Magnetic couplings, stirrer drives for Chemical Reactors bmd and cyclone: Absolutely tight, safe and dependable

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Magnetic couplings, stirrer drives for Chemical Reactors and cyclone: Absolutely tight, safe and dependable Büchi quality Easy maintenance Compact design Well designed Efficient stirring / mixing full vacuum - high pressure low high torque low high temperatures PED / ATEX corrosion resistant metals / ceramic BÜCHI THE WAY TO GET RESULTS!

Magnetic couplings The main difference of a magnetic stirrer drive and a conventional stirrer drive such as rubber gland, lip seal and mechanical seal is the fact, that the internal stirrer shaft is driven without any contact to the static seal. The external magnet and the internal magnet are virtually connected through a strong magnetic field. The external magnet is located outside the pressure chamber. The internal magnet, which is inside the pressure chamber, is connected to the stirrer shaft and rotates simultaneously with the motor driven external magnet. Buchi offers low to high torque magnetic couplings and stirrer drives, which fulfill high performance mixing also in high viscous media. external magnet internal magnet shaft closing cap stirrer shaft slide bearing Functional principle of a magnetic coupling drive magnetic force outer magnet Inner magnet closing cap, statically sealed coverplate, statically sealed pressure vessel stirrer shaft stirrer, n s =n d 2

magnetic coupling Buchi magnetic couplings hermetically seal the reaction chamber. The operation of the internal stirrer via the magnetic coupling requires a specific motor drive, which meets your requirements regarding viscosity of the media, stirrer speed and hazardous area (ATEX). Example: Powerful stirrer drive with magnetic coupling 300, EX version, installed on polyclave. Cyclone magnetic drive Buchi Magnetic drives incorporate a magnetic coupling with an electric motor. The stirrer speed is controlled by its own controller unit. Example: Powerful cyclone 300 magnetic stirrer drive with stirrer servo motor controller. 3

magnetic couplings for Lab reactors, stirred autoclaves Magnetic couplings 75 1200 Ncm torque ( 075 1200) ATEX-version optional 075 300 800 1200 For technical Details of standard 075 to 5400 please refer to the table on reverse side Special versions fully metal - free magnetic coupling 250«i» Threaded connections for metal cover plates or NS 29/32 connections for glass reactors 4

magnetic couplings for pilot scale reactors Magnetic couplings 1800 5400 Ncm torque ( 1800 5400) ATEX standard 1800 3600 5400 Applications 1800 on 100 liter Hastelloy reactor 5400 on 20 litre polymerization reactor 800 on custom kiloclave 300 with ATEX drive on polyclave 5

cyclone magnetic stirrer drives for Lab Reactors, stirred autoclaves Magnetic drives with 75 / 300 Ncm torque (cyclone 075 cyclone 300) Buchi cyclone 075 as well as the cyclone 300 are complete stirrer drives. They contain a magnetic coupling 075 / 300 with an electric motor. They can be installed on the reactor cover plate with an M36x1.5 thread. The cyclone 300 controller enables stepless stirrer speed adjustment of the servo motor. Stirrer speed and torque can be transferred via a RS 232 interface to bds measuring / display unit and/or to the bls software. The stirrer speed can be set electrically by a 4 20 ma Signal. cyclone 075 and cyclone 300 magnetic stirrer drives for full vacuum to high pressure reactors Applications cyclone 300 on versoclave midiclave with cyclone 300 Compact cyclone 075 stirrer drive for picoclabe Lab pressure reactor limbo li 350 bar high pressure reactor with cyclone 075 6

cyclone inert «i» metal free stirrer drives inert magnetic drive with 250 Ncm torque (cyclone 250 «i») and cyclone «i» cyclone 250 «i», 250 «i» The inert magnetic coupling 250 «i» and magnetic stirrer drive cyclone 250 «i» are specially developed to avoid corrosion in processes with highly aggressive media, or for processes where contact with metal parts is not permissible. Developed on the proven Büchi magnetic coupling design, nonmetallic materials such as ceramic and PEEK are used for all components in contact with the process media. High mechanical and chemical stability guarantees trouble-free operation under the harshest conditions. This new technology allows us to provide complete non-metallic pressure reactors with powerful high-torque and leak-free agitators. cyclone «i» The cyclone «i» is an economic inert stirrer concept with capability of mixing low viscosity media only. It can be used at pressures up to 6 bar in the inertclave. cyclone 250 «i» magnetic drive 250 «i» magnetic coupling cyclone «i» for low viscosity mixing Applications kiloclave inert, 250 «i» ATEX glass lined steel reactor: 10 Litre, 6 bar, 180 C inertclave, cyclone 250 «i» 1.6 Litre, 6 bar, 180 C inertclave, cyclone «i» 1 Litre, 6 bar, 180 C, 3-wall glass reactor 7

Technical data diekonkreten.ch 06/14 Type Dimensions in mm 075 250 «i» 300 800 1200 1800 3600 5400 cyclone 075 cyclone 250 «i» cyclone 300 Height 133 222 222 252 282 375 400 425 300 500 500 Diameter 46 67 67 67 67 160 160 160 96 115 115 Torque in Ncm 75 250 300 800 1200 1800 3600 5400 75 250 300 Pressure Vacuum 1 bar l l l l l l l l l l l Pressure 50 bar l l l Pressure 60 bar l l l l l t t t l l l Pressure 100 bar l l l l t t t l l Pressure 150 bar l l l l t t t l l Pressure 200 bar t t t t t t t t t Pressure 350 bar t t t t t t Operating Temperature 250 C l l l l l l l l l l l > 250 C w. cooling jacket/m. n n n n n n n n n n n Speed max. 1200 1/min. l l l l l l l l l l l max. 2000 1/min. l l l l l t t t l l l max. 2500 1/min. l t t t t l t max. 3000 1/min. l n t t l l t Bearing Slide bearing PTFE/Graphite l t l l l l t l Slide bearing PTFE n t n n n n t n Slide bearing PEEK n t n n n n t n Slide bearing Graphite n t n n n n t n Ball bearing Ceramic t l n t t l l l t l n Materials 1.4435/1.4571 l l l l l l l l l Hastelloy C22 l l l l l l l l l Ceramic l l others t l t t t t t t t l t stirrer shaft Ø (mm) 10 12/10 16 16 16 22 22 22 10 12/10 16 others t n n n n n n n n Length (mm) n n n n n n n n n n n Connection thread M 36x1,5 l l l l l t t t l l l NS 29/32 l l Flange t t t t t l l l t t t others t t t t t t t t t t t l Standard tspecial n customer specific Büchi AG Phone +41 (0) 44 905 51 11 Gschwaderstrasse 12 Fax +41 (0) 44 905 51 22 CH-8610 Uster/ Switzerland www.buchiglas.com 40.9P008.B010