Report No. ECL01H033498 Page 1 of 7 Applicant Address MITSUI HIGH-TEC (SHANGHAI) CO.,LTD NO.2001 XINJIN QIAO ROAD EXPORT PROCESSING ZONE PUDONG SHANGHAI CHINA The following sample(s) and sample information was/were submitted and identified by/on the behalf of the client Sample Name Ag Plating Sample Received Date Testing Period Jul.6,2015 Jul.6,2015 to Jul.10,2015 Test Requested As specified by client, to test Lead (Pb), Cadmium (Cd), Mercury (Hg), Hexavalent Chromium(Cr(VI)), Polybrominated Biphenyl(PBBs), Polybrominated Diphenyl Ethers(PBDEs), Fluorine(F), Chlorine(Cl), Bromine(Br), Iodine(I), Perfluorooctanoic Acid(PFOA),Perfluorooctane Sulfonates(PFOS), Antimony(Sb) in the submitted sample(s). Test Method Test Result(s) Please refer to the following page(s). Please refer to the following page(s). Test Result(s) Please refer to the following page(s). Tested by Reviewed by Approved by Date Jul.10,2015 Su Hongwei Senior Laboratory Manager No. R108725487 Centre Testing International (Shenzhen) Co., Ltd. Shanghai Branch No.1996,Xinjinqiao Road, Pudong New District,Shanghai,China
Report No. ECL01H033498 Page 2 of 7 Test Method Tested Item(s) Test Method Measured Equipment(s) Lead(Pb) Refer to IEC 62321-5:2013 Ed.1.0 ICP-OES Cadmium(Cd) Refer to IEC 62321-5:2013 Ed.1.0 ICP-OES Mercury(Hg) Refer to IEC 62321-4:2013 Ed.1.0 ICP-OES Hexavalent Chromium(Cr(VI)) IEC 62321:2008 Ed.1 Annex B IEC 62321:2008 Ed.1 Annex C UV-Vis Polybrominated Biphenyls(PBBs) IEC 62321:2008 Ed.1 Annex A GC-MS Polybrominated Diphenyl Ethers (PBDEs) IEC 62321:2008 Ed.1 Annex A GC-MS Fluorine (F) Refer to BS EN 14582:2007* 1 IC Chlorine (Cl) Refer to BS EN 14582:2007* 1 IC Bromine (Br) Refer to BS EN 14582:2007* 1 IC Iodine (I) Refer to BS EN 14582:2007* 1 IC Perfluorooctanoic Acid (PFOA) Refer to US EPA 3550C:2007 & US EPA 8321B:2007 LC-MS-MS Perfluorooctane Sulfonates (PFOS) Refer to US EPA 3550C:2007 & US EPA 8321B:2007 LC-MS-MS Antimony(Sb) Refer to US EPA 3050B:1996 ICP-OES
Report No. ECL01H033498 Page 3 of 7 Test Result(s) Tested Item(s) Result MDL Lead(Pb) N.D. 2 mg/kg Cadmium(Cd) N.D. 2 mg/kg Mercury(Hg) N.D. 2 mg/kg Hexavalent Chromium(Cr(VI)) N.D. 2 mg/kg Negative / Polybrominated Biphenyls(PBBs) Monobromobiphenyl N.D. 5 mg/kg Dibromobiphenyl N.D. 5 mg/kg Tribromobiphenyl N.D. 5 mg/kg Tetrabromobiphenyl N.D. 5 mg/kg Pentabromobiphenyl N.D. 5 mg/kg Hexabromobiphenyl N.D. 5 mg/kg Heptabromobiphenyl N.D. 5 mg/kg Octabromobiphenyl N.D. 5 mg/kg Nonabromobiphenyl N.D. 5 mg/kg Decabromobiphenyl N.D. 5 mg/kg Polybrominated Diphenyl Ethers(PBDEs) Monobromodiphenyl ether N.D. 5 mg/kg Dibromodiphenyl ether N.D. 5 mg/kg Tribromodiphenyl ether N.D. 5 mg/kg Tetrabromodiphenyl ether N.D. 5 mg/kg Pentabromodiphenyl ether N.D. 5 mg/kg Hexabromodiphenyl ether N.D. 5 mg/kg Heptabromodiphenyl ether N.D. 5 mg/kg Octabromodiphenyl ether N.D. 5 mg/kg Nonabromodiphenyl ether N.D. 5 mg/kg Decabromodiphenyl ether N.D. 5 mg/kg Tested Item(s) Result MDL Halogen Fluorine (F) N.D.* 2 50mg/kg Chlorine (Cl) N.D.* 2 50mg/kg Bromine (Br) N.D.* 2 50mg/kg Iodine (I) N.D.* 2 50mg/kg
Report No. ECL01H033498 Page 4 of 7 Tested Item(s) Result MDL Perfluorooctanoic Acid (PFOA) N.D.* 2 0.5μg/m 2 Perfluorooctane Sulfonates(PFOS) N.D.* 2 0.5μg/m 2 Antimony(Sb) N.D. 10 mg/kg Tested Sample/Part Description Silver-white plating Remark: -MDL = Method Detection Limit -N.D. = Not Detected (<MDL) -mg/kg = ppm = parts per million -Negative = Absence of Cr(VI), the detected Cr(VI) concentration in the boiling water extraction solution is less than 0.02 mg/kg with 50cm 2 sample surface area used. -* 1 = The specified area sample is extracted by an ultrasonic bath in ultra-pure water, and then the extracted liquid is analyzed by IC. -* 2 = The value is converted from the test result with the density and thickness provided by client (Density =10.49g/cm 3, thickness=4μm). Test Process 1. Lead(Pb), Cadmium(Cd) Take a portion of Add digestion reagent Take out the substrate after the plating had been dissolved Analyzed by ICP-OES 2. Mercury(Hg) Take a portion of Add digestion reagent Transfer the plating digestive solution into a volumetric flask Take out the substrate after the plating had been dissolved Analyzed by ICP-OES Transfer the plating digestive solution into a volumetric flask
Report No. ECL01H033498 Page 5 of 7 3. Hexavalent Chromium (Cr(VI)) (1)IEC 62321:2008 Ed.1 Annex B Take a portion of Extracted with boiling water Filter and remove Analyzed by UV-Vis Add test solution Adjust the ph value of the solution (2)IEC 62321:2008 Ed.1 Annex C Weigh sample and place it in a conical flask Add digestion solution Heat at 90-95 for 3 hours Add test solution Adjust the ph value of the solution Cool and filter Adjust the ph value of the solution Analyzed by UV-Vis 4. Polybrominated Biphenyls(PBBs), Polybrominated Diphenyl Ethers(PBDEs) Weigh sample and place it in a thimble Extracted with organic solvent Concentrate the extract Analyzed by GC-MS organic solvent Transfer the extract into a volumetric flask 5. Fluorine (F), Chlorine (Cl), Bromine (Br), Iodine (I) Take a certain sample into a container Add ultra-purity water Extracted in an ultrasonic equipment Analyzed by IC ultra-purity water Filter and transfer the extract
Report No. ECL01H033498 Page 6 of 7 6. Perfluorooctanoic Acid (PFOA),Perfluorooctane Sulfonates(PFOS) Sample preparation Extracted with organic solvent in an ultrasonic equipment Concentrate the extract Analyzed by LC-MS-MS organic solvent Transfer the extract into a volumetric flask 7. Antimony(Sb) Weigh sample and place it in a beaker Add digestion reagent Digest sample on electric hot plate till totally dissolved Analyzed by ICP-OES Dilute to the mark and mix thoroughly with Transfer the digested solution into a volumetric flask
Report No. ECL01H033498 Page 7 of 7 Photo(s) of (s) ECL01H033498 *** End of Report *** The test report is effective only with both signature and specialized stamp. The result(s) shown in this report refer only to (s) tested. Without written approval of CTI, this report can t be reproduced except in full.