SPES secondary beam planning

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SPES secondary beam planning A. Andrighetto INFN Laboratori di Legnaro SPES Workshop LNL, October 10th, 2016

Talk Overview I. SPES construction phases & +1 L.E. line planning II. Status of the RIB sistem III. First beam for users IV. Conclusion

3) Post acceleration area Project construction phases Exp. areas 1) RIB production area ALPI MRMS HRMS XTU-Tandem Phase 3 RFQ PIAVE CB Phase 2. Phase 3. Beam cooler 2) Beam Manipulation area 1+ Exp. areas Target LRMS Phase 2. Phase 1. Cyclotron Phase 1. 2016 - Building + First operation with the cyclotron NOW! Phase 2. 2017-19 - From C.B. to RFQ + SPES target, LRMS, 1+ Beam Lines Phase 3. 2019-20 - From the LRMS to the CB + rom RFQ to ALPI

The Low Energy 1+ beam line ( TIS Tape System ) 1+ line - A5 room TAPE SYSTEM MAGNETIC DIPOLE TRIPLET of QUADRUPOLES ELECTROSTATIC DIPOLE FRONT END WIEN FILTER Bunker A6 room Goal: To Have first no-accelerated RIB before end 2019

Working plan for the 1+ (TIS tape system) Working plan and follow-up for the three main issues listed below: 1) Bunker beam line (proton & RIB) 2) 1+ beam line 3) SPES ISOL laboratories operation Milestone 2019: first low intensity RIB @ SPES

Planning of Bunker beam line service plants to hubs (hydraulic, electrical, ) within January-April July-August May-June September the end 2018 of of 2018 2016 2017 A6 room BD mechanical installations vacuum service plants from hubs to the main apparatus controls & power supplies contingency & tests September 2018 June 2019

Planning of 1+ beam line within design the phase end of 2017 within November-December January-October 2018 January-February June 2017 2019 2018 March 2019 bunker A6 service plants to hubs (hydraulic, electrical, ) mechanical installations vacuum service plants from hubs to the main apparatus controls & power supplies CONSTRUCTION design phase for the & specific components INSTALLATION contingency & tests March June 2019

1+ beam line operation (from TIS to tape system) WIP for the specific 1+ beam line components magnetic dipole electrostatic triplet of quads tape system beam diagnostic box electrostatic dipole

Future Implementations Electrostatic dipoles Tape station for beam characterization SPES configuration means: - (almost) complete renewal of the cryogenic plant. - Laser tracking beamline alignment - Added new cavities Low intensity beam monitors MCP & grid beam monitor Low Energy Experimental Room (not financed yet) Alberto Andrighetto Alberto Andrighetto III SPES workshop: 10th October SPES workshop 2016 2016

Stautus of the RIB complex

The SPES TIS complex protons Fission fragments Ions Extraction Electrode (GND) Hot Transfer Line Ion Source (up to +40 kv) 8kW proton beam 7 UCx target discs

The OFF-LINE fron-end

Laboratories & Organization WG1: TIS WG2: Materials WG3: Laser WG4: Handling WG5: Front End

TIS unit endurance test: Tests at high temperature with Joule heating thermal load (1300A target heater, 350A line): heating power 12 kw > primary proton beam thermal load ( 10 kw) Before tests After tests 415 testing hours at high temperature -> 220 hours at maximum power (12kW) 79 heating cycles sustained -> 9 with current ramps of 1 s from 0 A to 1300A (!) to 350A (!) TIS UNIT STILL OPERATIVE!!

Plasma ion sources: off-line beam production Plasma Ion Source Ar beam Kr beam beam ion. eff. (%) injection mode cathode temp. ( C) Xe beam Sn beam Ar 6 gas tube 2200 Br WIP oven 2200 Kr 8,5 gas tube 2200 Y very low oven 2300 Sn 10 oven 2200 I 19 oven 2200 Xe 11 gas tube 2200 Alberto Andrighetto & Mattia Manzolaro

Sourface ion sources: off-line beam production Rb beam Sr beam beam ion. eff. (%) hot-cavity temp. ( C) hot-cavity material Na 47,6 2200 Ta K 55,4 2200 Ta Ga 1,4 2200 Ta Rb 54,5 2200 Ta Sr 18,5 2200 Ta In 3,2 2200 Ta Cs 43,2 2200 Ta Ba 58,8 2200 Ta La 20,1 2200 Ta Cs beam Ba beam Alberto Andrighetto & Mattia Manzolaro

Target materials production and tests New laboratory for the production of UC x at Legnaro Ready for UCx production Ventilation and fire extinguishing systems are ready, instruments are placed and ready to be used

Target material and UCx production On-line testing of the SPES target material and architecture @ ORNL (2010-2012) 40 MeV, 50 na proton beam on a UCx target 2010 Test Standard UC X 2011 Test Low density UC X Density (g/cm³) Diameter (mm) Thickness (g/cm²) Calculated porosity (%) 2010 2011 4.25 2.59 12.50 13.07 0.41 0.41 58 75

Target materials production and tests Synthesis of a novel type of UC x using graphene Experiment submitted & accepted at Karlsruhe: n. AUL-176 "Study of the use of Reduced Graphene Oxide as source of carbon for UCx-Graphene nanocomposites production" Final phase (Nov-Dec 2015, JRC-ITU Karlsruhe, ActusLab) Production of uranium carbide using graphite or graphene as carbon sources UO 2 +6C UC 2 +2C+2CO

Laser Laboratories.. Offline: Spectroscopy 3 Dye Laser @ 10 Hz rep. rate Online (SS laser): RIB prod. 3 TiSa Laser @ 10 khz rep. rate Diagnostic tools: Monochromator HCL ToF Mass Spectrometer Diagnostic tools: Λ-meter Alignments System Ion-Beam

Development of the RIB apparatus: resonant laser ionization Spectroscopy: New SS laser: Laser FE: Study of different elements of interest Offline-lab with 10Hz dye laser system HCL & ToF-MS Defining RIB production laser requirements 10 khz TiSa laser New laser lab requirements ToF system Hot cavity Efficiency measurements

The SMO test at LNL Simulation software Siemens in Tia Portal Movement test in automatic mode Experimental tests with 3 transponder

The agv trip

The new Chamber Unit Storage The layout: Storage cartesian system prototype

ISOL front end: mechanical design upgrades Proton Beam collimator box Pneumatic, hydraulic and power fast connections end 2016 Proton Beam diagnostic cross Within April 2017 Power cables without insulation Within April 2017 end 2016 for: High Power Faraday Cup High Power Beam Profiler General remarks for the Front-End design Elastomer seals are foreseen only in the fast connection for both the pneumatic and hydraulic loops (maybe VAT valves). Hydraulic loops have compatible interfaces for demineralized water (AISI304L/316L - copper or AISI304L/316L - aluminum) in order to prevent corrosion phenomena.

ISOL front end: general design upgrades Collimators Proton beam line RIB line Electrostatic module upgrade for the Wien Filter end 2017 actual NEW July 2016 High Power Beam Profiler and Faraday Cup end 2017 Mass resolution improvement from 80 to 140 Upgraded diagnostic boxes end 2016 elastic system for wires tested

ISOL front end: study of radiation damage on materials RESULTS of the study on elastomeric vacuum O-rings for the target chamber 1. Dosimetry calculations with MCNPX: LNL UniPv UniBs 2. Irradiation in a mixed n+g field at TRIGA reactor: UniPv (LENA) 3. Mechanical and physical tests at MaST Laboratory: UniBs FOUR TESTED PRODUCTS: EPDM 2 Best price/performance ratio Recommended up to 15 days life cycle and beyond PROSPECTS FOR RDS_SPES ACTIVITIES: Experimental study of other components: lubricants and greases, optical fibers, cable insulators, etc. Possible collaboration with ESS for rad-hard test of materials in reactor n+g mixed fields

First Beam for users

List Beam for users (SPES web-page) VISIT: https://web.infn.it/spes/index.php/characteristics/spes-beams-7037/spesbeamstable

Rb beams (Surface Ion Source) Mass scanning stable Isotopes: - 85 Rb (72,17 %) - 87 Rb (27,83 %) Rubidium (Rb) alkali metal atomic number Z = 37 standard atomic weight = 85,468 first ionization potential = 4,18 ev ionization efficiency = 54,5 % working temperature (hot-cavity) = 2200 C injection technique = folded Ta ribbon inside a tubular Ta oven calibrated solution = 10 µl (RbNO 3 in HNO 3(aq) ) total beam intensity 300 na beam RMS emittance = 1,5 π mm mrad extraction voltage = 25 kv Selectivity: Very Good (also without HRMS) isotopes produced @ SPES (p 238 U, 40 MeV 200 µa) Possible First Beam Production Yield: Very Good (pps)

Cs beams (Surface Ion Source) Mass scanning stable Isotopes: - 133 Cs (100 %) Caesium (Cs) alkali metal atomic number Z = 55 standard atomic weight = 132,905 first ionization potential = 3,89 ev ionization efficiency = 43,2 % working temperature (hot-cavity) = 2200 C injection technique = folded Ta ribbon inside a tubular Ta oven calibrated solution = 20 µl (CsNO 3 in HNO 3(aq) ) total beam intensity 300 na beam RMS emittance = 1,5 π mm mrad extraction voltage = 25 kv Selectivity: Good (also without HRMS) isotopes produced @ SPES (p 238 U, 40 MeV 200 µa) Possible Second Beam Production Yield: Very Good (pps)

Ba beams (Surface Ion Source) Mass scanning stable Isotopes: - 134 Ba (2,42 %) - 135 Ba (6,60 %) - 136 Ba (7,85 %) - 137 Ba (11,23 %) - 138 Ba (71,7 %) Production Yield: Good Barium (Ba) alkaline earth metal atomic number Z = 56 standard atomic weight = 137,327 first ionization potential = 5,21 ev ionization efficiency = 58,8 % working temperature (hot-cavity) = 2200 C injection technique = folded Ta ribbon inside a tubular Ta oven calibrated solution = 20 µl (BaCO 3 in HNO 3(aq) ) total beam intensity 300 na beam RMS emittance = 1,5 π mm mrad extraction voltage = 25 kv Selectivity: Good (also without HRMS) isotopes produced @ SPES (p 238 U, 40 MeV 200 µa) Possible good Beam (pps)

Sr beams (Surface Ion Source) Mass scanning stable Isotopes: - 84 Sr (0,56 %) - 86 Sr (9,86 %) - 87 Sr (7,00 %) - 88 Sr (82,58 %) Strontium (Sr) alkaline earth metal atomic number Z = 56 standard atomic weight = 87,62 first ionization potential = 5,70 ev ionization efficiency = 18,5 % working temperature (hot-cavity) = 2200 C injection technique = folded Ta ribbon inside a tubular Ta oven calibrated solution = 40 µl (Sr(NO 3 ) 2 in HNO 3(aq) ) total beam intensity 300 na beam RMS emittance = 1,5 π mm mrad extraction voltage = 25 kv Selectivity: Good (also without HRMS) isotopes produced @ SPES (p 238 U, 40 MeV 200 µa) Possible good Beam Production Yield: Good (pps)

Sn beams (Plasma Ion Source) Tin (Sn) post-transition metal atomic number Z = 50 standard atomic weight = 118,710 first ionization potential = 7,334 ev ionization efficiency = 9,5 % working temperature = 2200 C injection technique = folded Ta ribbon inside a tubular Ta oven (Sn metal) Sn beam intensity observed during the tests 300 na beam RMS emittance = 5 π mm mrad anode voltage = 150 V extraction voltage = 25 kv stable Isotopes: - 112 Sn (0,97 %) - 114 Sn (0,66 %) - 115 Sn (0,34 %) - 116 Sn (14,54 %) - 117 Sn (7,68 %) - 118 Sn (24,22 %) - 119 Sn (8,59 %) - 120 Sn (32,58 %) - 122 Sn (4,63 %) - 124 Sn (5,79%) isotopes produced @ SPES (p 238 U, 40 MeV 200 µa) important Beam

Sn in Laser Laboratory (Future LIS) Tin (Sn) post-transition metal atomic number Z = 50 standard atomic weight = 118,710 first ionization potential = 7,34 ev ionization efficiency = NA working temperature (hot-cavity) = NA injection technique = yes calibrated solution = yes total beam intensity NA important Beam Ionization wavelength path = yes Mass scanning stable Isotopes: - 114 Sn (0,96 %) - 115 Sn (0,66 %) - 116 Sn (14,3 %) - 117 Sn (7,61 %) - 118 Sn (24,03 %) - 119 Sn (8,58 %) - 120 Sn (32,85 %) - 122 Sn (4,72 %) - 124 Sn (5,94 %) Production Yield: Good isotopes produced @ SPES (p 238 U, 40 MeV 200 µa) (pps)

Kr beams (Plasma Ion Source) Mass scanning stable isotopes: - 78 Kr (0,35 %) - 80 Kr (2,25 %) - 82 Kr (11,6 %) - 83 Kr (11,5 %) - 84 Kr (57 %) - 86 Kr (17,3 %) Krypton (Kr) noble gas atomic number Z = 36 standard atomic weight = 83,798 first ionization potential = 13,99 ev ionization efficiency = 4,6 % working temperature = 2200 C gas injection rate (leak) = 5,0 10-6 mbar l/s total beam intensity 3000 na beam RMS emittance = 5 π mm mrad anode voltage = 150 V extraction voltage = 25 kv Selectivity: Bad (without HRMS) isotopes produced @ SPES (p 238 U, 40 MeV 200 µa)

Xe beams (Plasma Ion Source) Mass scanning stable Isotopes: - 124 Xe (0,1 %) - 126 Xe (0,09 %) - 128 Xe (1,91 %) - 129 Xe (26,4 %) - 130 Xe (4,1 %) - 131 Xe (21,2 %) - 132 Xe (26,9 %) - 134 Xe (10,4 %) - 136 Xe (8,9 %) Xenon (Xe) noble gas atomic number Z = 54 standard atomic weight = 131,293 first ionization potential = 12,13 ev ionization efficiency = 5,3 % working temperature = 2200 C gas injection rate (leak) = 5,0 10-6 mbar l/s total beam intensity 3000 na beam RMS emittance = 5 π mm mrad anode voltage = 150 V extraction voltage = 25 kv Selectivity: Bad (without HRMS) isotopes produced @ SPES (p 238 U, 40 MeV 200 µa)

Surface I. S. Surface I. S. Laser I. S. Plasma I. S. Beam Selectivity Calculation (using ORNL model) Proton beam: E= 40 MeV, I=200 µa No HRMS

Surface I. S. Surface I. S. Laser I. S. Plasma I. S. Beam Selectivity Calculation (using ORNL model) Proton beam: E= 40 MeV, I=200 µa No HRMS SPES devoted as 132 Sn factory?

Yield for possible n-poor beams Graphite Target Silicon Carbide Target (test 2006) Isotope Half-life Total Yield (FLUKA) P-> 12C t1/2 [nuclei/s] 7 Be 53 d 4,37E+12 8 B 770 ms 6,64E+11 11 C 20 m 2,45E+13 12 B 20 s 3,50E+08 12 N 11 ms 5,72E+11 13 N 9,9 m 3,33E+10 15 O 122 s 6,99E+08

Conclusion

Concerning the RIB complex The RIB source is almost ready for operation.. - TIS Unit ready; endurance tests running. - UCx LNL laboratory ready for operation. - Laser off-line lab fully operational; Al, Ge, Sn ionization scheme tested successfully. - New handling lab ready; AGV is moving in remote mode. - Rad-hard test for critical materials & components started.

Collaboration network with partners ITHEMBA RISP-KOREA ORNL- HRIBF CERN- ISOLDE INFN- Pavia GANIL-SPIRAL 2 ORSAY-ALTO SPES Exotic Beam INFN- Milano INFN- Bologna INFN- LNS INFN- Padova 33 Tesi Magistrali 20 Tesi Triennali 3 Tesi di PhD 15 Ospiti Stranieri (FAI) UNISI UNIPV UNIPD UNITN UNIBS DSF DEI DSF DIM DSC DEI DTG DIM DIM CONTROLS LASER ION SOURCES MATERIALS HANDLING FRONTEND

Second conclusion: thanks to the team! Thanks for your attention! Few results without them