Bottle Chart Parameter Water/ WW Methods SW84 6 Label Color Bottle Type (Mimimum requi) Preservative Holding Time GENERAL Acidity SM 19 th 2310B Alkalinity 310.1 (200ml) Ammonia 350.1 yellow 250 Plastic Biochemical Oxygen Demand Biochemical Oxygen Demand (carbonaceous) 405.1 (500ml) SM 18 th 5210B (500ml) Bromide 300.0 9056 None requi Chemical Oxygen Demand 410.4 yellow Chloride 300.0 9056 None requi Chlorine Residual 330.4 None requi Coliform, Coliform, Fecal SM 19 th Ed 9223 B SM 19 th Ed. 9222 D beige beige 2-100 ml sterile Plastic 100 ml sterile Plastic.008% Cool 4C.008% 30 hours 6 hours Color 110.2 (200ml) Conductivity 120.1 9050A Cyanide 335.3 9012 purple NaOH to >12 w/ascorbic acid Fluoride 300.0 9056 None requi Hardness, 130.2 <2 w/hno 3 180 days
Chromium VIaqueous SM 19 th 3500-Cr D Method 7196A 24 hours Chromium VIsoil Mercury Aqueous Mercury Solid Metals (Except Cr+6) Metals (Solid) 245.1 200.7 / 200.8 200.7 / 200.8 7196A *MOD 7470A 7471A 6010A / 6020A 6010A / 6020A 9 Oz Soil Jar (4oz) 24 Hours HNO 3 < 2 9 oz Glass (4oz) 28days HNO 3 < 2 6 months 9 oz Glass (4oz) 6 months Nitrate 300.0 9056 Nitrite 300.0 9056 48 hrs Nitrate-Nitrite 300.0 9056 yellow 250 ml H 2 SO 4 Nitrogen 351.3 yellow (150ml) Oil and Grease 1664A 2-1L Glass Orthophosphate 300.0 9056 Oxygen Dissolved Probe Oxygen Dissolved Winkler ph H 2 SO < 2 4 H 2 SO < 2 4 Cool 4C Filter 360.1 ** No Plastic None Requi 405.1 SM 19th 4500- H+ B Method 9040 B Phenols 420.2 9066 SS% (Residue settable) Silicon Recoverable Specific Conductance 160.5 200.7 120.1 Sulfate 300.0 Sulfide 376.2 6010A 9050A 9056 9030A **300 ml BOD Bottle Fix on Site Store in Dark None requi pink Sulfite 377.1 Surfactants 425.1 250 ml Amber glass (200ml) HNO3 <2 ZnAc Plus NaOH 9 None Requi 8 hours VA SM 5910 blue Amber Liter
Silica-Gel Treated Oil and Grease (TPH) 1664 2ea/1L Glass Temperature 170.1 None requi Carbon/Water TDS Residue(Filterable) TSS Residue(Non- Filterable) TR Residue total SM 19 th Ed. 5310C 160.1 160.2 160.3 9060 Turbidity 180.1 VSS (Residue-Volatile) 160.4 (200ml) DRINKING WATER Bromate 300.1 orange Chlorate 300.1 orange Chlorite 300.1 orange Haloacetic Acid 552.1 1L amber glass IC Parameters (NO 3, NO 2, F-, SO 4, Ortho-P,Bromide) NH 4 Cl 300.0 9056 Perchlorate 314.0 SUVA (DOC, UV254) SM 5910B SM 5310C Trihalomethanes 524.2 TOC TCLP + RCI SM 10 th Ed. 5310C 8260B 9060 250 ml plastic blue 1L amber glass 48 Hrs 3 40 ml vials Cool 4C w/.008% HAZARDOUS WASTE CHARACTERIZATION Ch 7 & 8 1010 1110 1311 9010A 9030A grey 7-Glass wide mouth liquid 2-Glass wide mouth solid Cool 4C
BTEX GC 602 8021 BTEX GC/MS 624 8260B ORGANICS dark blue dark blue Herbicides 615 8151A blue PCB 608 8082 blue 2ea/ 40 ml Glass Vial 2ea/ 40 ml Glass Viall HCl <2 HCl <2 PCB Oil 8082 40ml Vial Pesticides 608 8081A blue Organophosph oros Pesticides Semi-Volatiles s TOX Halogens Liq Aquous TOX Halogins-Oil (SGT) Hydrocarbon (DRO) (GRO) 622 8141A blue 625 8270C blue 9020B 1 L Amber Glass 9076 9 Oz Soil Jar 1664 2-1 L Glass TX1005 TX1006 8015 MOD blue 3-40 ml glass vial (2/3 full) 1 L Amber glass NaHSO4 to <2 28 Days 7 Days 7 Days 8015 MOD 2/40 ml VOA Vial 7 Days Volatile s 624 8260B blue 2/40 ml Glass Vial w/hcl <2
Radiological Gross Alpha Radiological Gross Beta Radium 226 & 228 RADIOLOGICAL Subcontract grey 1L Glass HNO 3 to <2 6 months Subcontract grey 1L Glass HNO 3 < 2 6 months Subcontract grey 1L Glass HNO 3 < 2 6 months HCl = Hydrochloric Acid HNO 3 = Nitric Acid H 2 SO 4 = Sulfuric Acid = Sodium Thiosulfate NaOH = Sodium Hydroxide NaHSO 4 = Sodium Bisulfate ZnAc = Zinc Acetate August 12, 2003