ECH 4615 PLANT DESIGN Spring 12

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ECH 4615 PLANT DESIGN Spring 12 Core Instruction Team: Prof. Dr. Aydin K. Sunol, ENC 3217 Ext: 4-3566 E-Mail: asunol@usf.edu Rana Falahat: rfalahat@mail.usf.edu ENG 301 Rosanna Ayala ENC 3205, 4-5861 e-mail: rayala@mail.usf.edu Prerequisites: Reacting Systems (pre), Process Controls(co), Eng. Econ or CI Class Hours and Place: Main Lecture: TTh 8:00-9:15, EDU 347 Tutorial / labs Sec 1: Th 2-4 45, ENB 116 Sec 2: Th 5 15-8 ENB 228 Group meetings will be arranged later and held at the UG Design lab ENC 2001 Office Hours: Prof. Sunol- M 10-11 AM; TTH 9:30-11 AM Also by Appointment Rosanna Ayala F 10-12 Rana Falahat W 11AM-1PM Required Text: Analysis, Synthesis, and Design of Chemical Processes, Turton, Baillie, Whiting, Swaeiwitz, Prentice Hall, 2002, 3 rd edition Grading: The letter grade you are guaranteed for a given performance is follows: 500-549 = D + 550-599 = C - 600-649 = C 650-699 = C + 700-749 = B - 750-799 = B 800-849 = B + 850-899 = A - 900-949 = A 950 + = A + The relative weights of various tasks is PROJECTS Group Design Project-Report 200 pts Progress 50 pts Presentation 75 pts Poster Presentation 75 pts Announced Quizzes (Best 8 out of 10) 200 pts Homework/Tutorials/Mini projects 250 pts Final Exam 150 pts There will be no make-ups for Quizzes. Class participation and contributions may improve your final grade by a letter, e.g. B to B+. The AIChE safety certification will provide a + enhancement of your final letter grade. The password for USF students at Sache http://sache.org/login.asp is usfbulls The completion of course requires successful completion of ALL the design project requirements.

Policies Regarding Management of the Course and Computer Usage 1. A late penalty of 10 % of the total available points/day will be applied for works turned after due date and hour. Maximum late penalty is 50%. After a solution is posted, no credits will be given. 2. You could use any electronic means and machine language to solve the assigned work. I am only interested in the technical quality of the engineering solutions and their efficient communication. However, I will discuss the pros and cons of software/hardware for your benefit. 3. The quality of answers/time you may get from me or your TA will improve significantly through use of electronic means, scheduled meetings, and visits during office hours 4. We will occasionally broadcast news (e.g. hints for solution of HW) through electronic means. 5. We may require you to submit copies of your work/computer programs via electronic means. 6. I will start and the end the class at the scheduled time, late arrivals and early departures distract me and your cohorts are not considered proper professional conduct, except in cases of emergency. 7. No food is allowed during lecture and workshops.

Objectives of the Course Upon completion of this course, you should be able to: Understand how chemical products enhance our standard of living individually and collectively. Discuss social (e.g. job) and economic (e.g. profit) impact of a chemical product, enterprise in the chemical business, and a chemical manufacturing facility on the various elements of the society and environment. Produce a conceptual design that is economically and technically feasible in addition to satisfying one or more of the following constraints/objectives: environmental, safety, flexibility, reliability, operability, ethics, national security, controllability. Estimate feasibility of a project, starting from material and energy balances, through equipment sizing, cost estimation, and profitability analysis. Make the sound decision, faced with a set of alternatives, by employing the appropriate technical and economic feasibility criteria. Make engineering assumptions. Learn to make decisions when multiple, possibly conflicting, objectives (criteria) exist. Learn to make decisions with limited available information. Use computer aided design tools and sensitivity analysis effectively. Analyze and evaluate information related to chemical plant and product design critically. Schedule various synthesis and analysis techniques to solve process and product systems engineering problems effectively. Communicate results of a major design project through a written report and professional presentation. Work in a group productively

See coverage from lecture outline REFERENCES (A subset of the List is placed in the library reserve) Popular Process and Product Design Texts 1. "Systematic Methods of Chemical Process Design" Biegler, Grossmann, Westerberg, Prentice Hall, 1997 2. Conceptual Design of Chemical Processes, James M. Douglas, McGraw-Hill, 1988 3. Strategy of process Engineering, Rudd and Watson, Wiley, 1968 4. Plant Design and Economics for Chemical Engineers, Max S. Peters and Klaus D. Timmerhaus, McGraw-Hill, 5 th Edition, 2003 5. A Guide To Chemical Engineering Process Design And Economics, Gael Ulrich, Wiley, 1984 6. Coulson and Richardson 's Chemical Engineering: Volume 6. Design: R.K. Sinnott, Towler 5th edition. B-H, 2009 7. Analysis, Synthesis, and Design of Chemical Processes, Turton, Baillie, Whiting, Swaeiwitz, Prentice Hall, 2002, 2 nd edition 8. Product and Process Design Principles: Synthesis, analysis, and evaluation Seider, Seader, Levin Wiley, 3rd edition, 2009 9. Process Design and Engineering Practice, Woods, D.R., Prentice-Hall, 1995 10. Engineering Design: A Materials and Processing Approach, Dieter, 3rd. Ed. McGraw Hill, 2000 11. Chemical Process: Design and Integration Smith, McGraw Hill, 2 nd ed., 2005 12. Chemical Product Design by Cussler and Moggridge, Cambridge Press, 2 nd ed, 2011

General References G1. Kirk-Othmer Encyclopedia of Chemical Technology* 5 th edition; Wiley Inter-science, 2007 G2. Encyclopedia of Chemical Processing and Design* McKetta ed., Marcel Decker, 1993 G3. Ullmann s Encyclopedia of Industrial Chemistry * 7 th ed., Wiley, 2011 G4. Perry's Chemical Engineering Handbook, 8 th ed. Green and Perry(eds.) McGraw Hill, 2008 G5. Chemical Process Equipment Selection and Design, Couper, Penney, Fair, Walas, Butterworth, 2005 The data sources for thermo-physical properties P1. The Properties of Gases and Liquids Poling, Prausnitz, O Connell, McGraw-Hill 5 th Edition, 2001. P2. Vapor-Liquid Equilibrium Data Collection, Gmehling, Onken, Arlt, Grenzeuser, DECHEMA, 1980 * several volumes. Chemical industry, chemical products, employment, C1. The Chemical Process Industries Infrastructure Couper, Beasley, and Penney, Marcel Dekker, 2001 * These multi-volume series are at the library reference section.

Specialized books/manuals S1. Pollution Prevention for Chemical Processes Allen and Rosselot, Wiley, 1997 S2. Handbook of Chemical Technology and Pollution Control, Hocking, Academic Press, 1998 S4. Green Engineering Allen and Shonnard, Prentice Hall, 2002 S5. Chemical Process Safety: Fundamentals with Applications, Crowl and Louvar, Pearson Education- 2011 3rd Edition S6. National Institute for Occupational Safety and Health, pocket guide to Chemical Hazards, NIOSH, 1987 Important Online Sources http://www.aiche.org/ http://sache.org/index.asp http://webbook.nist.gov/chemistry/ http://www.epa.gov/nrmrl/std/cppb/war/sim_war.htm

TOPICAL OUTLINE OF THE LECTURES Lecture 1. Jan 10 th Lecture 2. Jan 12 th Lecture 3. Jan 17 th Lecture 4. Jan 19 th Lecture 5. Jan 24 rd Lecture 6. Jan 26 th Lecture 7. Jan 31 st Lecture 8. Feb 2 nd Lecture 9. Feb 7 th Lecture 10. Feb 9 th Lecture 11. Feb 14 th Lecture 12. Feb 16 th Lecture 13. Feb 21 th Course outline Process Design Case Studies Workshop 1: Chemcad Tutorial Q1: M&E Balances. Q2. CHE Thermo. Product Design. Product Design Case Studies Workshop 2: COMSOL Q3. Reactors. Reactor Design: Reactor type and operating parameter selection Reactor Design: Design and instrumentation of reactors Workshop 3: Reactor Design Workshop Q4. Transport Phenomena. Environmental Impact Analysis and Green Engineering Waste Treatment Workshop 4: WAR Algorithm. Environmental Impact Analysis Q5. Mass transfer and Separation Processes: Separation Processes: Separation technology selection, Synthesis of separation systems Design and costing of Separation Units Workshop 5: Properties Estimation and Regression using Chemcad Q6. Heat Transfer. Heat Transfer: Selection and Design of heat exchange media and operating conditions; Review of heat transfer coefficient relations; Heat Transfer: Synthesis of heat exchange networks Workshop 6: Heat Exchanger Networks, Pinch Method Q7. Fluid Flow. Fluid Flow and Materials Handling Equipment Selection

Lecture 14. Feb 23 st Lecture 15. Feb 28 th Lecture 16. Mar 1 st Lecture 17. Mar 6 th Lecture 18. Mar 8 th Lecture 19. Mar 20 th Lecture 20. Mar 22 th Fluid Flow and Materials Handling Equipment Selection Workshop 7 : Chemcad Fluid Distribution System Design Q8. Environment and Safety; Risk assessment and Safety Risk assessment and Safety Workshop 8 : Workshop Relief Systems Q9. Design Trouble Shooting Report writing and technical presentations Workshop 9: Scheduling Problems Q10. Engineering Economics. Supply Chain Optimization Linear Programming Workshop 10. Linear Programming Design Presentations April 17 th, 19 th lecture period and April 19 th Workshop Capstone Design Poster Day: Apr 27 th Final Exam May 1 st 7:30-9:30 AM

Project Milestones Process Design Project Product Design Project Due Date Process Flowsheet Product Design Concepts January 31 th Material and Energy Balances Concept Selection February 14 th Equipment Sizing Product Design February 28 th Economic Feasibility Manufacturing and Economic Analysis March 7 th Group Project Draft Due Date: 5 PM April 4 th, 2011 Project reviews April 10 and 12 Group Presentations: April 17, 19 Final Electronic copy of report and presentation April 20 nd Poster Presentations due April 23 Project Poster Presentations: April 27 th

Project for Spring 2012 You are expected to produce a conceptual design that is economically and technically feasible in addition to satisfying the following constraints/objectives: environmental, safety, flexibility, reliability, operability, ethics, national security, controllability. The requirements include: participation in the group activities and meetings, written group report, oral group presentation to a technical audience and poster presentation to a general audience. The project areas: A Nutraceutical Products and Timed/Controlled Release Products B. AIChE Contest problem C. Energy Related Processes and Products D Alcohol free beverage process/products E. Biomedical and Biological Groups will be assigned. Please fill this form and turn it in Your Name: Personality type The project areas I am interested in: (List at most three in the order of preference) The three people I will like to work with: The two people I will not like to work with: