Validation of COMSOL -Based Performance Predictions of Bi-2212 Round Wire Prototype Coils

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Validation of COMSOL -Based Performance Predictions of Bi-2212 Round Wire Prototype Coils Ernesto S. Bosque U.P. Trociewitz Y.Kim, D.K. Hilton, C.L. English, D.S. Davis, G. Miller, D. Larbalestier

Bi-2212 RW: Performance limits Overview P.Chen 2 Bi 2 Sr 2 Ca 1 Cu 2 O 8+δ (high temperature superconductor, HTS) Performance limits Multiphysics FEA Introduction to the modeling effort Principal assumptions and definitions Analysis led design of prototype coils G.Miller The Prototype Coil Program Approaching operational limits Experimental validation of the modeling Summary

Advancing wire and over-pressure heat treatment (OPHT) processing Bi-2212 Round Wire: A brief introduction 3 Macroscopically isotropic, twisted round wire: Minimal field drift; appropriate for Nuclear Magnetic Resonance Magnetization even smaller than low temperature superconductors D.Larbalestier et al., Nature Materials 2014 D.Davis, et al. J.Jiang, et al.

4 P.Lee

5 R.Bjoerstad et al., CERN EuCARD-2 2015 Bi-2212 RW: Performance limits I c (B) field dependence I c (ε) strain along wire axis MTS stress-strain data taken from single wires Coil analogy azimuthal (hoop) strains in coils σ z ε z Azimuthal stress-strain in Coil Axial stress-strain along wire axis ε θ z y x σ θ N.Cheggour, U.Colorado-Boulder

6 Multiphysics FEA: Addressing primary concerns Models studied on a wire-by-wire level 4.2 K thermal strain Computation of magnetic fields 2D-axisymmetric (J. B. R) Lorentz Forces coil source stresses Field computed [T] x H = J r = 0 mm Above: Field generated by running 100 A/mm 2 in a single loop (1 mm dia wire; 10 mm dia loop) placed within a 10 T background field (range 9.97 [blue] to 10.05 [red] T). Lorentz stress [MPa]: J phi. B z. R r = 0

7 Multiphysics FEA: Addressing primary concerns Models studied on a wire-by-wire level 4.2 K thermal strain Computation of magnetic fields (J. B. R) Lorentz Forces coil source stresses Coupling the J. B. R to structural mechanics These coils epoxy impregnated; so stresses are redistributed across all materials within the coil pack Allows for reinforcement on coil level Each material defined with its own, experimentally tabulated material properties r = 0 Above: Field generated by running previous slide example after epoxy impregnating and over-banding Lorentz stress [MPa] is identical (J only in wire) Below: Structural mechanics coupling the Lorentz load with reinforcement lowers the hoop stress along the conductor.

Models studied on a wire-by-wire level 4.2 K thermal strain Multiphysics FEA: Addressing primary concerns Generated field map 8 Computation of magnetic fields (J. B. R) Lorentz Forces coil source stresses Coupling the J. B. R to structural mechanics These coils epoxy impregnated; so stresses are redistributed across all materials within the coil pack Allows for reinforcement on coil level Each material defined with its own, experimentally tabulated material properties Conductor elasticity modulus based on non-linear stress-strain data from short samples Fully coupled model accounts for movement of each conductor r = 0 Above: Resulting azimuthal strain for this example. Note the peak strain is on the ID of loop. Right: A cross section of a prototype coil. Shown is Riky-1, a magnet would with Bi-2212 [red] wires and later epoxy [blue] impregnated but otherwise not reinforced coil.

Multiphysics FEA: Analysis led design of prototype coils Prototype design constraints Geometry and background fields of the available LTS test beds Working hot zone of the furnace (OPHT facility) inner diameter of 130 mm; 450 mm height; 890 degc; 50 atm 9 Cyocooled 8 T 242 mm magnet ID 140 mm cryostat

Motivation for each prototype: First set of prototypes were scaled versions of a larger (high field NMR) demonstration coil (18 layers, ~10 turns) - intended to test manufacturing - designed for a now decommissioned 17 T testbed The Prototype Coil Program 10 Second set of prototypes were designed to approach the strain limits of a coil wound with Bi-2212 RW conductor (4 layers, 10 turns) (limited to the available 8 T background) - validating the FEA modeling efforts; qualification & quantification - examining reinforcement techniques Peak Azimuthal Strain under background fields Now using either prototype to target specific hurdles as we further develop Bi-2212 RW for high field NMR applications

Motivation for each prototype: The Prototype Coil Program 11 Second set of prototypes were designed to approach the strain limits of a coil wound with Bi-2212 RW conductor (4 layers, 10 turns) (limited to the available 8 T background) - validating the FEA modeling efforts; qualification & quantification - examining reinforcement techniques Below: Strain-limited performance envelope, increase of either background field and/or HTS current lead to 0.6% strain limit Parametric sweeps Input current and LTS Outsert fields are real knobs Strain-based performance envelopes

Prototype Coils: Experimental validation of modeling Second set of prototypes predictions First coil (not reinforced) was predicted to reach 0.6% azimuthal strain near ~280 A (231 A/mm 2 ) within an ~8 T background Second coil built with full reinforcement Third coil includes moderate reinforcement to reach 0.6% near ~350 A (489 A/mm 2 ) The third prototype was constructed with 1.0 mm wire; first and second had 1.3 mm wire. Roughly, B and R were held constant while increasing J e. The added strain was thus managed with the inclusion of moderate reinforcement. 12 #1 #1 #3 #3 #2

LEM HTS Current [A] Prototype Coils: Experimental validation of modeling Second set of prototypes predictions First coil (not reinforced) was predicted to reach 0.6% azimuthal strain near ~280 A (231 A/mm 2 ) within an ~8 T background Second coil built with full reinforcement Third coil includes moderate reinforcement to reach 0.6% near ~350 A (489 A/mm 2 ) Coil Voltages [mv] 400 200 0-200 -400-600 -800 Riky3 HTS Ramp 20170524 1 400 350 300 250 200 150 100 The third prototype was constructed with 1.0 mm wire; first and second had 1.3 mm wire. Roughly, B and R were held constant while increasing J e. The added strain was thus managed with the inclusion of moderate reinforcement. #1 #3 #2 13-1000 50-1200 0 6711.5 6711.5 6711.6 6711.7 6711.7 6711.7 6711.8 Time [s]

14 Another of the second set of prototype coils Intended to further validate the model by including an incrementally larger amount of reinforcement. This coil is predicted to reach its critical strain at a current of ~450 A (628 A/mm 2 ) within an ~8 T background. Prototype Coils: The next ones

15 Another of the first set of prototype coils As well as further validation, the first type of prototype coils were a thicker build. Hence, this cleverly designed coil should experimentally reveal a peak strain gradient with plenty of spatial resolution. The predicted strain limited performance for this coil peaks at a current of ~420 A (586 A/mm 2 ) within an ~8 T background. Prototype Coils: The next ones

Next up: the NMR demonstration coil Coil parameters Wire diameter: 1.0 mm wire I op : 310 A ID: 44.45 mm Background: 16 T (Adding: 5.3 T) A Bi-2212 Insert for High Field NMR 16 Computation 16.7 million degrees of freedom (10 hrs to mesh) 45 minutes to compute (89 GB ram) So what? Confidence from the prototypes predicts: 21.3 T [909 MHz] is achieved at 0.4% azimuthal strain; 23.5 T [1 + GHz] is plausible even with this demo coil - 2212 macroscopically isotropic and should prove to have better field temporal stability Platypus nested in IMPDAHMA G.Miller

Bi-2212 coil reinforcement is developing well, and Bi-2212 technology is ever advancing FEA tools have been developed to confidently build Bi-2212 coils that approach the conductor operating limits Summary 17 This conductor was once I c limited Now it is strain limited Newest short sample shows at least 50% J c improvement over wires used in these prototype coils J.Jiang, et al. Coil reinforcement allows for more use of this higher I c (B) limit, and otherwise provides tolerance to approaching ε critical = 0.6%

Acknowledgements 18 This work is supported by the National Science Foundation under DMR-1157490, the State of Florida, and a grant from the National Institute of Health under 1 R21 GM111302-01.