No. KE/2016/52417 Date 2016/05/26 Page 1 of 6 The following sample(s) was/were submitted and identified by/on behalf of the client as Sample Description Style/Item No. Material Component Color Sample Receiving Date Testing Period Sample Submitted By PVC JWS60 PVC WHITE 2016/05/23 2016/05/23 TO 2016/05/26 ============================================================================================ Test Requested Test Method Test Result(s) Conclusion As specified by client, with reference to RoHS Directive 2011/65/EU Annex II to determine Cadmium, Lead, Mercury, Cr(VI), PBBs, PBDEs contents in the submitted sample. Please refer to next pages. Please refer to next page(s). Based on the performed tests on submitted samples, the test results of Cadmium, Lead, Mercury, Cr(VI), PBBs, PBDEs comply with the limits as set by RoHS Directive 2011/65/EU Annex II; recasting 2002/95/EC.
No. KE/2016/52417 Date 2016/05/26 Page 2 of 6 Test Result(s) PART NAME No.1 Test Item(s) Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether WHITE PVC POWDER Unit mg/kg With reference to IEC 62321-5 2013 and performed by ICP-AES. mg/kg With reference to IEC 62321-5 2013 and performed by ICP-AES. mg/kg With reference to IEC 62321-4 2013 and performed by ICP-AES. mg/kg Method With reference to IEC 62321 2008 and performed by UV-VIS. MDL Result No.1 Limit 2 n.d. 100 2 n.d. 1000 2 n.d. 1000 2 n.d. 1000 mg/kg - n.d. 1000 mg/kg With reference to IEC 62321-6 2015 5 n.d. - mg/kg and performed by GC/MS. - n.d. 1000
No. KE/2016/52417 Date 2016/05/26 Page 3 of 6 Note 1. mg/kg = ppm;0.1wt% = 1000ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. " - " = Not Regulated 5. This report supersedes all previous documents bearing the test report number KA/201X/XXXXX. 6. This is the additional test report of KA/201X/XXXXX which was issued on yyyy/mm/dd. Please refer to KA/201X/XXXXX for original information.
No. KE/2016/52417 Date 2016/05/26 Page 4 of 6 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr6+ test method excluded) 2) Name of the person who made measurement Jony Liu 3) Name of the person in charge of measurement Ray Chang Cutting / Preparation Sample Measurement Pb Cd Hg Cr 6+ Acid digestion by suitable acid depended on different sample material (as below table) Microwave digestion with HNO 3 /HCl/HF Add appropriate amount of digestion reagent Filtration Heat to appropriate temperature to extract Solution Residue Cool, filter digestate through filter 1) Alkali Fusion 2) HCl to dissolve ICP-AES Sample Material Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2O 2 Add diphenyl-carbazide for color development Measure the absorbance at 540 nm by UV-VIS Glass Gold, platinum, palladium, ceramic HNO 3/HF Aqua regia Silver HNO 3 Plastic Others H 2SO 4, H 2O 2, HNO 3, HCl Any acid to total digestion Note**(1) For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2) For metallic material, add pure water and heat to boiling.
No. KE/2016/52417 Date 2016/05/26 Page 5 of 6 PBB/PBDE analytical FLOW CHART 1) Name of the person who made measurement Dorothy Chen 2) Name of the person in charge of measurement Ray Chang Sample Sample pretreatment Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report
No. KE/2016/52417 Date 2016/05/26 Page 6 of 6 * The tested sample / part is marked by an arrow if it's shown on the photo. * ** End of Report **