocouples are a very important class of device as they provide the most commonly used method of measuring temperatures in industry. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (8)

(1) THERMOELECTRIC EFFECT SENSORS (THERMOCOUPLES) Thermocouples are manufactured from various combinations of the base metals copper and iron, the base-metal alloys of alumel (Ni/Mn/Al/Si), chromel (Ni/Cr), constantan (Cu/Ni), nicrosil (Ni/Cr/Si) and nisil (Ni/Si/Mn), the noble metals platinum and tungsten, and the noble-metal alloys of platinum/rhodium and tungsten/rhenium. Only certain combinations of these are used as thermocouples and each standard combination is known by an internationally recognized type letter, for instance type K is chromel alumel. The e.m.f. temperature characteristics for some of these standard thermocouples are shown in the figure. E.m.f. temperature characteristics for some standard thermocouple materials. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (9) (1) THERMOELECTRIC EFFECT SENSORS (THERMOCOUPLES) A typical thermocouple, made from one chromel wire and one constantan wire, is shown in Figure (a). For analysis purposes, it is useful to represent the thermocouple by its equivalent electrical circuit, shown in figure (b). The e.m.f. generated at the point, where the different wires are connected together, is represented by a voltage source, E 1, and the point is known as the hot junction. The temperature of the hot junction is customarily shown as T h on the diagram. (a) Thermocouple; (b) equivalent circuit. Measuring junction Chromel Constantan Chromel Potentiometer The e.m.f. generated at the hot junction is measured at the open ends of the thermocouple, which is known as the reference junction. Ice bath Reference junction Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (10)

(I) THERMOCOUPLE TYPES The five standard base-metal thermocouples are chromel constantan (type (yp E), iron constantan (type (yp J), chromel alumel (type K), nicrosil nisil (type N) and copper constantan (type T). These are all relatively cheap to manufacture but they become inaccurate with age and have a short life. In many applications, performance is also affected through contamination by the working environment. To overcome this, the thermocouple can be enclosed in a protective sheath, but this has the adverse effect of introducing a significant time constant, making the thermocouple slow to respond to temperature changes. Therefore, as far as possible, thermocouples are used without protection. Chromel constantan devices give the highest measurement sensitivity of 80 μv/ C, with an inaccuracy of ±0.5% and a useful measuring range of -200 C up to 900 C. Unfortunately, whilst they can operate satisfactorily in oxidizing environments when unprotected, their performance and life are seriously affected by reducing atmospheres. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (11) (I) THERMOCOUPLE TYPES The five standard base-metal thermocouples are chromel constantan (type (yp E), iron constantan (type (yp J), chromel alumel (type K), nicrosil nisil (type N) and copper constantan (type T). These are all relatively cheap to manufacture but they become inaccurate with age and have a short life. In many applications, performance is also affected through contamination by the working environment. To overcome this, the thermocouple can be enclosed in a protective sheath, but this has the adverse effect of introducing a significant time constant, making the thermocouple slow to respond to temperature changes. Therefore, as far as possible, thermocouples are used without protection. Chromel constantan devices give the highest measurement sensitivity of 80 μv/ C, with an inaccuracy of ±0.5% and a useful measuring range of -200 C up to 900 C. Unfortunately, whilst they can operate satisfactorily in oxidizing environments when unprotected, their performance and life are seriously affected by reducing atmospheres. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (12)

(I) THERMOCOUPLE TYPES Iron constantan thermocouples have a sensitivity of 60 μv/ C and are the preferred type for general-purpose measurements in the temperature range -150 C to +1000 C, where the typical measurement inaccuracy is ±0.75%. Their performance is little affected by either oxidizing or reducing atmospheres. Copper constantan devices have a similar measurement sensitivity of 60 μv/ C and find their main application in measuring subzero temperatures down to -200 C C, with an inaccuracy of ±0.75%. They can also be used in both oxidising and reducing atmospheres to measure temperatures up to 350 C. Chromel alumel thermocouples have a measurement sensitivity of only 45 μv/ C, although their characteristic is particularly linear over the temperature range between 700 C and 1200 C and this is therefore their main application. Like chromel constantan constantan devices, they are suitable for oxidizing atmospheres but not for reducing ones unless protected by a sheath. Their measurement inaccuracy is ±0.75%. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (13) (I) THERMOCOUPLE TYPES Nicrosil nisil thermocouples are a recent development that resulted from attempts to improve the performance and stability of chromel alumel thermocouples. Their thermoelectric characteristic has a very similar shape to type K devices, with equally good linearity over a large temperature measurement range, measurement sensitivity of 40 μv/ C C and measurement uncertainty of ±0.75%. The operating environment limitations are the same as for chromel alumel devices but their long-term stability and life are at least three times better. Noble-metal thermocouples are always expensive but enjoy high stability and long life even when used at high h temperatures, though h they cannot be used in reducing atmospheres. Thermocouples made from platinum and a platinum rhodium alloy (type R and type S) have a low inaccuracy of only ±0.5% and can measure temperatures up to 1500 C, but their measurement sensitivity is only 10 μv/ C. Alternative devices made from tungsten and a tungsten/rhenium alloy have a better sensitivity of 20 μv/ C and can measure temperatures up to 2300 C, though they cannot be used in either oxidizing or reducing atmospheres. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (14)

(II) THERMOCOUPLE PROTECTION Thermocouples are delicate devices that must be treated carefully if their specified operating characteristics are to be maintained. One major source of error is induced strain in the hot junction. This reduces the e.m.f. output, and precautions are normally taken to minimize induced strain by mounting the thermocouple horizontally rather than vertically. Common sheath materials for thermocouples Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (15) (III) THE THERMOPILE The thermopile is the name given to a temperature-measuring device that consists of several thermocouples connected together in series, such that all the reference junctions are at the same cold temperature and all the hot junctions are exposed to the temperature being measured, as shown in the shown figure. Thermopile Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (16)

(V) DIGITAL THERMOMETER Thermocouples are also used in digital thermometers, of which both simple and intelligent versions exist. A simple digital thermometer is the combination of a thermocouple, a battery-powered, dual slope digital it voltmeter to measure the thermocouple output, and an electronic display. This provides a low noise, digital output that can resolve temperature differences as small as 0.1 C. The accuracy achieved is dependent on the accuracy of the thermocouple element, but reduction of measurement inaccuracy to ±0.5% is achievable. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (17) (2) VARYING RESISTANCE DEVICES Varying resistance devices rely on the physical principle of the variation of resistance with temperature. t The devices are known as either resistance thermometers or thermistors according to whether the material used for their construction is a metal or a semiconductor, and both are common measuring devices. The normal method of measuring resistance is to use a d.c. bridge. The excitation voltage of the bridge has to be chosen very carefully because, although a high value is desirable for achieving high measurement sensitivity, the selfheating effect of high currents flowing in the temperature transducer creates an error by increasing the temperature of the device and so changing the resistance value. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (18)

(I) RESISTANCE THERMOMETERS Resistance thermometers, which are alternatively known as resistance temperature devices (or RTDs), rely on the principle that the resistance of a metal varies with temperature according to the relationship: This equation is non-linear and so is inconvenient for measurement purposes. The equation becomes linear if all the terms in a 2 T 2 and higher powers of T are negligible such that the resistance and temperature are related according to: Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (19) (I) RESISTANCE THERMOMETERS This equation is approximately true over a limited temperature range for some metals, notably platinum, copper and nickel, whose characteristics are summarized in the figure. Typical resistance temperature characteristic s of metals. The working range of each of these four types of resistance thermometer is as shown below: Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (20)

(II) THERMISTORS Thermistors are manufactured from beads of semiconductor material prepared from oxides of the iron group of metals such as chromium, cobalt, iron, manganese and nickel. Normally, thermistors have a negative temperature coefficient, i.e. the resistance decreases as the temperature increases, according to: The major advantages of thermistors are their relatively low cost and their small size. Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (21) THANK YOU Ossama Abouelatta Mechanical Engineering Department Faculty of Engineering i Albaha University Albaha, KSA email: o_abouelatta@yahoo.com Assoc. Prof. Ossama Abouelatta, Department of Mechanical Engineering, Faculty of Engineering, Albaha University (22)