Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 1 of 8 The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description : Style/Item No. : Color : Sample Receiving Date : Testing Period : Sample Submitted By : FAL FAL CLEAR 2018/01/19 2018/01/19 TO 2018/01/25 =========================================================================================== Test Result(s) : Please refer to next page(s).
Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 2 of 8 Test Result(s) PART NAME NO.1 : CLEAR FAL FILM WITH ADHESIVE Test Item (s): Unit Method Cadmium (Cd) mg/kg With reference to IEC 62321-5: 2013 and performed by ICP-AES. Lead (Pb) mg/kg With reference to IEC 62321-5: 2013 and performed by ICP-AES. Mercury (Hg) mg/kg With reference to IEC 62321-4: 2013 and performed by ICP-AES. Hexavalent Chromium Cr(VI) mg/kg With reference to IEC 62321-7-2:2017 and performed by UV-VIS. Result MDL No.1 2 n.d. 2 n.d. 2 n.d. 8 n.d. Sum of PBBs mg/kg - n.d. Monobromobiphenyl mg/kg 5 n.d. Dibromobiphenyl mg/kg 5 n.d. Tribromobiphenyl mg/kg 5 n.d. Tetrabromobiphenyl mg/kg 5 n.d. With reference to IEC 62321-6:2015 Pentabromobiphenyl mg/kg 5 n.d. and performed by GC/MS. Hexabromobiphenyl mg/kg 5 n.d. Heptabromobiphenyl mg/kg 5 n.d. Octabromobiphenyl mg/kg 5 n.d. Nonabromobiphenyl mg/kg 5 n.d. Decabromobiphenyl mg/kg 5 n.d. Sum of PBDEs mg/kg - n.d. Monobromodiphenyl ether mg/kg 5 n.d. Dibromodiphenyl ether mg/kg 5 n.d. Tribromodiphenyl ether mg/kg 5 n.d. Tetrabromodiphenyl ether mg/kg 5 n.d. With reference to IEC 62321-6:2015 Pentabromodiphenyl ether mg/kg 5 n.d. and performed by GC/MS. Hexabromodiphenyl ether mg/kg 5 n.d. Heptabromodiphenyl ether mg/kg 5 n.d. Octabromodiphenyl ether mg/kg 5 n.d. Nonabromodiphenyl ether mg/kg 5 n.d. Decabromodiphenyl ether mg/kg 5 n.d.
Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 3 of 8 Test Item (s): Unit Method DIBP (Di-isobutyl phthalate) (CAS No.: 84-69-5) DBP (Dibutyl phthalate) (CAS No.: 84-74-2) BBP (Butyl Benzyl phthalate) (CAS No.: 85-68-7) DEHP (Di- (2-ethylhexyl) phthalate) (CAS No.: 117-81-7) Halogen Halogen-Fluorine (F) (CAS No.: 14762-94-8) Halogen-Chlorine (Cl) (CAS No.: 22537-15-1) Halogen-Bromine (Br) (CAS No.: 10097-32-2) Halogen-Iodine (I) (CAS No.: 14362-44-8) mg/kg With reference to IEC 62321-8:2017. Analysis was performed by GC/MS. mg/kg With reference to IEC 62321-8:2017. Analysis was performed by GC/MS. mg/kg With reference to IEC 62321-8:2017. Analysis was performed by GC/MS. mg/kg With reference to IEC 62321-8:2017. Analysis was performed by GC/MS. mg/kg With reference to BS EN 14582:2016. Analysis was performed by IC. mg/kg With reference to BS EN 14582:2016. Analysis was performed by IC. mg/kg With reference to BS EN 14582:2016. Analysis was performed by IC. mg/kg With reference to BS EN 14582:2016. Analysis was performed by IC. MDL Result No.1 Note: 1. mg/kg = ppm;0.1wt% = 1000ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 5. This report supersedes all previous documents bearing the test report number KA/201X/XXXXX. 6. This is the additional test report of KA/201X/XXXXX which was issued on yyyy/mm/dd. Please refer to KA/201X/XXXXX for original information.
Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 4 of 8 Analytical flow chart of Heavy Metal These samples were dissolved totally by pre-conditioning method according to below flow chart. ( Cr 6+ test method excluded) Technician : Jony Liu Supervisor: Ray Chang Cutting Preparation Sample Measurement Pb/Cd/Hg Cr 6+ Microwave digestion / Hotplate digestion Non-metal Metal Solution Filtration Residue 1) Alkali fusion 2) HCl to dissolve ABS / PC / PVC Dissolving by ultrasonication Digesting at 60 by ultrasonication Others Digesting at 150~160 Separating to get aqueous phase Boiling water extraction Cool, filter digestate through filter Filtration ICP-AES ph adjustment Add diphenyl-carbazide for color development Add diphenylcarbazide for color development Measure the absorbance at 540 nm by UV-VIS Measure the absorbance at 540 nm by UV-VIS
Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 5 of 8 PBB/PBDE analytical FLOW CHART 1) Name of the person who made measurement: Dorothy Chen 2) Name of the person in charge of measurement: Ray Chang Sample Sample pretreatment Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report
Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 6 of 8 Analytical flow chart of phthalate content Name of the person who made measurement: Dorothy Chen Name of the person in charge of measurement: Ray Chang Test method: IEC 62321-8 Sample pretreatment/separation Sample dissolved/extracted by THF Dilute Extracted solution Analysis was performed by GC/MS Data
Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 7 of 8 Analytical flow chart of halogen content 1) Name of the person who made measurement: Jean Hung 2) Name of the person in charge of measurement: Ray Chang Sample picture and report number Sample pretreatment/separation Weighting and putting sample in cell Oxygen Bomb Combustion /Absorption Dilution to fixed volume Analysis was performed by IC
Chemical Laboratory - Kao., Test Report No. : KE/2018/11379 Date : 2018/01/25 Page : 8 of 8 * The tested sample / part is marked by an arrow if it's shown on the photo. * ** End of Report **