No. CE/2012/C1503 Date 2012/12/18 Page 1 of 6 The following sample(s) was/were submitted and identified by/on behalf of the client as Sample Description Buyer/Order No. Other Info. Sample Receiving Date Testing Period GAP FILLER 3500S35 RICK STEWART REPORT PER REQUEST FOR QUOTE, DATED 10/5/11 2012/12/11 2012/12/11 TO 2012/12/18 ========================================================================================= Test Requested As specified by client, to test Cadmium, Lead, Mercury, Cr(VI), PBBs, PBDEs contents in the submitted sample. Test Method Test Result(s) Please refer to next pages. Please refer to next page(s). Company.
No. CE/2012/C1503 Date 2012/12/18 Page 2 of 6 Test Result(s) PART NAME No.1 Test Item(s) Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether MIXED BLUE AND WHITE PASTE Unit Method With reference to IEC 62321 2008 and performed by ICP-AES. With reference to IEC 62321 2008 and performed by ICP-AES. With reference to IEC 62321 2008 and performed by ICP-AES. With reference to IEC 62321 2008 and performed by UV-VIS. Result MDL No.1 - n.d. With reference to IEC 62321 2008 and 5 n.d. performed by GC/MS. - n.d. Company.
No. CE/2012/C1503 Date 2012/12/18 Page 3 of 6 Note 1. = ppm;0.1wt% = 1000ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. " - " = Not Regulated 5. The sample(s) was/were analyzed on behalf of the applicant as mixing sample in one testing. The above result(s) was/were only given as the informality value. Company.
No. CE/2012/C1503 Date 2012/12/18 Page 4 of 6 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr 6+ test method excluded) 2) Name of the person who made measurement Climbgreat Yang 3) Name of the person in charge of measurement Troy Chang Cutting / Preparation Sample Measurement Pb Cd Acid digestion by suitable acid depended on different sample material (as below table) Hg Microwave digestion with HNO 3 /HCl/HF Cr 6+ (Note**) Add appropriate amount of digestion reagent Filtration Solution ICP-AES Sample Material Residue 1) Alkali Fusion 2) HCl to dissolve Digestion Acid Heat to appropriate temperature to extract Cool, filter digestate through filter Add diphenyl-carbazide for color development Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2 O 2 Glass Gold, platinum, palladium, ceramic HNO 3 /HF Aqua regia Silver HNO 3 Plastic Others H 2 SO 4, H 2 O 2, HNO 3, HCl Added appropriate reagent to total digestion measure the absorbance at 540 nm by UV-VIS Note**(1) For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2) For metallic material, add pure water and heat to boiling. Company.
No. CE/2012/C1503 Date 2012/12/18 Page 5 of 6 PBB/PBDE analytical FLOW CHART Name of the person who made measurement Roman Wong Name of the person in charge of measurement Troy Chang First testing process Optional screen process Confirmation process Sample Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report Company.
No. CE/2012/C1503 Date 2012/12/18 Page 6 of 6 * The tested sample / part is marked by an arrow if it's shown on the photo. * ** End of Report ** Company.