Page:1of12 Thefolowingsampleswas/weresubmittedandidentifiedby/onbehalfoftheapplicantas: Sam plesubm ittedb y : Sam pledescription : EL EK TRISOL A TH ERM OB ON D SEL F-B ON DIN G IN SUL ATION V ARN ISH Style/Item N o. : B E-,GT-,H T-,K T-,QT-,RT-,ST-,TT-,V T-SERIES Sam plereceivingdate : 2018/04/02 TestingPeriod : 2018/04/02 T O 2018/04/13 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = TestRequested : (1) As specifiedbyclient,withreferencetoroh S 2011/65/EU AnnexIIandam endingdirective(eu) 2015/863todeterm inecadm ium,l ead,m ercury,cr(v I),PB B s,pb DEs,DB P,B B P,DEH P,DIB P contents in thesubm ittedsam ple(s). (2) Pleaserefertonextpages fortheotheritem (s). TestR esu lt(s) : Pleaserefertofollowingpages.
Page:2of12 TestR esu lt(s) PART N AM E N o.1 : B ROW N L UM P TestItem(s) Cadm ium (Cd) Unit M ethod W ithreferencetoiec 62321-5(2013)and perform edbyicp-aes. Result M DL N o.1 2 n.d. L ead(pb) W ithreferencetoiec 62321-5(2013)and perform edbyicp-aes. 2 n.d. M ercury(h g) W ithreferencetoiec 62321-4(2013)and perform edbyicp-aes. 2 n.d. H exavalentchrom ium Cr(V I) W ith reference to IE C 62321-7-2(2017)and perform edbyuv -V IS. 8 n.d. Sum ofpbbs - n.d. M onobrom obiphenyl D ibrom obiphenyl T ribrom obiphenyl T etrabrom obiphenyl P entabrom obiphenyl H exabrom obiphenyl H eptabrom obiphenyl Octabrom obiphenyl N onabrom obiphenyl D ecabrom obiphenyl Sum ofpbdes W ithreferencetoiec 62321-6(2015)and perform edbygc/m S. - n.d. M onobrom odiphenylether D ibrom odiphenylether T ribrom odiphenylether T etrabrom odiphenylether P entabrom odiphenylether H exabrom odiphenylether H eptabrom odiphenylether Octabrom odiphenylether N onabrom odiphenylether D ecabrom odiphenylether
Page:3of12 TestItem(s) Unit M ethod M DL B B P (B utylb enzylphthalate) (CAS N o.:85-68-7) DB P (Dibutylphthalate)(CAS N o.:84-74-2) DEH P (Di-(2-ethylhexyl) phthalate)(cas N o.:117-81-7) DIB P (Di-isobutylphthalate)(CAS N o.:84-69-5) D ID P (D i-is odecylphthalate) (C A S N o.:26761-40-0;68515-49- 1) D IN P (D i-is ononylphthalate) (C A S N o.:28553-12-0;68515-48- 0) D N OP (D i-n-octylphthalate) (CAS N o.:117-84-0) H exabrom ocyclododecane (H B CDD)andallm ajor dias tereois om ers identified (α - H B CDD, β - H B CDD, γ - H B CDD) (CAS N o.:25637-99-4and3194-55-6(134237-51-7,134237-50-6, 134237-52-8)) W ithreferencetoiec 62321(2008).Analysis was perform edbygc/m S. Result N o.1 50 87.6 Perfluorooctanesulfonates (PFOS-Acid,M etalsalt,am ide) W ithreferencetous EPA 3550C (2007). Analysis was perform edbyl C/M S. 10 n.d. PFOA (CAS N o.:335-67-1) W ithreferencetous EPA 3550C (2007). Analysis was perform edbyl C/M S. 10 n.d. Antim ony(sb) W ithreferencetous EPA 3052(1996). Analysis was perform edbyicp-aes. 2 n.d. B eryllium (B e) W ithreferencetous EPA 3052(1996). Analysis was perform edbyicp-aes. 2 n.d.
Page:4of12 TestItem(s) Unit M ethod M DL H alogen H alogen-flu orine(f) (CAS N o.:14762-94-8) H alogen-chlorine(cl) (CAS N o.:22537-15-1) H alogen-b rom ine(b r) (CAS N o.:10097-32-2) H alogen-iodine(i) (CAS N o.:14362-44-8) W ithreferencetob S EN 14582(2016). Analysis was perform edbyic. W ithreferencetob S EN 14582(2016). Analysis was perform edbyic. W ithreferencetob S EN 14582(2016). Analysis was perform edbyic. W ithreferencetob S EN 14582(2016). Analysis was perform edbyic. Result N o.1 N ote: 1. = ppm ; 0.1wt% = 1000ppm 2. M DL = M ethoddetection L im it 3. n.d.= N otdetected= less than M DL 4. "-"= N otregulated PFO S ReferenceInformation:PO Ps-(EU)757/2010 OutlawingPFOS as substances orpreparations in concentrations above0.001% (10ppm ),in sem i-finished products orarticles orparts atalevelabove0.1%(1000ppm ),in textiles orothercoatedm aterials above1µ g/m ².
Page:5of12 #FLOW A nalyticalflow chartofh eavy M etal T hesesamples weredissolvedtotalybypre-conditioningmethodaccordingtobelow flow chart.(cr 6+ test methodexcluded) T echnician :RitaChen Supervisor:T roychang C u tting Preparation SampleM easurem ent Pb/Cd/Hg Cr 6+ Aciddigestion with microwave/hotplate N on-m etal M etal Solution Filtration Residu e 1) Alkalifu s ion 2) H Cltodissolve A BS /PC /PVC O thers Dissolvingby u ltras onication Digestingat 60 by u ltras onication D iges tingat 150~160 Separatingto get aqueous phase B oilingwater extraction C ool,filter diges tatethrou gh filter ICP-AES ph adjustm ent Add diphenylcarbazideforcolor dev elopm ent Add diphenyl-carbazidefor colordev elopm ent M easurethe abs orbanceat 540 nm byuv -V IS M eas u retheabs orbanceat 540nm byuv -V IS
Page:6of12 #PIC A nalyticalflow chart PBB /PBDE T echnician :YalingT u Supervisor:TroyChang Firsttestingprocess Optionals creen proces s Confirm ation process Sam ple S am plepretreatm ent Screen analysis Sam pleextraction / Soxhletmethod C oncentrate/d ilu te Extractedsolution Filter GC/M S
Page:7of12 A nalyticalflow chart-phthalate Technician:AndyH su Supervisor:TroyChang Testm ethod:iec 62321-8 S am plepretreatm ent/s eparation Sam pledissolved/extractedbyth F DiluteExtractedsolution Analysis was perform edbygc/m S
Page:8of12 A nalyticalflow chart-h BCDD T echnician:yalingt u Supervisor:TroyChang Sam plepretreatm ent Sam pleextraction /U ltras onicm ethod Concentrate/DiluteExtractedsolution Filter Analysis was perform edbygc/m S Data
Page:9of12 A nalyticalflow chart-h alogen Technician:RitaChen Supervisor:TroyChang Sam plepretreatm ent/s eparation W eightingandputtingsam plein cel Oxygen B om bcom bu stion /Absorption Dilution tofixedvolum e Analysis was perform edbyic
Page:10of12 A nalyticalflow chart-pfo A /PFO S T echnician:yalingt u Supervisor:TroyChang S am plepretreatm ent S am ple extraction by U ltras onicextraction (Referencem ethod:us EPA 3550C) Concentrate/DiluteExtractedsolution Analysis was perform edbyl C/M S Data
P age:11of12 Thesesam ples weredissolvedtotallybypre-conditioningm ethodaccordingto below flow chart. Technician:RitaChen Supervisor:TroyChang Flow ChartofdigestionfortheelementsanalysisperformedbyICP-A ES C u tting/preparation Sam plem easurem ent Aciddigestion bysuitableaciddependedon diferent s am plem aterial(as below table) Filtration Solution Residue 1) AlkaliFusion 2) H Cltodissolve ICP-AES Steel,copper,aluminum,solder Glass Gold,platinum,paladium,ceram ic Silver Plastic Others Aquaregia,H N O3,H Cl,H F,H 2O2 H N O3/H F Aquaregia H N O3 H 2SO4,H 2O2,H N O3,H Cl A dded appropriatereagent to totaldiges tion
Page:12of12 *Thetestedsample/partismarkedbyanarrow ifit'sshownonthephoto.* **EndofReport **